3,4-DIHYDROQUINAZOLIN-2(1H)-ONE

Product Name: 3,4-DIHYDROQUINAZOLIN-2(1H)-ONE
CAS No.: 66655-67-2
Chemical Name: 3,4-DIHYDROQUINAZOLIN-2(1H)-ONE
Synonyms: 3,4-Dihydro-1H-quizolin-2-one;3,4-DIHYDROQUINAZOLIN-2(1H)-ONE;3,4-Dihydro-2(1H)-quinazolinone;3,4-DIHYDRO-1H-QUINAZOLIN-2-ONE;2(1H)-Quinazolinone, 3,4-dihydro-;1,2,3,4-tetrahydroquinazolin-2-one
CBNumber: CB52463929
Molecular Formula: C8H8N2O
Formula Weight: 148.16
MOL File: 66655-67-2.mol

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3,4-DIHYDROQUINAZOLIN-2(1H)-ONE Property

Melting point:: 241-242℃
Boiling point:: 257℃
Density: 1.19
Flash point:: 120℃
storage temp.: Sealed in dry,Room Temperature
pka: 12?+-.0.20(Predicted)

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: D456150
Product name: 3,4-Dihydroquinazolin-2(1H)-one
Packaging: 10mg
Price: $45
Updated: 2021/12/16

AK Scientific

Product number: 2076AJ
Product name: 3,4-Dihydro-1H-quinazolin-2-one
Packaging: 250mg
Price: $315
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0298300
Product name: 3,4-DIHYDRO-1H-QUINAZOLIN-2-ONE
Purity: 95.00%
Packaging: 5MG
Price: $498.63
Updated: 2021/12/16

AK Scientific

Product number: 2076AJ
Product name: 3,4-Dihydro-1H-quinazolin-2-one
Packaging: 5g
Price: $3164
Updated: 2021/12/16

J&W Pharmlab

Product number: 70R0384
Product name: 3,4-Dihydro-1H-quinazolin-2-one
Purity: 96%
Packaging: 1g
Price: $549
Updated: 2021/12/16

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3,4-DIHYDROQUINAZOLIN-2(1H)-ONE Chemical Properties,Usage,Production

Synthesis

4403-69-4

13939-06-5

66655-67-2

The general procedure for the synthesis of 3,4-dihydro-1H-quinazolin-2-one from 2-aminobenzylamine and molybdenum hexacarbonyl was as follows: the reaction was carried out in a two-chamber system. First, 2-aminobenzylamine, Pd(OAc)2 (0.05 eq.) and Cu(OAc)2 (0.5 eq.) were added to the reaction chamber and dissolved in 1,4-dioxane (2 mL). In a CO chamber, Mo(CO)6 (200 mg) was dissolved in 1,4-dioxane (2 mL). Subsequently, 1,8-diazabicyclo[5.4.0]undec-7-ene was added to the system. The two-compartment system was placed in a Dry-Syn heating block and heated to 95°C for the reaction. Upon completion of the reaction, the reaction mixture was filtered through a short silica gel plug and subsequently purified by fast column chromatography.

References

[1] Molecules, 2017, vol. 22, # 10,

3,4-DIHYDROQUINAZOLIN-2(1H)-ONE Preparation Products And Raw materials

Raw materials

Preparation Products

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3,4-DIHYDROQUINAZOLIN-2(1H)-ONE Suppliers

China 40 India 1 United States 2 Global 43

SynAsst Chemical.

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ShangHai AmK Pharmaceutical Technology Co., Ltd.

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JW & Y Pharmlab Co., Ltd.

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Shanghai ZiHao Pharmaceutical Co., Ltd.

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Shanghai SPAR pharmaceutical technology co., LTD

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Shanghai Jizhi Biochemical Technology Co. Ltd.

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66655-67-2, 3,4-DIHYDROQUINAZOLIN-2(1H)-ONERelated Search:

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3,4-DIHYDROQUINAZOLIN-2(1H)-ONE

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66655-67-2

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