ChemicalBook > CAS DataBase List > 2,6-Dichloro-4-iodophenol

2,6-Dichloro-4-iodophenol

Product Name: 2,6-Dichloro-4-iodophenol
CAS No.: 34074-22-1
Chemical Name: 2,6-Dichloro-4-iodophenol
Synonyms: 2,6-Dichloro-4-iodophenol;Phenol, 2,6-dichloro-4-iodo-;2,6-Dichloro-4-iodophenol 98%
CBNumber: CB52665365
Molecular Formula: C6H3Cl2IO
Formula Weight: 288.9
MOL File: 34074-22-1.mol

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2,6-Dichloro-4-iodophenol Property

Melting point:: 91-92 °C
Boiling point:: 278.2±40.0 °C(Predicted)
Density: 2.158±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 6.42±0.23(Predicted)
Appearance: White to off-white Solid

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Safety

HS Code: 2908190090

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

ChemScene

Product number: CS-0031438
Product name: 2,6-Dichloro-4-iodophenol
Purity: ≥98.0%
Packaging: 1g
Price: $40
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2601-M-00
Product name: 2,6-Dichloro-4-iodophenol
Packaging: 250mg
Price: $92
Updated: 2021/12/16

Matrix Scientific

Product number: 096476
Product name: 2,6-Dichloro-4-iodophenol
Purity: 95+%
Packaging: 250mg
Price: $167
Updated: 2021/12/16

ChemScene

Product number: CS-0031438
Product name: 2,6-Dichloro-4-iodophenol
Purity: ≥98.0%
Packaging: 5g
Price: $195
Updated: 2021/12/16

Matrix Scientific

Product number: 096476
Product name: 2,6-Dichloro-4-iodophenol
Purity: 95+%
Packaging: 1g
Price: $370
Updated: 2021/12/16

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2,6-Dichloro-4-iodophenol Chemical Properties,Usage,Production

Synthesis

87-65-0

34074-22-1

The general procedure for the synthesis of 2,6-dichloro-4-iodophenol from 2,6-dichlorophenol was as follows: 2,6-dichlorophenol (10 g, 61.35 mmol, 1.00 eq.) and N-iodosuccinimide (NIS, 27.6 g, 245.33 mmol, 2.00 eq.) were dissolved in methanol (100 mL) and stirred at room temperature for 1 hour. After completion of the reaction, the mixture was concentrated under reduced pressure. The concentrated residue was redissolved in ethyl acetate (50 mL) and washed with saturated saline (3 x 30 mL). The organic layer was dried over anhydrous sodium sulfate and concentrated under reduced pressure. The residue was purified by silica gel column chromatography using petroleum ether (100%) as eluent to afford 2,6-dichloro-4-iodophenol (10.5 g, 59% yield) as a yellow solid.1H-NMR (300 MHz, CDCl3): δ 9.83 (s, 1H), 7.27 (s, 2H) ppm.

References

[1] Patent: WO2006/100026, 2006, A1. Location in patent: Page/Page column 121
[2] Synthetic Communications, 2014, vol. 44, # 14, p. 2094 - 2102
[3] Journal of the Brazilian Chemical Society, 2010, vol. 21, # 4, p. 770 - 774
[4] Synthetic Communications, 2012, vol. 42, # 16, p. 2407 - 2414
[5] Advanced Synthesis and Catalysis, 2013, vol. 355, # 14-15, p. 2936 - 2941

2,6-Dichloro-4-iodophenol Preparation Products And Raw materials

Raw materials

Preparation Products

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34074-22-1, 2,6-Dichloro-4-iodophenolRelated Search:

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Phenol, 2,6-dichloro-4-iodo-

2,6-Dichloro-4-iodophenol

2,6-Dichloro-4-iodophenol 98%

34074-22-1