ChemicalBook > CAS DataBase List > 1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE

1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE

Product Name
1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE
CAS No.
57616-69-0
Chemical Name
1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE
Synonyms
CEDI-010;(3-Chloropropyl)pyrrolidine Hydrochloride;N-(3-Chloropropyl)pyrrolidine Hydrochloride;1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE
CBNumber
CB5361951
Molecular Formula
C7H15Cl2N
Formula Weight
184.11
MOL File
57616-69-0.mol
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1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE Property

Melting point:
134-136 °C
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
form 
fused solid
color 
Brown
InChI
InChI=1S/C7H14ClN.ClH/c8-4-3-7-9-5-1-2-6-9;/h1-7H2;1H
InChIKey
UUPCYQIIQHSPKR-UHFFFAOYSA-N
SMILES
C1CN(CCCCl)CC1.Cl
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Safety

HazardClass 
IRRITANT
HS Code 
2933998090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
C350965
Product name
(3-Chloropropyl)pyrrolidineHydrochloride
Packaging
100mg
Price
$45
Updated
2021/12/16
TRC
Product number
C350965
Product name
(3-Chloropropyl)pyrrolidineHydrochloride
Packaging
1g
Price
$75
Updated
2021/12/16
AK Scientific
Product number
J94644
Product name
(3-Chloropropyl)pyrrolidineHCl
Packaging
10g
Price
$80
Updated
2021/12/16
Biosynth Carbosynth
Product number
FC74715
Product name
1-(3-Chloropropyl)-pyrrolidine hydrochloride
Packaging
2g
Price
$100
Updated
2021/12/16
Biosynth Carbosynth
Product number
FC74715
Product name
1-(3-Chloropropyl)-pyrrolidine hydrochloride
Packaging
1g
Price
$60
Updated
2021/12/16
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1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE Chemical Properties,Usage,Production

Synthesis

123-75-1

627-30-5

57616-69-0

165 mL (2 mol) of tetrandrine, 67 mL (1 mol) of 3-chloro-1-propanol and 200 mL of toluene were added sequentially to the reaction flask. The reaction mixture was heated to reflux temperature and maintained for 3 hours. Upon completion of the reaction, it was cooled to room temperature and the solid product was isolated. The solid was collected by diafiltration and the filter cake was washed with 20 mL of toluene. The temperature of the filtrate was controlled at about 75°C and 200 mL of thionyl chloride was slowly added dropwise. After the dropwise addition, the reaction was refluxed for 2 hours. At the end of the reaction, the mixture was cooled to room temperature and subsequently concentrated to dryness under reduced pressure. The resulting residue was recrystallized from anhydrous ethanol to give 105 g of the final white solid product N-(3-chloropropyl)pyrrole hydrochloride in 62.3% yield with a melting point of 169-173°C.

References

[1] Patent: US2013/85140, 2013, A1. Location in patent: Paragraph 0070; 0071

1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE Suppliers

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View Lastest Price from 1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE manufacturers

Career Henan Chemical Co
Product
1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE 57616-69-0
Price
US $1.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
1lg; 2kg; 5kg; 10kg; 100kg
Release date
2019-08-31

57616-69-0, 1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDERelated Search:

Pyrrolidine 1-(3-CHLOROPROPYL)-PYRROLIDINE 1-(3-CHLORO-3-PHENYLPROPYL)PYRROLIDINE HYDROCHLORIDE 5-CHLORO-6-((2-IMINOPYRROLIDIN-1-YL)METHYL)-5,6-DIHYDROPYRIMIDIN-4(3H)-ONE HYDROCHLORIDE 1-[(2,2-DICHLOROCYCLOPROPYL)METHYL]PYRROLIDINE 1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE

  • 1-(3-CHLOROPROPYL)-PYRROLIDINE HYDROCHLORIDE
  • (3-Chloropropyl)pyrrolidine Hydrochloride
  • N-(3-Chloropropyl)pyrrolidine Hydrochloride
  • CEDI-010
  • 57616-69-0
  • Amines and Anilines