ChemicalBook > CAS DataBase List > DIPHENYLIODONIUM TRIFLUOROMETHANESULFONATE

DIPHENYLIODONIUM TRIFLUOROMETHANESULFONATE

Uses

Product Name: DIPHENYLIODONIUM TRIFLUOROMETHANESULFONATE
CAS No.: 66003-76-7
Chemical Name: DIPHENYLIODONIUM TRIFLUOROMETHANESULFONATE
Synonyms: DIPHENYLIODONIUM TRIFLATE;DPIT;DIPHENYLIODONIUM TRIFLATE , ELECTRO;DIPHENYLIODONIUM TRIFLATE, 99+%, ELECTRO;Diphenyliodonium trifluoromethansulfonate;DIPHENYLIODONIUM TRIFLUOROMETHANESULFONATE;DIPHENYLIODONIUM TRIFLUOROMETHANESULPHONATE;DiphenyliodoniumTrifluoromethanesulfonate>Diphenyliodoniumtrifluoromethanesulphonate98%;Diphenyliodonium trifluoromethanesulphonate 98%
CBNumber: CB5395554
Molecular Formula: C12H10I.CF3O3S
Formula Weight: 430.18
MOL File: 66003-76-7.mol

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DIPHENYLIODONIUM TRIFLUOROMETHANESULFONATE Property

Melting point:: 180-181 °C (lit.)
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
solubility: PGMEA: ~1%
form: Crystalline Powder
color: White to slightly yellow
Sensitive: Light Sensitive
BRN: 3582403
InChI: InChI=1S/C12H10I.CHF3O3S/c1-3-7-11(8-4-1)13-12-9-5-2-6-10-12;2-1(3,4)8(5,6)7/h1-10H;(H,5,6,7)/q+1;/p-1
InChIKey: SBQIJPBUMNWUKN-UHFFFAOYSA-M
SMILES: C1(C=CC=CC=1)[I+]C1=CC=CC=C1.C(F)(F)(F)S([O-])(=O)=O
CAS DataBase Reference: 66003-76-7(CAS DataBase Reference)
EPA Substance Registry System: Iodonium, diphenyl-, 1,1,1-trifluoromethanesulfonate (1:1) (66003-76-7)

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-36
WGK Germany: 3
F: 8-10
Hazard Note: Irritant
HazardClass: 6.1
HS Code: 29319090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 530972
Product name: Diphenyliodonium triflate
Purity: electronic grade, ≥99%
Packaging: 1g
Price: $132.72
Updated: 2025/07/31

TCI Chemical

Product number: D2253
Product name: Diphenyliodonium Trifluoromethanesulfonate
Purity: >98.0%(T)
Packaging: 1g
Price: $84
Updated: 2025/07/31

TCI Chemical

Product number: D2253
Product name: Diphenyliodonium Trifluoromethanesulfonate
Purity: >98.0%(T)
Packaging: 5g
Price: $261
Updated: 2025/07/31

TCI Chemical

Product number: D2253
Product name: Diphenyliodonium Trifluoromethanesulfonate
Purity: >98.0%(T)
Packaging: 25g
Price: $859
Updated: 2025/07/31

TRC

Product number: D494955
Product name: Diphenyliodonium Trifluoromethanesulfonate
Packaging: 50mg
Price: $60
Updated: 2021/12/16

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DIPHENYLIODONIUM TRIFLUOROMETHANESULFONATE Chemical Properties,Usage,Production

Uses

Diphenyliodonium Trifluoromethanesulfonate is a useful research chemical.

Uses

Reagent for phenylation.

Uses

Cationic photoinitiator. Photoacid generator.

Synthesis

591-50-4

1493-13-6

71-43-2

66003-76-7

5.5 mmol of m-chloroperoxybenzoic acid as an oxidizing agent was added to the reaction flask along with 5.5 mmol of iodobenzene, 15 mL of dichloromethane, 5 mmol of benzene, 10 mmol of trifluoromethanesulfonic acid, and a stirrer, and a condensation tube was installed to condense the reaction from the bottom to the top at room temperature. Subsequently, the reaction flask was heated in an oil bath at 40 °C for the condensation reflux reaction. The reaction was continued under magnetic stirring for 1 hour. Upon completion of the reaction, the reaction solution was rotary dried using a rotary evaporator (40 °C water bath). To the dried product, 20 mL of ether was added and stirred at room temperature for 30 min, after which the mixture was cooled in a 0-4 °C medical refrigerator for 15 min. After removal, the mixture was withdrawn and filtered through a Büchner funnel using ether as eluent. The solid product on the filter paper was collected and dried in an oven at 100 °C for 24 h. Diaryl iodonium trifluoromethanesulfonate was finally obtained in 88% yield. During rotary drying, the control conditions were 0.1 MPa and 40 °C.

References

[1] Organic Letters, 2011, vol. 13, # 13, p. 3462 - 3465
[2] Chemistry--A European Journal, 2012, vol. 18, # 44, p. 14140 - 14149,10
[3] Organic Letters, 2015, vol. 17, # 18, p. 4554 - 4557
[4] Organic Letters, 2015, vol. 17, # 11, p. 2688 - 2691
[5] Angewandte Chemie - International Edition, 2016, vol. 55, # 31, p. 8928 - 8932

DIPHENYLIODONIUM TRIFLUOROMETHANESULFONATE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from DIPHENYLIODONIUM TRIFLUOROMETHANESULFONATE manufacturers

LY Global chemicals co.,ltd .

Product: DIPHENYLIODONIUM TRIFLUOROMETHANESULFONATE 66003-76-7
Price: US $0.00/kg
Min. Order: 1kg
Purity: 98.0%min
Supply Ability: 100kg
Release date: 2023-03-20

Career Henan Chemical Co

Product: DIPHENYLIODONIUM TRIFLUOROMETHANESULFONATE 66003-76-7
Price: US $3.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 200KG
Release date: 2020-01-08

66003-76-7, DIPHENYLIODONIUM TRIFLUOROMETHANESULFONATERelated Search:

Diphenylacetyl chloride O-Diphenylphosphinylhydroxylamine Diphenyl(trimethylsilyl)phosphine Perfluoro-1-iodohexane Perfluorobutyl iodide Scandium trifluoromethanesulfonate FLUOROSULFONIC ACID Dess-Martin periodinane Trifluoromethanesulfonic acid DIPHENYLIODONIUM IODIDE (4-METHOXYPHENYL)PHENYLIODONIUM TRIFLATE DIPHENYLIODONIUM TRIFLUOROMETHANESULFONATE PHENYL[2-(TRIMETHYLSILYL)PHENYL]IODONIUM TRIFLATE BIS(4-TERT-BUTYLPHENYL)IODONIUM TRIFLATE Trifluoromethane

DIPHENYLIODONIUM TRIFLATE

DIPHENYLIODONIUM TRIFLUOROMETHANESULFONATE

DIPHENYLIODONIUM TRIFLUOROMETHANESULPHONATE

DIPHENYLIODONIUM TRIFLATE, 99+%, ELECTRO

Diphenyliodonium trifluoromethanesulphonate 98%

Diphenyliodoniumtrifluoromethanesulphonate98%

Diphenyliodonium·trifluoromethanesulfonic acidanion

Diphenyliodonium triflate,Diphenyliodonium trifluoromethanesulfonate

Diphenyliodonium trifluoromethansulfonate

Diphenyliodonium trifluoromethanesulfonic acid salt

DPIT

Diphenyliodonium triflate electronic grade, >=99%

Iodonium, diphenyl-, 1,1,1-trifluoromethanesulfonate (1:1)

DIPHENYLIODONIUM TRIFLATE , ELECTRO

DiphenyliodoniumTrifluoromethanesulfonate&gt

Diphenyliodonium trifluoromethanesulfonate, 99%,

66003-76-7

C13H10F3lO3S

C6H52ICF3So3

C12H10ICF3O3S

C13H10F3IO3S

Hypervalent Iodine

Oxidation

Synthetic Reagents

Iodonium Sulfonium & Oxonium Compounds

Diphenyliodonium Compounds

Hypervalent Iodine Compounds

Photopolymerization Initiators

Diphenyliodonium Compounds

Functional Materials

Hypervalent Iodine Compounds

Iodonium Sulfonium & Oxonium Compounds

Photopolymerization Initiators

Synthetic Organic Chemistry