1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE
- Product Name
- 1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE
- CAS No.
- 439811-37-7
- Chemical Name
- 1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE
- Synonyms
- 1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE;tert-butyl 4-(4-broMobenzoyl)piperidine-1-carboxylate;tert-butyl 4-[(4-broMophenyl)carbonyl]piperidine-1-carboxylate;4-(4-bromobenzoyl)piperidine-1-carboxylic acid tert-butyl ester;1-Piperidinecarboxylic acid, 4-(4-bromobenzoyl)-, 1,1-dimethylethyl ester
- CBNumber
- CB5413232
- Molecular Formula
- C17H22BrNO3
- Formula Weight
- 368.27
- MOL File
- 439811-37-7.mol
1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE Property
- Boiling point:
- 452.3±40.0 °C(Predicted)
- Density
- 1.325±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C
- pka
- -2.47±0.40(Predicted)
- Appearance
- Off-white to light yellow Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P403+P233Store in a well-ventilated place. Keep container tightly closed.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- B200940
- Product name
- 1-Boc-4-(4-bromo-benzoyl)-piperidine
- Packaging
- 100mg
- Price
- $100
- Updated
- 2021/12/16
- Product number
- B200940
- Product name
- 1-Boc-4-(4-bromo-benzoyl)-piperidine
- Packaging
- 250mg
- Price
- $200
- Updated
- 2021/12/16
- Product number
- FB51872
- Product name
- 1-Boc-4-(4-bromo-benzoyl)piperidine
- Packaging
- 500mg
- Price
- $220
- Updated
- 2021/12/16
- Product number
- 074243
- Product name
- 1-Boc-4-(4-Bromobenzoyl)piperidine
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $231
- Updated
- 2021/12/16
- Product number
- FB51872
- Product name
- 1-Boc-4-(4-bromo-benzoyl)piperidine
- Packaging
- 100mg
- Price
- $111
- Updated
- 2021/12/16
1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE Chemical Properties,Usage,Production
Synthesis
746550-66-3
24424-99-5
439811-37-7
Step 1. Synthesis of tert-butyl 4-(4-bromobenzoyl)-piperidine-1-carboxylate. To a 250 mL round bottom flask was added 4-(4-bromobenzoyl)piperidine (5 g, 20 mmol), tetrahydrofuran (30 mL), water (30 mL), sodium carbonate (10 g, 90 mmol) and di-tert-butyl dicarbonate (4.35 g, 20.0 mmol). The reaction mixture was stirred at room temperature for 2 h and then partitioned with ethyl acetate and water. The aqueous layer was extracted twice with ethyl acetate, the organic phases were combined, washed with brine, dried, filtered and concentrated to give 7.1 g (100% yield) of tert-butyl 4-(4-bromobenzoyl)-piperidine-1-carboxylate.
References
[1] Patent: WO2016/205590, 2016, A1. Location in patent: Paragraph 00596
[2] Patent: WO2013/147711, 2013, A1. Location in patent: Page/Page column 231
[3] Patent: US2014/371199, 2014, A1. Location in patent: Paragraph 0801
[4] Patent: US2005/54628, 2005, A1. Location in patent: Page/Page column 23-24
[5] Patent: US2005/49269, 2005, A1. Location in patent: Page/Page column 12; 21
1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE Preparation Products And Raw materials
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View Lastest Price from 1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE manufacturers
- Product
- 1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE 439811-37-7
- Price
- US $9.80/KG
- Min. Order
- 1g
- Purity
- ≥99%
- Supply Ability
- 100kg
- Release date
- 2020-01-08
- Product
- 1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE 439811-37-7
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 95-99%
- Supply Ability
- 1ton
- Release date
- 2020-01-08