ChemicalBook > CAS DataBase List > 1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE

1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE

Product Name
1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE
CAS No.
439811-37-7
Chemical Name
1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE
Synonyms
1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE;tert-butyl 4-(4-broMobenzoyl)piperidine-1-carboxylate;tert-butyl 4-[(4-broMophenyl)carbonyl]piperidine-1-carboxylate;4-(4-bromobenzoyl)piperidine-1-carboxylic acid tert-butyl ester;1-Piperidinecarboxylic acid, 4-(4-bromobenzoyl)-, 1,1-dimethylethyl ester
CBNumber
CB5413232
Molecular Formula
C17H22BrNO3
Formula Weight
368.27
MOL File
439811-37-7.mol
More
Less

1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE Property

Boiling point:
452.3±40.0 °C(Predicted)
Density 
1.325±0.06 g/cm3(Predicted)
storage temp. 
2-8°C
pka
-2.47±0.40(Predicted)
Appearance
Off-white to light yellow Solid
More
Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P403+P233Store in a well-ventilated place. Keep container tightly closed.

P405Store locked up.

P501Dispose of contents/container to..…

More
Less

N-Bromosuccinimide Price

TRC
Product number
B200940
Product name
1-Boc-4-(4-bromo-benzoyl)-piperidine
Packaging
100mg
Price
$100
Updated
2021/12/16
TRC
Product number
B200940
Product name
1-Boc-4-(4-bromo-benzoyl)-piperidine
Packaging
250mg
Price
$200
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB51872
Product name
1-Boc-4-(4-bromo-benzoyl)piperidine
Packaging
50mg
Price
$69.5
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB51872
Product name
1-Boc-4-(4-bromo-benzoyl)piperidine
Packaging
100mg
Price
$111
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB51872
Product name
1-Boc-4-(4-bromo-benzoyl)piperidine
Packaging
250mg
Price
$137.5
Updated
2021/12/16
More
Less

1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE Chemical Properties,Usage,Production

Synthesis

746550-66-3

24424-99-5

439811-37-7

Step 1. Synthesis of tert-butyl 4-(4-bromobenzoyl)-piperidine-1-carboxylate. To a 250 mL round bottom flask was added 4-(4-bromobenzoyl)piperidine (5 g, 20 mmol), tetrahydrofuran (30 mL), water (30 mL), sodium carbonate (10 g, 90 mmol) and di-tert-butyl dicarbonate (4.35 g, 20.0 mmol). The reaction mixture was stirred at room temperature for 2 h and then partitioned with ethyl acetate and water. The aqueous layer was extracted twice with ethyl acetate, the organic phases were combined, washed with brine, dried, filtered and concentrated to give 7.1 g (100% yield) of tert-butyl 4-(4-bromobenzoyl)-piperidine-1-carboxylate.

References

[1] Patent: WO2016/205590, 2016, A1. Location in patent: Paragraph 00596
[2] Patent: WO2013/147711, 2013, A1. Location in patent: Page/Page column 231
[3] Patent: US2014/371199, 2014, A1. Location in patent: Paragraph 0801
[4] Patent: US2005/54628, 2005, A1. Location in patent: Page/Page column 23-24
[5] Patent: US2005/49269, 2005, A1. Location in patent: Page/Page column 12; 21

1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

More
Less

1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE Suppliers

Pure Chemistry Scientific Inc.
Tel
001-857-928-2050 or 1-888-588-9418
Fax
001-617-206-9595
Email
sales@chemreagents.com
Country
United States
ProdList
10186
Advantage
62
Accela ChemBio Co.,Ltd.
Tel
021-50795510 4000665055
Fax
021-50795055
Email
sales@accelachem.com
Country
China
ProdList
11035
Advantage
64
Shanghai Hanhong Scientific Co.,Ltd.
Tel
021-54306202 13764082696
Email
info@hanhongsci.com
Country
China
ProdList
42934
Advantage
64
Chemsky(shanghai)International Co.,Ltd.
Tel
021-50135380
Email
shchemsky@sina.com
Country
China
ProdList
32321
Advantage
50
Shanghai Sphchem Co., Ltd.
Tel
021-56491756 13512199871
Fax
021-5649-1756
Email
2819742715@qq.com
Country
China
ProdList
4000
Advantage
55
Chengdu HappySyn Pharmaceutical Technology Co., Ltd.
Tel
028-85114309 18982182443
Email
yangli@happysyn.com
Country
China
ProdList
2151
Advantage
55
NovoChemy Ltd.
Tel
021-31261262/ 49 (0)17662837245
Fax
(0)21-33250524
Email
sales@novochemy.com
Country
Germany
ProdList
6328
Advantage
58
Shanghai Topbiochem Technology Co., Ltd
Tel
+86-21-60341587
Fax
+86-21-61294319
Email
sales@topbiochem.com
Country
China
ProdList
6175
Advantage
58
Shanghai Yolne Chemical Co., Ltd.
Tel
021-62960152
Fax
021-52212593
Email
934678158@qq.com
Country
China
ProdList
9899
Advantage
55
Taizhou Tongxin Bio-Tech Co., Ltd
Tel
0523-86818997 18652728585
Email
sales@allyrise.com
Country
China
ProdList
2966
Advantage
60
More
Less

View Lastest Price from 1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE manufacturers

Career Henan Chemical Co
Product
1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE 439811-37-7
Price
US $9.80/KG
Min. Order
1g
Purity
≥99%
Supply Ability
100kg
Release date
2020-01-08
Career Henan Chemical Co
Product
1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE 439811-37-7
Price
US $1.00/KG
Min. Order
1KG
Purity
95-99%
Supply Ability
1ton
Release date
2020-01-08

439811-37-7, 1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINERelated Search:


  • 1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE
  • tert-butyl 4-(4-broMobenzoyl)piperidine-1-carboxylate
  • tert-butyl 4-[(4-broMophenyl)carbonyl]piperidine-1-carboxylate
  • 1-Piperidinecarboxylic acid, 4-(4-bromobenzoyl)-, 1,1-dimethylethyl ester
  • 4-(4-bromobenzoyl)piperidine-1-carboxylic acid tert-butyl ester
  • 439811-37-7