Synthesis
ChemicalBook > CAS DataBase List > 2-Amino-3,5-dibromobenzoic acid

2-Amino-3,5-dibromobenzoic acid

Synthesis
Product Name
2-Amino-3,5-dibromobenzoic acid
CAS No.
609-85-8
Chemical Name
2-Amino-3,5-dibromobenzoic acid
Synonyms
NA-693;3,5-DIBROM;Ambroxol-10;Ambroxol Acid;Bromhexine Acid;Ambroxol Imp.16;BUTTPARK 89\07-50;RARECHEM AL BO 1185;3,5-DIBROMOANTHRANILIC ACID;DibromoanthranilicImpurity 1
CBNumber
CB5446030
Molecular Formula
C7H5Br2NO2
Formula Weight
294.93
MOL File
609-85-8.mol
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2-Amino-3,5-dibromobenzoic acid Property

Melting point:
235-236 °C(lit.)
Boiling point:
367.6±42.0 °C(Predicted)
Density 
2.158±0.06 g/cm3(Predicted)
solubility 
DMSO (Slightly), Methanol (Slightly)
pka
4.16±0.10(Predicted)
form 
Powder
color 
White to beige
BRN 
779291
CAS DataBase Reference
609-85-8(CAS DataBase Reference)
NIST Chemistry Reference
3,5-Dibromoanthranilic acid(609-85-8)
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38-37/38-36
Safety Statements 
26-37/39
WGK Germany 
3
HS Code 
29224985
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TCI Chemical
Product number
D4177
Product name
3,5-Dibromoanthranilic Acid
Purity
>98.0%(HPLC)(T)
Packaging
5g
Price
$25
Updated
2024/03/01
TCI Chemical
Product number
D4177
Product name
3,5-Dibromoanthranilic Acid
Purity
>98.0%(HPLC)(T)
Packaging
25g
Price
$87
Updated
2024/03/01
Alfa Aesar
Product number
L07419
Product name
2-Amino-3,5-dibromobenzoic acid, 98%
Packaging
5g
Price
$30.65
Updated
2024/03/01
Alfa Aesar
Product number
L07419
Product name
2-Amino-3,5-dibromobenzoic acid, 98%
Packaging
25g
Price
$86.65
Updated
2024/03/01
TRC
Product number
A610705
Product name
2-Amino-3,5-dibromobenzoicAcid
Packaging
1g
Price
$40
Updated
2021/12/16
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2-Amino-3,5-dibromobenzoic acid Chemical Properties,Usage,Production

Synthesis

A solution of bromine (7.2 g, 2 mL, 40 mmol) in 47 mL glacial acetic acid was added dropwise to sodium 2-aminobenzoate (6.4 g, 40 mmol) in 32 mL of glacial acetic acid  at 15 °С and the mixture was stirred for 1 h at the same temperature. The product  was filtered off, washed with benzene and dried in the dark. The bromobenzoic acids  containing mixture (0.5 g) was added to 10 mL of boiling water followed by the  addition of 1.3 mL of concentrated hydrochloric acid and hot filtration under vacuum.  The insoluble material contained 2-amino-3,5-dibromobenzoic acid, whereas 2- amino-5-bromobenzoic acid precipitated upon cooling of the filtrate. IR (suspension in nujol, cm−1 ): 3469, 3364,  1682, 1600, 1564, 1538, 1454, 1421, 1378, 1328, 1307, 1226, 1063, 902, 882, 790,  711, 691, 591, 543.

Chemical Properties

White to light yellow crystal powder

2-Amino-3,5-dibromobenzoic acid Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-Amino-3,5-dibromobenzoic acid manufacturers

Henan Aochuang Chemical Co.,Ltd.
Product
2-Amino-3,5-dibromobenzoic acid 609-85-8
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
1ton
Release date
2022-10-10
Zhuozhou Wenxi import and Export Co., Ltd
Product
2-Amino-3,5-dibromobenzoic acid 609-85-8
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-06-27
Career Henan Chemical Co
Product
2-Amino-3,5-dibromobenzoic acid 609-85-8
Price
US $6.68/KG
Min. Order
1KG
Purity
97%-99%
Supply Ability
1kg-1000kg
Release date
2020-01-08

609-85-8, 2-Amino-3,5-dibromobenzoic acidRelated Search:


  • Benzoic acid, 2-amino-3,5-dibromo-
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  • Ambroxol-10
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  • 3,5-Dibromoanthranilic acid (DBAA)
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  • 609-85-8
  • Br2C6H22NH2CO2H
  • Aromatic Amino Acids
  • AMINE
  • Peptide Synthesis
  • Specialty Synthesis
  • Unnatural Amino Acid Derivatives
  • Aromatic Carboxylic Acids, Amides, Anilides, Anhydrides & Salts
  • Benzoic acid
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