ChemicalBook > CAS DataBase List > 5-Fluoro-2-iodopyridine

5-Fluoro-2-iodopyridine

Product Name: 5-Fluoro-2-iodopyridine
CAS No.: 159870-80-1
Chemical Name: 5-Fluoro-2-iodopyridine
Synonyms: 2-Iodo-5-Fluoropyridine;5-FLUORO-2-IODOPYRIDINE;Pyridine, 5-fluoro-2-iodo-;5-Fluoro-2-iodopyridine 97%;5-FLUORO-2-IODOPYRIDINE ISO 9001：2015 REACH
CBNumber: CB5451508
Molecular Formula: C5H3FIN
Formula Weight: 222.99
MOL File: 159870-80-1.mol

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5-Fluoro-2-iodopyridine Property

Boiling point:: 197℃
Density: 2.046
Flash point:: 73℃
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: -0.58±0.10(Predicted)
color: yellow to off-white solid

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: F598843
Product name: 5-Fluoro-2-iodopyridine
Packaging: 250mg
Price: $85
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H32-K-33
Product name: 5-Fluoro-2-iodopyridine
Packaging: 250mg
Price: $96
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H32-K-33
Product name: 5-Fluoro-2-iodopyridine
Packaging: 1g
Price: $237
Updated: 2021/12/16

Matrix Scientific

Product number: 076243
Product name: 5-Fluoro-2-iodopyridine
Purity: 95+%
Packaging: 250mg
Price: $297
Updated: 2021/12/16

Apolloscientific

Product number: PC445023
Product name: 5-Fluoro-2-iodopyridine
Purity: 97%
Packaging: 1g
Price: $148
Updated: 2021/12/16

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5-Fluoro-2-iodopyridine Chemical Properties,Usage,Production

Synthesis

41404-58-4

159870-80-1

General procedure for the synthesis of 5-fluoro-2-iodopyridine from 2-bromo-5-fluoropyridine: under nitrogen protection, Cu2O (7.2 mg, 10 mol%), L-proline (11.5 mg, 20 mol%), 2-bromo-5-fluoropyridine (0.50 mmol), potassium iodide (KI, 249 mg, 0.75 mmol) and ethanol (EtOH, 1.5 mL). After sealing the Schlenk tube with a PTFE valve, the reaction mixture was stirred at 110 °C. The reaction process was monitored by gas chromatography (GC) analysis. Upon completion of the reaction, the yield was determined by GC using an appropriate internal standard (e.g., chlorobenzene or 1-chloro-4-methylbenzene) for highly volatile products; or the solvent was removed by distillation under reduced pressure. The resulting crude product was purified by silica gel column chromatography (eluent ratio of petroleum ether/ethyl acetate = 10/1) to give the target product 5-fluoro-2-iodopyridine.

References

[1] Catalysis Today, 2016, vol. 274, p. 129 - 132

5-Fluoro-2-iodopyridine Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 5-Fluoro-2-iodopyridine manufacturers

PNP Biotech Co. Ltd

Product: 5-Fluoro-2-iodopyridine 159870-80-1
Price: US $0.00/kg
Min. Order: 25kg
Purity: 98%
Supply Ability: Inquiry
Release date: 2023-07-12

Shanghai Rlavie Technology Co ltd

Product: 5-Fluoro-2-iodopyridine 159870-80-1
Price: US $0.00-0.00/G
Min. Order: 0.0001G
Purity: 98%min
Supply Ability: 50kgs/month
Release date: 2022-08-18

Dideu Industries Group Limited

Product: 5-FLUORO-2-IODOPYRIDINE 159870-80-1
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons min
Release date: 2021-09-01

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