ChemicalBook > CAS DataBase List > (3-FLUOROBENZYL)METHYLAMINE

(3-FLUOROBENZYL)METHYLAMINE

Product Name: (3-FLUOROBENZYL)METHYLAMINE
CAS No.: 90389-84-7
Chemical Name: (3-FLUOROBENZYL)METHYLAMINE
Synonyms: Aids011076;Aids-011076;(3-FLUOROBENZYL)METH;90389-40-5 (Hydrochloride);(3-FLUOROBENZYL)METHYLAMINE;3-FLUORO-N-METHYLBENZYLAMINE;N-Methyl-3-fluorobenzylamine;(3-Fluorobenzyl)methylamine95%;3-Fluoro-N-methylbenzylamine>3-Fluoro-N-methylbenzylamine ,97%
CBNumber: CB5453087
Molecular Formula: C8H10FN
Formula Weight: 139.17
MOL File: 90389-84-7.mol

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(3-FLUOROBENZYL)METHYLAMINE Property

Boiling point:: 183-184 °C (lit.)
Density: 1.015 g/mL at 25 °C (lit.)
refractive index: n20/D 1.4990(lit.)
Flash point:: 152 °F
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
form: Liquid
pka: 9.39±0.10(Predicted)
color: Colorless to tan

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Safety

Hazard Codes: Xn
Risk Statements: 22-41
Safety Statements: 26-36/39
RIDADR: UN 2735 8/PG III
WGK Germany: 2
HazardClass: 8
PackingGroup: III
HS Code: 29214990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H302Harmful if swallowed

H318Causes serious eye damage

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 631108
Product name: 3-Fluoro-N-methylbenzylamine
Purity: 97%
Packaging: 1g
Price: $36
Updated: 2023/06/20

Sigma-Aldrich

Product number: 631108
Product name: 3-Fluoro-N-methylbenzylamine
Purity: 97%
Packaging: 5g
Price: $146
Updated: 2023/01/07

TCI Chemical

Product number: F0805
Product name: 3-Fluoro-N-methylbenzylamine
Purity: >97.0%(GC)(T)
Packaging: 1g
Price: $36
Updated: 2025/07/31

TRC

Product number: F593120
Product name: 3-Fluoro-n-methylbenzylamine
Packaging: 1g
Price: $75
Updated: 2021/12/16

Frontier Specialty Chemicals

Product number: JK181720
Product name: 3-Fluoro-N-methylbenzylamine
Purity: 97%
Packaging: 1g
Price: $58
Updated: 2021/12/16

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(3-FLUOROBENZYL)METHYLAMINE Chemical Properties,Usage,Production

Chemical Properties

Colorless liquid

Synthesis

74-89-5

456-48-4

90389-84-7

Step A: Methylamine (15.3 mL, 40% aqueous solution, 177 mmol) was slowly added dropwise to a stirred solution of 3-fluorobenzaldehyde (20.0 g, 161 mmol) in methanol (150 mL) at room temperature. The reaction mixture was cooled to 0 °C after 6 h of continuous stirring at room temperature, followed by batchwise addition of sodium borohydride (6.10 g, 161 mmol). After removal of the cooling bath, the reaction mixture was gradually warmed to room temperature and stirring was continued for 16.5 hours. Upon completion of the reaction, the reaction was quenched with deionized water and carefully acidified with 2N hydrochloric acid. The acidified mixture was extracted with dichloromethane (3 times). The aqueous phase was subsequently alkalized with 6N sodium hydroxide solution and again extracted with dichloromethane (4 times). All organic phase extracts were combined, dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure to afford the target product N-methyl-3-fluorobenzylamine (21.51 g, 96% yield) as a clarified oil. Its 1H NMR (300 MHz, CDCl3) data were as follows: δ 7.32 (td, J = 7.5, 1.7 Hz, 1H), 7.28-7.19 (m, 1H), 7.14-6.98 (m, 2H), 3.80 (s, 2H), 2.45 (s, 3H), 1.47 (br s, 1H).

References

[1] Patent: US2006/111393, 2006, A1. Location in patent: Page/Page column 26-27

(3-FLUOROBENZYL)METHYLAMINE Preparation Products And Raw materials

Raw materials

Methylamine Sodium borohydride 3-Fluorobenzaldehyde

Preparation Products

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View Lastest Price from (3-FLUOROBENZYL)METHYLAMINE manufacturers

Career Henan Chemical Co

Product: (3-FLUOROBENZYL)METHYLAMINE 90389-84-7
Price: US $7.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: JD 374
Release date: 2019-09-01

Career Henan Chemical Co

Product: (3-FLUOROBENZYL)METHYLAMINE 90389-84-7
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 25kg
Release date: 2019-07-12

90389-84-7, (3-FLUOROBENZYL)METHYLAMINERelated Search:

(3-Nitrobenzyl)methylamine N-(4-Methoxybenzyl)-N-methylamine (2-FLUOROBENZYL)METHYLAMINE,(2-Fluorobenzyl)methylamine95%,(2-FLUOROBENZYL)METHYLAMINE 95% Flumazenil (4-FLUORO-BENZYL)-METHYL-AMINE 3-Fluorobenzylamine N,N-DIETHYL-3,6-DIFLUOROPHTHALAMIC ACID N-(3-Acetylphenyl)-3-fluorobenzamide TETRAFLUOROPHTHALIMIDE 4-(3-FLUOROBENZYL)MORPHOLINE alpha-Trifluoromethyl-(3-fluorobenzyl)amine Hydrochloride 4-BENZOYL-1-(3-FLUOROBENZYL)-3-METHYL-3,4-DIHYDRO-2(1H)-QUINOXALINONE N-(3,5-DICHLOROPHENYL)-1-(3,4-DIFLUOROBENZYL)-6-OXO-1,6-DIHYDRO-3-PYRIDINECARBOXAMIDE 1-(3,4-DIFLUOROBENZYL)-N-(3,4-DIMETHYLPHENYL)-6-OXO-1,6-DIHYDRO-3-PYRIDINECARBOXAMIDE 6-(4-CHLOROPHENYL)-1-(3-FLUOROBENZYL)-2-OXO-1,2-DIHYDRO-3-PYRIDINECARBONITRILE N1-[3-(2,3,4,5,6-PENTAFLUOROPHENOXY)PHENYL]-3-FLUOROBENZAMIDE 5-(4-CHLOROPHENYL)-1-(3-FLUOROBENZYL)-2-OXO-1,2-DIHYDRO-3-PYRIDINECARBONITRILE METHYL 2-(([1-(3,4-DIFLUOROBENZYL)-6-OXO-1,6-DIHYDRO-3-PYRIDINYL]CARBONYL)AMINO)BENZENECARBOXYLATE

(3-FLUOROBENZYL)METHYLAMINE

3-FLUORO-N-METHYLBENZYLAMINE

(3-Fluorobenzyl)methylamine95%

1-(3-fluorophenyl)-N-methyl-methanamine

90389-40-5 (Hydrochloride)

Aids011076

Aids-011076

Benzenemethanamine, 3-fluoro-N-methyl-

N-Methyl-3-fluorobenzylamine

3-Fluoro-N-methylbenzylamine ,97%

(3-FLUOROBENZYL)METH

(3-fluorophenyl)-N-methylmethanamine

3-Fluoro-<i>N</i>-methylbenzylamine

3-Fluoro-N-methylbenzylamine&gt

90389-84-7

Organic Building Blocks

Nitrogen Compounds

Building Blocks

Amines

API intermediates

Amines

Nitrogen Compounds

Polyamines

Amines and Anilines