(3-FLUOROBENZYL)METHYLAMINE
- Product Name
- (3-FLUOROBENZYL)METHYLAMINE
- CAS No.
- 90389-84-7
- Chemical Name
- (3-FLUOROBENZYL)METHYLAMINE
- Synonyms
- Aids011076;Aids-011076;(3-FLUOROBENZYL)METH;90389-40-5 (Hydrochloride);(3-FLUOROBENZYL)METHYLAMINE;3-FLUORO-N-METHYLBENZYLAMINE;N-Methyl-3-fluorobenzylamine;(3-Fluorobenzyl)methylamine95%;3-Fluoro-N-methylbenzylamine>3-Fluoro-N-methylbenzylamine ,97%
- CBNumber
- CB5453087
- Molecular Formula
- C8H10FN
- Formula Weight
- 139.17
- MOL File
- 90389-84-7.mol
(3-FLUOROBENZYL)METHYLAMINE Property
- Boiling point:
- 183-184 °C (lit.)
- Density
- 1.015 g/mL at 25 °C (lit.)
- refractive index
- n20/D 1.4990(lit.)
- Flash point:
- 152 °F
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- form
- Liquid
- pka
- 9.39±0.10(Predicted)
- color
- Colorless to tan
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H302Harmful if swallowed
H318Causes serious eye damage
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- 631108
- Product name
- 3-Fluoro-N-methylbenzylamine
- Purity
- 97%
- Packaging
- 1g
- Price
- $36
- Updated
- 2023/06/20
- Product number
- 631108
- Product name
- 3-Fluoro-N-methylbenzylamine
- Purity
- 97%
- Packaging
- 5g
- Price
- $146
- Updated
- 2023/01/07
- Product number
- F0805
- Product name
- 3-Fluoro-N-methylbenzylamine
- Purity
- >97.0%(GC)(T)
- Packaging
- 1g
- Price
- $36
- Updated
- 2025/07/31
- Product number
- F593120
- Product name
- 3-Fluoro-n-methylbenzylamine
- Packaging
- 1g
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 071765
- Product name
- (3-Fluorobenzyl)methylamine
- Purity
- 95+%
- Packaging
- 1g
- Price
- $21
- Updated
- 2021/12/16
(3-FLUOROBENZYL)METHYLAMINE Chemical Properties,Usage,Production
Chemical Properties
Colorless liquid
Synthesis
74-89-5
456-48-4
90389-84-7
Step A: Methylamine (15.3 mL, 40% aqueous solution, 177 mmol) was slowly added dropwise to a stirred solution of 3-fluorobenzaldehyde (20.0 g, 161 mmol) in methanol (150 mL) at room temperature. The reaction mixture was cooled to 0 °C after 6 h of continuous stirring at room temperature, followed by batchwise addition of sodium borohydride (6.10 g, 161 mmol). After removal of the cooling bath, the reaction mixture was gradually warmed to room temperature and stirring was continued for 16.5 hours. Upon completion of the reaction, the reaction was quenched with deionized water and carefully acidified with 2N hydrochloric acid. The acidified mixture was extracted with dichloromethane (3 times). The aqueous phase was subsequently alkalized with 6N sodium hydroxide solution and again extracted with dichloromethane (4 times). All organic phase extracts were combined, dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure to afford the target product N-methyl-3-fluorobenzylamine (21.51 g, 96% yield) as a clarified oil. Its 1H NMR (300 MHz, CDCl3) data were as follows: δ 7.32 (td, J = 7.5, 1.7 Hz, 1H), 7.28-7.19 (m, 1H), 7.14-6.98 (m, 2H), 3.80 (s, 2H), 2.45 (s, 3H), 1.47 (br s, 1H).
References
[1] Patent: US2006/111393, 2006, A1. Location in patent: Page/Page column 26-27
(3-FLUOROBENZYL)METHYLAMINE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from (3-FLUOROBENZYL)METHYLAMINE manufacturers
- Product
- (3-FLUOROBENZYL)METHYLAMINE 90389-84-7
- Price
- US $7.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- JD 374
- Release date
- 2019-09-01
- Product
- (3-FLUOROBENZYL)METHYLAMINE 90389-84-7
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 25kg
- Release date
- 2019-07-12