2-CHLORO-5-NITROANISOLE
- Product Name
- 2-CHLORO-5-NITROANISOLE
- CAS No.
- 1009-36-5
- Chemical Name
- 2-CHLORO-5-NITROANISOLE
- Synonyms
- 2-METHOXY-4-NIT;2-Chloro-5-nitropheno;2-CHLORO-5-NITROANISOLE;2-Chloro-5-nitroanisole >2-chloro-5-nitrobenzyl ether;2-METHOXY-4-NITROCHLOROBENZENE;4-Chloro-3-methoxynitrobenzene;1-chloro-2-methoxy-4-nitro-benzen;1-Chloro-2-methoxy-4-nitrobenzene;2-Chloro-5-nitrophenyl methyl ether
- CBNumber
- CB5469406
- Molecular Formula
- C7H6ClNO3
- Formula Weight
- 187.58
- MOL File
- 1009-36-5.mol
2-CHLORO-5-NITROANISOLE Property
- Melting point:
- 81-83°C
- Boiling point:
- 287.3±20.0 °C(Predicted)
- Density
- 1.366±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- solubility
- Chloroform, Ethyl Acetate
- form
- Solid
- color
- Brown
- CAS DataBase Reference
- 1009-36-5(CAS DataBase Reference)
- EPA Substance Registry System
- 2-Chloro-5-nitroanisole (1009-36-5)
Safety
- Hazard Codes
- Xi,N,Xn
- Risk Statements
- 36/37/38-51-22-36/38
- Safety Statements
- 26-36/37/39-28
- Hazard Note
- Irritant
- HS Code
- 29093090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
N-Bromosuccinimide Price
- Product number
- C1773
- Product name
- 2-Chloro-5-nitroanisole
- Purity
- min. 98.0 %
- Packaging
- 5G
- Price
- $31
- Updated
- 2025/07/31
- Product number
- C1773
- Product name
- 2-Chloro-5-nitroanisole
- Purity
- min. 98.0 %
- Packaging
- 25G
- Price
- $93
- Updated
- 2025/07/31
- Product number
- C373775
- Product name
- 2-Chloro-5-nitroanisole
- Packaging
- 50g
- Price
- $1285
- Updated
- 2021/12/16
- Product number
- C373775
- Product name
- 2-Chloro-5-nitroanisole
- Packaging
- 1g
- Price
- $50
- Updated
- 2021/12/16
- Product number
- 4654-5-Y9
- Product name
- 2-Chloro-5-nitroanisole
- Packaging
- 25g
- Price
- $64
- Updated
- 2021/12/16
2-CHLORO-5-NITROANISOLE Chemical Properties,Usage,Production
Chemical Properties
White Solid
Uses
2-Chloro-5-nitroanisole (cas# 1009-36-5) is a compound useful in organic synthesis.
Synthesis
97-52-9
1009-36-5
General procedure for the synthesis of 2-chloro-5-nitroanisole from 2-methoxy-4-nitroaniline: In an agate mortar, camphorsulfonic acid (1.5 mmol), tert-butyl nitrite (3.0 mmol), benzyltriethylammonium chloride (2.5 mmol), and a catalytic amount of copper(II) chloride (1 mol%) were mixed with 2-methoxy-4-nitroaniline (1.25 mmol) were mixed. The mixture was vigorously ground for 15-20 min until nitrogen release stopped completely. Upon completion of the reaction (confirmed by thin layer chromatography), the crude product was treated according to the treatment of aryl bromide reaction and purified by column chromatography using hexane/dichloromethane as eluting solvent. The physical properties and 1H NMR data of the resulting product were consistent with those of commercially available analytically pure samples.
References
[1] Tetrahedron, 2013, vol. 69, # 16, p. 3511 - 3517
[2] Environmental Toxicology and Chemistry, 2001, vol. 20, # 7, p. 1381 - 1389
[3] Tetrahedron Letters, 2010, vol. 51, # 51, p. 6769 - 6771
[4] Tetrahedron, 2010, vol. 66, # 37, p. 7418 - 7422
[5] Chemische Berichte, 1899, vol. 32, p. 2623
2-CHLORO-5-NITROANISOLE Preparation Products And Raw materials
Raw materials
Preparation Products
2-CHLORO-5-NITROANISOLE Suppliers
- Tel
- 18210857532; 18210857532
- Fax
- 86-10-82849933
- jkinfo@jkchemical.com
- Country
- China
- ProdList
- 96815
- Advantage
- 76
- Tel
- 821-50328103-801 18930552037
- Fax
- 86-21-50328109
- 3bsc@sina.com
- Country
- China
- ProdList
- 15838
- Advantage
- 69
- Tel
- 021-67121386
- Fax
- 021-67121385
- Sales-CN@TCIchemicals.com
- Country
- China
- ProdList
- 24529
- Advantage
- 81
- Tel
- 021-021-58432009 400-005-6266
- Fax
- 021-58436166
- sales8178@energy-chemical.com
- Country
- China
- ProdList
- 44801
- Advantage
- 61
- Tel
- 86-027-67849912
- Fax
- 86-027-87531808
- sales@chemwish.com
- Country
- China
- ProdList
- 35896
- Advantage
- 56
- Tel
- +86 (0) 571 85 58 67 18
- Fax
- 0086-571-85864795
- Country
- China
- ProdList
- 18207
- Advantage
- 66
- Tel
- 13817811078
- Fax
- 86-021-50426522,50426273
- sales@jingyan-chemical.com
- Country
- China
- ProdList
- 9976
- Advantage
- 60
- Tel
- +86-21-54098501
- Fax
- +86-21-54096319
- sales@sinch.com.cn
- Country
- China
- ProdList
- 11598
- Advantage
- 64
- Tel
- 021-54306202 13764082696
- info@hanhongsci.com
- Country
- China
- ProdList
- 42934
- Advantage
- 64
- Tel
- 010-59484199 18611897322
- sales@eternalchem.com
- Country
- China
- ProdList
- 4383
- Advantage
- 60
View Lastest Price from 2-CHLORO-5-NITROANISOLE manufacturers
- Product
- 2-CHLORO-5-NITROANISOLE 1009-36-5
- Price
- US $100.00-1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2023-12-25
- Product
- 2-Chloro-5-nitroanisole 1009-36-5
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 99.0%+
- Supply Ability
- 100 tons
- Release date
- 2020-01-07
- Product
- 2-CHLORO-5-NITROANISOLE 1009-36-5
- Price
- US $2.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 100kg
- Release date
- 2018-12-24