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2-CHLORO-5-NITROANISOLE

Product Name
2-CHLORO-5-NITROANISOLE
CAS No.
1009-36-5
Chemical Name
2-CHLORO-5-NITROANISOLE
Synonyms
2-METHOXY-4-NIT;2-Chloro-5-nitropheno;2-CHLORO-5-NITROANISOLE;2-Chloro-5-nitroanisole >2-chloro-5-nitrobenzyl ether;2-METHOXY-4-NITROCHLOROBENZENE;4-Chloro-3-methoxynitrobenzene;1-chloro-2-methoxy-4-nitro-benzen;1-Chloro-2-methoxy-4-nitrobenzene;2-Chloro-5-nitrophenyl methyl ether
CBNumber
CB5469406
Molecular Formula
C7H6ClNO3
Formula Weight
187.58
MOL File
1009-36-5.mol
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2-CHLORO-5-NITROANISOLE Property

Melting point:
81-83°C
Boiling point:
287.3±20.0 °C(Predicted)
Density 
1.366±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
solubility 
Chloroform, Ethyl Acetate
form 
Solid
color 
Brown
CAS DataBase Reference
1009-36-5(CAS DataBase Reference)
EPA Substance Registry System
2-Chloro-5-nitroanisole (1009-36-5)
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Safety

Hazard Codes 
Xi,N,Xn
Risk Statements 
36/37/38-51-22-36/38
Safety Statements 
26-36/37/39-28
Hazard Note 
Irritant
HS Code 
29093090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TCI Chemical
Product number
C1773
Product name
2-Chloro-5-nitroanisole
Purity
min. 98.0 %
Packaging
5G
Price
$31
Updated
2025/07/31
TCI Chemical
Product number
C1773
Product name
2-Chloro-5-nitroanisole
Purity
min. 98.0 %
Packaging
25G
Price
$93
Updated
2025/07/31
TRC
Product number
C373775
Product name
2-Chloro-5-nitroanisole
Packaging
50g
Price
$1285
Updated
2021/12/16
TRC
Product number
C373775
Product name
2-Chloro-5-nitroanisole
Packaging
1g
Price
$50
Updated
2021/12/16
SynQuest Laboratories
Product number
4654-5-Y9
Product name
2-Chloro-5-nitroanisole
Packaging
25g
Price
$64
Updated
2021/12/16
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2-CHLORO-5-NITROANISOLE Chemical Properties,Usage,Production

Chemical Properties

White Solid

Uses

2-Chloro-5-nitroanisole (cas# 1009-36-5) is a compound useful in organic synthesis.

Synthesis

97-52-9

1009-36-5

General procedure for the synthesis of 2-chloro-5-nitroanisole from 2-methoxy-4-nitroaniline: In an agate mortar, camphorsulfonic acid (1.5 mmol), tert-butyl nitrite (3.0 mmol), benzyltriethylammonium chloride (2.5 mmol), and a catalytic amount of copper(II) chloride (1 mol%) were mixed with 2-methoxy-4-nitroaniline (1.25 mmol) were mixed. The mixture was vigorously ground for 15-20 min until nitrogen release stopped completely. Upon completion of the reaction (confirmed by thin layer chromatography), the crude product was treated according to the treatment of aryl bromide reaction and purified by column chromatography using hexane/dichloromethane as eluting solvent. The physical properties and 1H NMR data of the resulting product were consistent with those of commercially available analytically pure samples.

References

[1] Tetrahedron, 2013, vol. 69, # 16, p. 3511 - 3517
[2] Environmental Toxicology and Chemistry, 2001, vol. 20, # 7, p. 1381 - 1389
[3] Tetrahedron Letters, 2010, vol. 51, # 51, p. 6769 - 6771
[4] Tetrahedron, 2010, vol. 66, # 37, p. 7418 - 7422
[5] Chemische Berichte, 1899, vol. 32, p. 2623

2-CHLORO-5-NITROANISOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-CHLORO-5-NITROANISOLE Suppliers

SIGMA-RBI
Tel
--
Fax
--
Country
Switzerland
ProdList
6896
Advantage
91
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View Lastest Price from 2-CHLORO-5-NITROANISOLE manufacturers

Henan Fengda Chemical Co., Ltd
Product
2-CHLORO-5-NITROANISOLE 1009-36-5
Price
US $100.00-1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
g-kg-tons, free sample is available
Release date
2023-12-25
Shaanxi Dideu Medichem Co. Ltd
Product
2-Chloro-5-nitroanisole 1009-36-5
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
99.0%+
Supply Ability
100 tons
Release date
2020-01-07
Career Henan Chemical Co
Product
2-CHLORO-5-NITROANISOLE 1009-36-5
Price
US $2.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
100kg
Release date
2018-12-24

1009-36-5, 2-CHLORO-5-NITROANISOLERelated Search:


  • 1-Chloro-2-methoxy-4-nitrobenzene
  • 4-Chloro-3-methoxynitrobenzene, 1-Chloro-2-methoxy-4-nitrobenzene, 2-Chloro-5-nitrophenyl methyl ether
  • 2-METHOXY-4-NITROCHLOROBENZENE
  • 2-CHLORO-5-NITROANISOLE
  • 1-Chloro-2-Methoxy-4-nitrobenzene, 98.0%(GC)
  • 4-Chloro-3-methoxynitrobenzene
  • 2-METHOXY-4-NIT
  • 1-chloro-2-methoxy-4-nitro-benzen
  • 2-Chloro-5-nitroanisole &gt
  • Benzene, 1-chloro-2-methoxy-4-nitro-
  • 2-CHLORO-5-NITROANISOLE ISO 9001:2015 REACH
  • 2-Chloro-5-nitropheno
  • 2-Chloro-5-nitrophenyl methyl ether
  • 2-chloro-5-nitrobenzyl ether
  • 1009-36-5
  • C7H6ClNO3
  • Building Blocks
  • Chemical Synthesis
  • Aromatics
  • Miscellaneous Reagents
  • New Products for Chemical Synthesis
  • Nitrogen Compounds
  • Organic Building Blocks
  • Anisoles, Alkyloxy Compounds & Phenylacetates
  • Chlorine Compounds
  • Nitro Compounds
  • Anisole