ChemicalBook > CAS DataBase List > (3-AMINO-PYRIDIN-4-YL)-METHANOL

(3-AMINO-PYRIDIN-4-YL)-METHANOL

Product Name: (3-AMINO-PYRIDIN-4-YL)-METHANOL
CAS No.: 152398-05-5
Chemical Name: (3-AMINO-PYRIDIN-4-YL)-METHANOL
Synonyms: 3-Aminopyridine-4-methanol;(3-Amino-4-pyridyl)methanol;4-Pyridinemethanol, 3-amino-;(3-amino-4-pyridinyl)methanol;3-AMINO-4-HYDROXYMETHYLPYRIDINE;(3-AMINO-PYRIDIN-4-YL)-METHANOL;4-Pyridinemethanol,3-amino-(9CI);(3-Amino-pyridin-4-yl)-methanol ,96%;3-Amino-4-hydroxymethylpyridine ,96%;(3-Amino-pyridin-4-yl)-methanol AldrichCPR
CBNumber: CB5695319
Molecular Formula: C6H8N2O
Formula Weight: 124.14
MOL File: 152398-05-5.mol

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(3-AMINO-PYRIDIN-4-YL)-METHANOL Property

Melting point:: 118.7-118.9°C
Boiling point:: 366.6±27.0 °C(Predicted)
Density: 1.257±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
form: solid
pka: 13.31±0.10(Predicted)
Appearance: White to yellow Solid

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Safety

Hazard Codes: Xi,Xn
Risk Statements: 22-36/37/38
Safety Statements: 26-36
WGK Germany: 3
HazardClass: IRRITANT
HS Code: 29333990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: ADE000287
Product name: (3-Amino-pyridin-4-yl)-methanol
Purity: AldrichCPR
Packaging: 1g
Price: $179
Updated: 2025/07/31

TRC

Product number: A616715
Product name: (3-Amino-pyridin-4-yl)-methanol
Packaging: 250mg
Price: $215
Updated: 2021/12/16

Apolloscientific

Product number: OR303706
Product name: (3-Amino-4-pyridinyl)methanol
Packaging: 1g
Price: $247
Updated: 2021/12/16

Frontier Specialty Chemicals

Product number: JK206828
Product name: (3-Amino-pyridin-4-yl)methanol
Purity: 96%
Packaging: 1g
Price: $258
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA50916
Product name: (3-Aminopyridin-4-yl)methanol
Packaging: 1g
Price: $311.4
Updated: 2021/12/16

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(3-AMINO-PYRIDIN-4-YL)-METHANOL Chemical Properties,Usage,Production

Chemical Properties

White solid

Synthesis

7579-20-6

152398-05-5

Step 2: Three aliquots were carefully added to an anhydrous THF (200 mL) slurry of solid compound 3-aminoisonicotinic acid (9.5 g, 69 mmol) to LiAlH4 (9.5 g, 250 mmol). The resulting reaction mixture was stirred at room temperature for 2 days. Upon completion of the reaction, it was cooled in an ice bath and water (10 mL), 15% NaOH aqueous solution (10 mL) and water (30 mL) were added sequentially dropwise to quench the reaction. The reaction mixture was filtered through a diatomaceous earth pad and washed several times with THF. After evaporation of the solvent, the resulting oil solidified on standing. The reaction mixture was purified using silica gel fast chromatography with 5% CH3OH (containing NH3)/EtOAc as eluent to afford the target product 3-amino-4-hydroxymethylpyridine 6.21 g (72% yield).LC-MS: m/z = 125 ([M+H]+).

References

[1] Patent: WO2004/831, 2003, A1. Location in patent: Page 22
[2] Patent: WO2008/108957, 2008, A2. Location in patent: Page/Page column 95
[3] Australian Journal of Chemistry, 1993, vol. 46, # 7, p. 987 - 993
[4] Patent: WO2011/38572, 2011, A1. Location in patent: Page/Page column 71; 72

(3-AMINO-PYRIDIN-4-YL)-METHANOL Preparation Products And Raw materials

Raw materials

Acetic anhydride tert-Butyl methyl ether Acetamide Chloroform Tetrahydrofuran 3,4-Pyridinedicarboxylic acid Lithium Aluminum Hydride Bromine Acetic acid Methanol Sodium hydroxide Magnesium sulfate Sodium carbonate

Preparation Products

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View Lastest Price from (3-AMINO-PYRIDIN-4-YL)-METHANOL manufacturers

Zibo Hangyu Biotechnology Development Co., Ltd

Product: (3-AMINO-PYRIDIN-4-YL)-METHANOL 152398-05-5
Price: US $60.00-600.00/KG
Min. Order: 1KG
Purity: 0.99
Supply Ability: 20 tons
Release date: 2023-10-12

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