2-Chloro-6-phenylnicotinonitrile

Product Name: 2-Chloro-6-phenylnicotinonitrile
CAS No.: 43083-14-3
Chemical Name: 2-Chloro-6-phenylnicotinonitrile
Synonyms: 2-Chloro-6-phenylnicotinonitrile;2-chloro-6-phenylpyridine-3-carbonitrile;2-Chloro-6-phenyl-3-pyridinecarbonitrile;3-Pyridinecarbonitrile, 2-chloro-6-phenyl-;2-Chloro-6-phenylnicotinonitrile ISO 9001：2015 REACH;JR-13560, 2-Chloro-6-phenylpyridine-3-carbonitrile, 97%;2-Chloro-6-phenylpyridine-3-carbonitrile, 2-Chloro-3-cyano-6-phenylpyridine
CBNumber: CB5703690
Molecular Formula: C12H7ClN2
Formula Weight: 214.65
MOL File: 43083-14-3.mol

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2-Chloro-6-phenylnicotinonitrile Property

Melting point:: 155-159°C
Boiling point:: 376.4±42.0 °C(Predicted)
Density: 1.30±0.1 g/cm3(Predicted)
storage temp.: Store at room temperature
pka: -3.62±0.10(Predicted)
Appearance: Light yellow to yellow Solid
CAS DataBase Reference: 43083-14-3(CAS DataBase Reference)

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Safety

Hazard Codes: T
HazardClass: IRRITANT
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: C380453
Product name: 2-Chloro-6-phenylnicotinonitrile
Packaging: 250mg
Price: $55
Updated: 2021/12/16

Matrix Scientific

Product number: 042600
Product name: 2-Chloro-6-phenylnicotinonitrile
Purity: >95%
Packaging: 1g
Price: $31
Updated: 2021/12/16

Apolloscientific

Product number: OR01798
Product name: 2-Chloro-6-phenylnicotinonitrile
Packaging: 1g
Price: $31
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H37-5-T5
Product name: 2-Chloro-6-phenylnicotinonitrile
Packaging: 1g
Price: $34
Updated: 2021/12/16

AK Scientific

Product number: V0652
Product name: 2-Chloro-6-phenylnicotinonitrile
Packaging: 1g
Price: $39
Updated: 2021/12/16

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2-Chloro-6-phenylnicotinonitrile Chemical Properties,Usage,Production

Synthesis

24388-23-6

40381-90-6

43083-14-3

General procedure for the synthesis of 2-chloro-6-phenylnicotinonitrile from (4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzene and 2,6-dichloronicotinonitrile: 2,6-dichloronicotinonitrile (0.865 g) and 4,4,5,5-tetramethyl-2-phenyl-1,3,2-dioxaborolane (1.021 g) were dissolved in a mixture of glycol dimethyl ether (60 mL) and water (20 mL) in a solvent mixture. Sodium bicarbonate (1 M) and [1,1'-bis(diphenylphosphino)ferrocene]palladium dichloride (0.366 g) were added, and the reaction mixture was heated to 90 °C under argon protection for 6 hours. After completion of the reaction, the aqueous phase was separated and extracted with ethyl acetate. The organic phases were combined, washed with saturated aqueous sodium chloride solution, dried over anhydrous sodium sulfate and filtered. The residue was purified by column chromatography (eluent: petroleum ether/ethyl acetate, 99:1 to 95:5, v/v) to afford 2-chloro-6-phenylnicotinonitrile (0.680 g, 63.4% yield) as a white solid.

References

[1] Patent: CN106146493, 2016, A. Location in patent: Paragraph 0164; 0165; 0166; 0167

2-Chloro-6-phenylnicotinonitrile Preparation Products And Raw materials

Raw materials

Preparation Products

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2-Chloro-6-phenylnicotinonitrile Suppliers

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View Lastest Price from 2-Chloro-6-phenylnicotinonitrile manufacturers

Dideu Industries Group Limited

Product: 2-Chloro-6-phenylnicotinonitrile 43083-14-3
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons Min
Release date: 2021-10-28

Career Henan Chemical Co

Product: 2-Chloro-6-phenylnicotinonitrile 43083-14-3
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 1ton
Release date: 2019-07-11

43083-14-3, 2-Chloro-6-phenylnicotinonitrileRelated Search:

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2-Chloro-6-phenylnicotinonitrile

2-chloro-6-phenylpyridine-3-carbonitrile

2-Chloro-6-phenylpyridine-3-carbonitrile, 2-Chloro-3-cyano-6-phenylpyridine

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2-Chloro-6-phenylnicotinonitrile ISO 9001：2015 REACH

2-Chloro-6-phenyl-3-pyridinecarbonitrile

43083-14-3

C12H7ClN2

Pyridines