2'-Hydroxypropiophenone

ChemicalBook > CAS DataBase List > 2'-Hydroxypropiophenone

2'-Hydroxypropiophenone

Product Name: 2'-Hydroxypropiophenone
CAS No.: 610-99-1
Chemical Name: 2'-Hydroxypropiophenone
Synonyms: 2-Propionylphenol;o-Propiophenol;2'-hydroxy acetone;o-Hydroxylpropioph;2'-Hydroxypropiophen;2-HYDROXYNITROBENZENE;O-HYDROXYPROPIOPHENONE;2-HYDROXYPROPIOPHENONE;2'-HYDROXYPROPIOPHENONE;o-Hydroxylpropiophenone
CBNumber: CB5717338
Molecular Formula: C9H10O2
Formula Weight: 150.17
MOL File: 610-99-1.mol

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2'-Hydroxypropiophenone Property

Melting point:: 20-22 °C
Boiling point:: 115 °C15 mm Hg(lit.)
Density: 1.094 g/mL at 25 °C(lit.)
refractive index: n20/D 1.548(lit.)
Flash point:: >230 °F
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
solubility: Chloroform (Slightly), Methanol (Slightly)
form: Oil
pka: 8.33±0.35(Predicted)
color: Colourless
BRN: 1860264
LogP: 2.540
CAS DataBase Reference: 610-99-1(CAS DataBase Reference)
NIST Chemistry Reference: ortho-Hydroxypropiophenone(610-99-1)

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-36
WGK Germany: 3
HS Code: 29145090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: H55103
Product name: 2′-Hydroxypropiophenone
Purity: 97%
Packaging: 25g
Price: $62.4
Updated: 2024/03/01

TCI Chemical

Product number: H0298
Product name: 2'-Hydroxypropiophenone
Purity: >97.0%(GC)
Packaging: 25g
Price: $39
Updated: 2024/03/01

TRC

Product number: H996363
Product name: 2''-Hydroxypropiophenone
Packaging: 1g
Price: $45
Updated: 2021/12/16

Frontier Specialty Chemicals

Product number: JK336074
Product name: 2'-Hydroxypropiophenone
Purity: 97%
Packaging: 25g
Price: $41
Updated: 2021/12/16

Matrix Scientific

Product number: 139835
Product name: 2'-Hydroxypropiophenone
Purity: 95%+
Packaging: 1g
Price: $101
Updated: 2021/12/16

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2'-Hydroxypropiophenone Chemical Properties,Usage,Production

Chemical Properties

CLEAR BROWNISH LIQUID

Preparation

Obtained by Fries rearrangement of phenyl propionate
with aluminium chloride in refluxing carbon disulfide ?, then at 130–150° for 2–3 h after solvent elimination (32–35%)
with aluminium chloride in chlorobenzene using microwave irradiation for 3 ? min at 106° (28%)
with aluminium chloride in nitrobenzene at 50° for 18 h (16%) or at ? 20° for 48 h (10%)
with aluminium chloride in nitromethane at 20° for 7 days (20%)
with aluminium chloride in heptane at 80–90° for 7 h (53%) or in tetrachlo-? roethane at 95° for 5 h (43%)
with aluminium chloride without solvent at 250° for 5 min or at 180–200° for ? 15 min (76–78%), at 140–160° (32–35%), at 140°
with zirconium chloride in o-dichlorobenzene at 120° for 3 h (83%)
with titanium tetrachloride in o-dichlorobenzene at 150° for 1 h (62%) ?, in nitromethane at 20° for 7 days (13%) or without solvent at 50° for 10 h (30%)
with titanium tetrabromide in o-dichlorobenzene at 150° for 1 h (60%)
with stannic chloride at 50° for 3 h (25%)
with boron trifluoride at 120–135° for 15 min (15%)
with zinc chloride at 180–200° for 15 min (10%)
with polyphosphoric acid at 100° (13%)
Also obtained by Friedel–Crafts acylation of phenol with propionyl chloride in the presence of aluminium chloride (40%), at 120–130° for 1 h (45%) according to the method
Also obtained by acylation of phenol with propionic acid
in the presence of boron trifluoride at 165° for 1 h (45%) or at 80° for ? 2 h (8%)
in the presence of polyphosphoric acid at 100° for 10 min (by-product)
in the presence of zinc chloride at 160° for 1 h
Also obtained by isomerization of 4-hydroxypropiophenone with aluminium chloride (1.5 equiv) at 165° for 1 h (40%) or at 180–200° for 15 min (55%)
Also obtained by demethylation of 2-propionylanisole with fuming hydrochloric acid (d = 1.19) in a sealed tube at 110° for 6 h
Also obtained (by-product) by heating 3-tert-butyl-4-hydroxypropiophenone with aluminium chloride at 170° for 15 min (13%)
Also obtained by treatment of 2,3-dimethylchromone with sodium ethoxide in boiling ethanol for 30 h according to the method
Also obtained from 2-allylphenol by treatment with perbenzoic acid in ethyl ether, first at 0°, then between 0° and 25° for 24 h (78%)
Also obtained by reaction of 2-bromophenyl propionate in a ethyl ether/hexane/THF mixture at low temperature (?78 to ?95°) with sec-butyllithium to give, after hydrolysis, the titled ketone (metal-promoted Fries rearrangement) (17%)
Also obtained by reaction of ethylmagnesium bromide
with 2-hydroxybenzamide in boiling benzene, followed by hydrolysis ? (30%)
with 2-hydroxy-N,N-diethylbenzamide in boiling benzene, followed by ? hydrolysis (82–84%)
Also isolated by heating of 1-(o-hydroxyphenyl)cyclopropyltrimethylam-monium iodide for 1 h at 140° with 1.5 equiv of N,N-diisopropylethylamine (not water-free) (38%)
Also obtained by hydrolysis of 2-(1-methyliminopropyl)phenol (4aa) with aqueous acetic acid/THF at 40° for 4 h (86%)
Also obtained by photolysis of phenyl propionate in water or in solution containing b-cyclodextrine (254 nm) at 25° for 2 h
Also obtained by treatment of 2-(1-hydroxypropyl)phenol with MnO2 in methylene chloride for 7 h at r.t.

Definition

ChEBI: 2'-hydroxypropiophenone is an aromatic ketone.

2'-Hydroxypropiophenone Preparation Products And Raw materials

Raw materials

Preparation Products

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2'-Hydroxypropiophenone Suppliers

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View Lastest Price from 2'-Hydroxypropiophenone manufacturers

Hebei Weibang Biotechnology Co., Ltd

Product: 2'-Hydroxypropiophenone 610-99-1
Price: US $10.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 10 mt
Release date: 2022-10-10

Hebei Mojin Biotechnology Co., Ltd

Product: 2'-Hydroxypropiophenone 610-99-1
Price: US $0.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 50000KG/month
Release date: 2023-09-08

Wuhan Monad Medicine Tech Co.,LTD

Product: 2'-Hydroxypropiophenone 610-99-1
Price: US $10.00/KG
Min. Order: 1KG
Purity: 99.99%
Supply Ability: 20 tons/month
Release date: 2020-12-25

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610-99-1

HOC6H4COCH2CH3

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Building Blocks

Carbonyl Compounds

Organic Building Blocks

Building Blocks

Carbonyl Compounds

Chemical Synthesis

Ketones

Organic Building Blocks

Aromatic Propiophenones (substituted)

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