3-(2-nitrophenyl)propionic acid
- Product Name
- 3-(2-nitrophenyl)propionic acid
- CAS No.
- 2001-32-3
- Chemical Name
- 3-(2-nitrophenyl)propionic acid
- Synonyms
- 3-(2-Nitrophenyl);2-Nitrobenzenepropanoic acid;3-(2-Nitrophenyl)propionsure;3-(2-nitrophenyl)propionic acid;3-(2-Nitrophenyl)propanoic acid;Benzenepropanoic acid, 2-?nitro-;2-(2-Carboxyethyl)-1-nitrobenzene
- CBNumber
- CB5930409
- Molecular Formula
- C9H9NO4
- Formula Weight
- 195.17
- MOL File
- 2001-32-3.mol
3-(2-nitrophenyl)propionic acid Property
- Melting point:
- 115 °C
- Boiling point:
- 331.83°C (rough estimate)
- Density
- 1.3544 (rough estimate)
- refractive index
- 1.5700 (estimate)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 4.5(at 25℃)
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P330Rinse mouth.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- N498113
- Product name
- 3-(2-nitrophenyl)propanoicAcid
- Packaging
- 250mg
- Price
- $330
- Updated
- 2021/12/16
- Product number
- CS-0059193
- Product name
- 3-(2-Nitrophenyl)propanoicacid
- Purity
- >97.0%
- Packaging
- 250mg
- Price
- $54
- Updated
- 2021/12/16
- Product number
- 0290AB
- Product name
- 3-(2-Nitrophenyl)propanoicacid
- Packaging
- 250mg
- Price
- $128
- Updated
- 2021/12/16
- Product number
- 0290AB
- Product name
- 3-(2-Nitrophenyl)propanoicacid
- Packaging
- 1g
- Price
- $238
- Updated
- 2021/12/16
- Product number
- 165314
- Product name
- 3-(2-Nitrophenyl)propanoic acid
- Packaging
- 500mg
- Price
- $265
- Updated
- 2021/12/16
3-(2-nitrophenyl)propionic acid Chemical Properties,Usage,Production
Synthesis
59803-35-9
2001-32-3
In a single-necked round-bottomed flask (2L), diethyl 2-(2-nitrobenzyl)malonate (8.7 g, 0.029 mol), 6N hydrochloric acid (131 mL) and acetic acid (131 mL) were added. The reaction mixture was heated and refluxed for 48 h, during which the reaction progress was monitored by thin layer chromatography (TLC). Upon completion of the reaction, the reaction mixture was alkalized with 6 M sodium hydroxide solution (500 mL) and subsequently extracted with ethyl acetate (3 x 250 mL). The organic phases were combined, dried with anhydrous magnesium sulfate and concentrated under reduced pressure to remove the solvent. The crude product was purified by column chromatography (silica gel: 100-200 mesh, eluent: 40% hexane solution of ethyl acetate) to give 3-(2-nitrophenyl)propionic acid (5.4 g, 94% yield).
References
[1] Patent: WO2010/127855, 2010, A1. Location in patent: Page/Page column 145; 146
[2] Chemische Berichte, 1923, vol. 56, p. 2450
[3] Patent: WO2005/40119, 2005, A1. Location in patent: Page/Page column 48-49
[4] Patent: WO2005/40100, 2005, A1. Location in patent: Page/Page column 75-77
3-(2-nitrophenyl)propionic acid Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-(2-nitrophenyl)propionic acid manufacturers
- Product
- 3-(2-nitrophenyl)propionic acid 2001-32-3
- Price
- US $6.68/KG
- Min. Order
- 1KG
- Purity
- 97%-99%
- Supply Ability
- 1kg-1000kg
- Release date
- 2020-01-08