2-AMINO-5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOLE

Product Name: 2-AMINO-5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOLE
CAS No.: 28004-63-9
Chemical Name: 2-AMINO-5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOLE
Synonyms: AKOS B014677;TIMTEC-BB SBB007063;ART-CHEM-BB B014677;IFLAB-BB F1386-0069;CHEMBRDG-BB 5313490;5-(2,4-Dichlorophenyl);5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOL-2-AMINE;2-AMINO-5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOLE;1,3,4-Thiadiazol-2-aMine, 5-(2,4-dichlorophenyl)-;5-(2,4-DICHLOROPHENYL)-[1,3,4]THIADIAZOL-2-YL-AMINE
CBNumber: CB6101543
Molecular Formula: C8H5Cl2N3S
Formula Weight: 246.12
MOL File: 28004-63-9.mol

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2-AMINO-5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOLE Property

Melting point:: 240-242℃ (ethanol water )
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C

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Safety

Hazard Codes: Xi
HazardClass: IRRITANT

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: D435313
Product name: 5-(2,4-Dichlorophenyl)-1,3,4-thiadiazol-2-amine
Packaging: 500mg
Price: $130
Updated: 2021/12/16

Matrix Scientific

Product number: 007785
Product name: 5-(2,4-Dichlorophenyl)-[1,3,4]thiadiazol-2-yl-amine
Packaging: 500mg
Price: $168
Updated: 2021/12/16

AK Scientific

Product number: 2698AB
Product name: 5-(2,4-Dichlorophenyl)-1,3,4-thiadiazol-2-amine
Packaging: 1g
Price: $172
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD113695
Product name: 5-(2,4-Dichlorophenyl)-1,3,4-thiadiazol-2-amine
Packaging: 2g
Price: $218
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD113695
Product name: 5-(2,4-Dichlorophenyl)-1,3,4-thiadiazol-2-amine
Packaging: 500mg
Price: $75
Updated: 2021/12/16

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2-AMINO-5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOLE Chemical Properties,Usage,Production

Synthesis

6957-92-2

28004-63-9

General method: In step 2, the Schiff base intermediate was dissolved in 1,4-dioxane, iodine and potassium carbonate were added, and the cyclization reaction was carried out at 80 °C. The reaction mixture was refluxed for 4 hours and the progress of the reaction was monitored by thin layer chromatography (TLC). After completion of the reaction, the mixture was cooled to room temperature and the reaction was quenched by the addition of 5% sodium thiosulfate solution (20 ml). The target organic compounds in the reaction mixture were extracted with ethyl acetate. The organic phase was separated and collected and the solvent was removed by evaporation to give a solid product of 2-amino-5-(2,4-dichlorophenyl)-1,3,4-thiadiazole.

References

[1] Monatshefte fur Chemie, 2013, vol. 144, # 5, p. 681 - 686
[2] Bioorganic Chemistry, 2018, vol. 78, p. 201 - 209
[3] Archiv der Pharmazie, 2015, vol. 348, # 1, p. 10 - 22
[4] Turkish Journal of Chemistry, 2018, vol. 42, # 3, p. 839 - 858
[5] Indian Journal of Chemistry, 1970, vol. 8, p. 509 - 513

2-AMINO-5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-AMINO-5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOLE Suppliers

Canada 1 China 26 France 1 Germany 1 India 1 Russia 4 Switzerland 1 The Netherlands 1 Ukraine 1 United Kingdom 3 United States 11 Global 51

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28004-63-9, 2-AMINO-5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOLERelated Search:

2-AMINO-5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOLE 2-AMINO-5-(2-CHLOROPHENYL)-1,3,4-THIADIAZOLE 2-AMINO-5-PHENYL-1 3 4-THIADIAZOLE 96 2-AMINO-5-(4-CHLOROPHENYL)-1 3 4- 5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOL-2-YLAMINE HYDROCHLORIDE

AKOS B014677

5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOL-2-AMINE

5-(2,4-DICHLOROPHENYL)-[1,3,4]THIADIAZOL-2-YL-AMINE

TIMTEC-BB SBB007063

5-(2,4-dichlorophenyl)-1,3,4-thiadiazol-2-amine(SALTDATA: FREE)

1,3,4-Thiadiazol-2-aMine, 5-(2,4-dichlorophenyl)-

5-(2,4-Dichlorophenyl)

CHEMBRDG-BB 5313490

IFLAB-BB F1386-0069

ART-CHEM-BB B014677

2-AMINO-5-(2,4-DICHLOROPHENYL)-1,3,4-THIADIAZOLE

28004-63-9