2-Bromo-3-methoxy-6-nitropyridine

Product Name: 2-Bromo-3-methoxy-6-nitropyridine
CAS No.: 76066-07-4
Chemical Name: 2-Bromo-3-methoxy-6-nitropyridine
Synonyms: 2-Bromo-3-methoxy-6-nitropyridine;6-Bromo-5-methoxy-2-nitropyridine;Pyridine, 2-bromo-3-methoxy-6-nitro-;2-Bromo-3-methoxy-6-nitropyridine ISO 9001：2015 REACH
CBNumber: CB61175628
Molecular Formula: C6H5BrN2O3
Formula Weight: 233.02
MOL File: 76066-07-4.mol

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2-Bromo-3-methoxy-6-nitropyridine Property

Melting point:: 140-1420C
Boiling point:: 364.4±37.0 °C(Predicted)
Density: 1.730±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
solubility: DMSO (Slightly), Methanol (Slightly)
form: Solid
pka: -10.90±0.10(Predicted)
color: White to Off-White

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

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N-Bromosuccinimide Price

TRC

Product number: B684790
Product name: 2-Bromo-3-methoxy-6-nitropyridine
Packaging: 100mg
Price: $225
Updated: 2021/12/16

Usbiological

Product number: B2860-46
Product name: 2-Bromo-3-methoxy-6-nitropyridine
Packaging: 50mg
Price: $425
Updated: 2021/12/16

Matrix Scientific

Product number: 129768
Product name: 2-Bromo-3-methoxy-6-nitro-pyridine
Purity: 95%+
Packaging: 1g
Price: $450
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB19123
Product name: 2-Bromo-3-methoxy-6-nitropyridine
Packaging: 2g
Price: $450
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB19123
Product name: 2-Bromo-3-methoxy-6-nitropyridine
Packaging: 5G
Price: $650
Updated: 2021/12/16

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2-Bromo-3-methoxy-6-nitropyridine Chemical Properties,Usage,Production

Chemical Properties

Off-White Solid

Synthesis

24100-18-3

76066-07-4

General procedure for the synthesis of 2-bromo-3-methoxy-6-nitropyridine from 2-bromo-3-methoxypyridine: 2-bromo-3-methoxypyridine (4.45 g, 23.7 mmol) was slowly added to a mixture of fuming nitric acid and concentrated sulfuric acid (1:1, v/v, total of 18 mL) that had been pre-cooled to 0 °C. The reaction mixture was kept stirred at 55 °C for 1.5 hours. Upon completion of the reaction, the mixture was carefully poured into ice water (150 mL) and a precipitate was immediately generated. The resulting precipitate was the target product 2-bromo-3-methoxy-6-nitropyridine, which could be used in the subsequent reaction without further purification. Yield: 3.54 g (64%) as a light yellow solid.1H NMR (DMSO-d6, 400 MHz) δ 8.41 (d, 1H), 7.80 (d, 1H), 4.06 (s, 3H).

References

[1] Journal of Medicinal Chemistry, 2009, vol. 52, # 3, p. 637 - 645
[2] Tetrahedron, 1986, vol. 42, # 5, p. 1475 - 1485
[3] Pharmazie, 2000, vol. 55, # 12, p. 907 - 912
[4] Journal of Medicinal Chemistry, 1981, vol. 24, # 1, p. 39 - 42
[5] Patent: WO2007/51981, 2007, A1. Location in patent: Page/Page column 56

2-Bromo-3-methoxy-6-nitropyridine Preparation Products And Raw materials

Raw materials

Preparation Products

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2-Bromo-3-methoxy-6-nitropyridine Suppliers

Canada 2 China 74 Germany 1 India 2 United Kingdom 1 United States 12 Global 92

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View Lastest Price from 2-Bromo-3-methoxy-6-nitropyridine manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 2-Bromo-3-methoxy-6-nitropyridine 76066-07-4
Price: US $1.00-1.00/Kg/Drum
Min. Order: 1g
Purity: 98%
Supply Ability: 50tons
Release date: 2020-05-12

Dideu Industries Group Limited

Product: 2-Bromo-3-methoxy-6-nitropyridine 76066-07-4
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons min
Release date: 2021-09-08

Career Henan Chemical Co

Product: 2-Bromo-3-methoxy-6-nitropyridine 76066-07-4
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 200kg
Release date: 2019-12-31

76066-07-4, 2-Bromo-3-methoxy-6-nitropyridineRelated Search:

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2-Bromo-3-methoxy-6-nitropyridine

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2-Bromo-3-methoxy-6-nitropyridine ISO 9001：2015 REACH

76066-07-4

blocks

Bromides

NitroCompounds

Pyridines

Heterocyclic Compounds

Heterocycles