ChemicalBook > CAS DataBase List > 5-HYDROXY-2-NITROPYRIDINE

5-HYDROXY-2-NITROPYRIDINE

Product Name
5-HYDROXY-2-NITROPYRIDINE
CAS No.
15206-26-5
Chemical Name
5-HYDROXY-2-NITROPYRIDINE
Synonyms
6-Nitropyridin-3-ol;6-NITRO-3-PYRIDINOL;3-Pyridinol, 6-nitro-;5-HYDROXY-2-NITROPYRIDINE;6-Nitro-3-hydroxy-pyridine;5-HYDROXY-2-NITROPYRIDINE 97%;3-Pyridinol,6-nitro-(8CI,9CI);5-HYDROXY-2-NITROPYRIDINE ISO 9001:2015 REACH
CBNumber
CB4691738
Molecular Formula
C5H4N2O3
Formula Weight
140.1
MOL File
15206-26-5.mol
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5-HYDROXY-2-NITROPYRIDINE Property

Boiling point:
443.8±30.0 °C(Predicted)
Density 
1.507
storage temp. 
Inert atmosphere,Room Temperature
pka
2.15±0.10(Predicted)
form 
solid
color 
Yellow
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Safety

HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
A417825
Product name
5-Hydroxy-2-nitropyridine
Packaging
100mg
Price
$65
Updated
2021/12/16
Usbiological
Product number
278770
Product name
5-Hydroxy-2-nitropyridine
Packaging
500mg
Price
$842
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0012707
Product name
5-HYDROXY-2-NITROPYRIDINE
Purity
95.00%
Packaging
250MG
Price
$933.24
Updated
2021/12/16
AK Scientific
Product number
W3318
Product name
5-Hydroxy-2-nitropyridine
Packaging
1g
Price
$315
Updated
2021/12/16
Matrix Scientific
Product number
072180
Product name
5-Hydroxy-2-nitropyridine
Purity
95+%
Packaging
1g
Price
$585
Updated
2021/12/16
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5-HYDROXY-2-NITROPYRIDINE Chemical Properties,Usage,Production

Synthesis

39856-50-3

15206-26-5

5-Bromo-2-nitropyridine (10.0 g, 49 mmol) was used as a starting material to form a suspension with borate (13.7 g, 54 mmol), Pd(OAc)2 (121 mg, 0.54 mmol) and KOAc (14.4 g, 147 mmol) in DMF (180 mL). The reaction mixture was heated to 100 °C and maintained at this temperature for 16 h of reaction. After completion of the reaction, the solvent was removed under vacuum. The remaining residue was mixed with EtOAc (600 mL) and the resulting EtOAc solution was washed sequentially with water (100 mL) and brine (100 mL) and then dried with Na2SO4. After drying, the solution was concentrated to a residue and subsequently mixed with NaBO4-H2O (19.0 g, 125 mmol), THF (180 mL) and H2O (180 mL). The resulting mixture was stirred at room temperature for 16 hours. At the end of the reaction, the aqueous and organic phases were separated and the organic phase was washed with EtOAc (100 mL x 2). The organic solutions were combined and concentrated to give the final 6-nitropyridin-3-ol (1.5 g, 21.8% yield) as a yellow solid.

References

[1] Patent: WO2014/52365, 2014, A1. Location in patent: Page/Page column 168

5-HYDROXY-2-NITROPYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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5-HYDROXY-2-NITROPYRIDINE Suppliers

PharmaBlock Sciences (Nanjing),Inc.
Tel
025-86918202 4000255188
Fax
86-025-86918232
Email
sales@pharmablock.com
Country
China
ProdList
5000
Advantage
55
Shijiazhuang Sdyano Fine Chemical Co., Ltd.
Tel
0311-89250318 031166536426
Fax
4000311741
Email
master@sjzsdyn.com
Country
China
ProdList
2807
Advantage
65
Pure Chemistry Scientific Inc.
Tel
001-857-928-2050 or 1-888-588-9418
Fax
001-617-206-9595
Email
sales@chemreagents.com
Country
United States
ProdList
10186
Advantage
62
Shanghai Hanhong Scientific Co.,Ltd.
Tel
021-54306202 13764082696
Email
info@hanhongsci.com
Country
China
ProdList
42934
Advantage
64
China Langchem Inc.
Tel
0086-21-58956006
Fax
0086-21-58956100
Country
China
ProdList
7811
Advantage
57
SpringPharma Tech Co.,Ltd
Tel
+86-25-68710855, +86-25-68710897
Fax
025-68710856
Email
sales@springpharma.net
Country
China
ProdList
1261
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62
Shanghai Topbiochem Technology Co., Ltd
Tel
021-58170097
Email
info@topbiochem.com
Country
China
ProdList
9510
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58
Shanghai Keepontech Co.,Ltd
Tel
021-54849683 13601642561
Fax
+86-21-54375689
Email
sales@keepontech.com
Country
China
ProdList
998
Advantage
59
Shanghai Yolne Chemical Co., Ltd.
Tel
021-62960152
Fax
021-52212593
Email
934678158@qq.com
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China
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9899
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55
Shanghai Raise Chemical Technology Co.,Ltd
Tel
+86-021-50935922
Fax
+86-021-33847795
Country
China
ProdList
7865
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55
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View Lastest Price from 5-HYDROXY-2-NITROPYRIDINE manufacturers

Shaanxi Dideu Medichem Co. Ltd
Product
6-Nitro-pyridin-3-ol 15206-26-5
Price
US $1.00-1.00/Kg/Drum
Min. Order
1g
Purity
98%
Supply Ability
50tons
Release date
2020-05-12
Dideu Industries Group Limited
Product
5-HYDROXY-2-NITROPYRIDINE 15206-26-5
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons min
Release date
2021-09-22
Career Henan Chemical Co
Product
5-HYDROXY-2-NITROPYRIDINE 15206-26-5
Price
US $9.80/KG
Min. Order
1g
Purity
≥99%
Supply Ability
100kg
Release date
2020-01-08