ChemicalBook > CAS DataBase List > 5-HYDROXY-2-NITROPYRIDINE

5-HYDROXY-2-NITROPYRIDINE

Product Name
5-HYDROXY-2-NITROPYRIDINE
CAS No.
15206-26-5
Chemical Name
5-HYDROXY-2-NITROPYRIDINE
Synonyms
6-Nitropyridin-3-ol;6-NITRO-3-PYRIDINOL;3-Pyridinol, 6-nitro-;5-HYDROXY-2-NITROPYRIDINE;6-Nitro-3-hydroxy-pyridine;5-HYDROXY-2-NITROPYRIDINE 97%;3-Pyridinol,6-nitro-(8CI,9CI);5-HYDROXY-2-NITROPYRIDINE ISO 9001：2015 REACH
CBNumber
CB4691738
Molecular Formula
C5H4N2O3
Formula Weight
140.1
MOL File
15206-26-5.mol
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5-HYDROXY-2-NITROPYRIDINE Property

Boiling point:
443.8±30.0 °C(Predicted)
Density 
1.507
storage temp. 
Inert atmosphere,Room Temperature
pka
2.15±0.10(Predicted)
form 
solid
color 
Yellow
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Safety

HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
A417825
Product name
5-Hydroxy-2-nitropyridine
Packaging
100mg
Price
$65
Updated
2021/12/16
Usbiological
Product number
278770
Product name
5-Hydroxy-2-nitropyridine
Packaging
500mg
Price
$842
Updated
2021/12/16
ChemScene
Product number
CS-W005777
Product name
6-Nitropyridin-3-ol
Purity
97.14%
Packaging
100mg
Price
$45
Updated
2021/12/16
Apolloscientific
Product number
OR959407
Product name
6-Nitropyridin-3-ol
Purity
95%
Packaging
100mg
Price
$63
Updated
2021/12/16
ChemScene
Product number
CS-W005777
Product name
6-Nitropyridin-3-ol
Purity
97.14%
Packaging
250mg
Price
$76
Updated
2021/12/16
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5-HYDROXY-2-NITROPYRIDINE Chemical Properties,Usage,Production

Synthesis

39856-50-3

15206-26-5

5-Bromo-2-nitropyridine (10.0 g, 49 mmol) was used as a starting material to form a suspension with borate (13.7 g, 54 mmol), Pd(OAc)2 (121 mg, 0.54 mmol) and KOAc (14.4 g, 147 mmol) in DMF (180 mL). The reaction mixture was heated to 100 °C and maintained at this temperature for 16 h of reaction. After completion of the reaction, the solvent was removed under vacuum. The remaining residue was mixed with EtOAc (600 mL) and the resulting EtOAc solution was washed sequentially with water (100 mL) and brine (100 mL) and then dried with Na2SO4. After drying, the solution was concentrated to a residue and subsequently mixed with NaBO4-H2O (19.0 g, 125 mmol), THF (180 mL) and H2O (180 mL). The resulting mixture was stirred at room temperature for 16 hours. At the end of the reaction, the aqueous and organic phases were separated and the organic phase was washed with EtOAc (100 mL x 2). The organic solutions were combined and concentrated to give the final 6-nitropyridin-3-ol (1.5 g, 21.8% yield) as a yellow solid.

References

[1] Patent: WO2014/52365, 2014, A1. Location in patent: Page/Page column 168

5-HYDROXY-2-NITROPYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 5-HYDROXY-2-NITROPYRIDINE manufacturers

Shaanxi Dideu Medichem Co. Ltd
Product
6-Nitro-pyridin-3-ol 15206-26-5
Price
US $1.00-1.00/Kg/Drum
Min. Order
1g
Purity
98%
Supply Ability
50tons
Release date
2020-05-12
Dideu Industries Group Limited
Product
5-HYDROXY-2-NITROPYRIDINE 15206-26-5
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons min
Release date
2021-09-22
Career Henan Chemical Co
Product
5-HYDROXY-2-NITROPYRIDINE 15206-26-5
Price
US $9.80/KG
Min. Order
1g
Purity
≥99%
Supply Ability
100kg
Release date
2020-01-08

15206-26-5, 5-HYDROXY-2-NITROPYRIDINERelated Search:

3-Methoxy-5-nitropyridin-2-ol 2-HYDROXY-5-NITROPYRIDINE,2-Hydroxy-5-nitropyridine, 99+%,2-Hydroxy-5-nitropyridine, 98+% 4-Hydroxy-3-Nitropyridine 3-Nitro-4-pyridinol 2-HYDROXY-5-NITROPYRIDINE-3-CARBOXYLIC ACID 2-HYDROXY-3-NITROPYRIDINE-5-CARBOXYLIC ACID 3-BROMO-2-HYDROXY-5-NITROPYRIDINE 3-HYDROXY-4-NITROPYRIDINE,3-Hydroxy-4-nitropyridine97% 5-BROMO-2-HYDROXY-3-NITROPYRIDINE,3-Bromo-6-hydroxy -5-nitropyridine,5-Bromo-3-nitro-2-pyridinol, 5-Bromo-2-hydroxy-3-nitropyridine 3-HYDROXY-5-NITROPYRIDINE,3-HYDROXY-5-NITROPYRIDINE 98%,3-Hydroxy-5-nitropyridine98% 4-Chloro-2-hydroxy-3-nitropyridine 2-Hydroxy-4-nitropyridine97%,2-HYDROXY-4-NITROPYRIDINE 5-CHLORO-2-HYDROXY-3-NITROPYRIDINE,5-Chloro-2-hydroxy-3-nitropyridine 95+% 3-CHLORO-2-HYDROXY-5-NITROPYRIDINE 4-Hydroxy-2-nitropyridine97%,4-HYDROXY-2-NITROPYRIDINE,4-HYDROXY-2-NITROPYRIDINE 97% 4-Hydroxy-3-nitropyridine N-oxide 97+%,4-HYDROXY-3-NITROPYRIDINE N-OXIDE 2,4-Hydroxy-3-nitropyridine. 6-Hydroxy-5-nitro-2-picoline 5-FLUORO-2-HYDROXY-3-NITROPYRIDINE

  • 5-HYDROXY-2-NITROPYRIDINE
  • 6-NITRO-3-PYRIDINOL
  • 3-Pyridinol,6-nitro-(8CI,9CI)
  • 5-HYDROXY-2-NITROPYRIDINE 97%
  • 6-Nitropyridin-3-ol
  • 3-Pyridinol, 6-nitro-
  • 5-HYDROXY-2-NITROPYRIDINE ISO 9001：2015 REACH
  • 6-Nitro-3-hydroxy-pyridine
  • 15206-26-5
  • Heterocycle-Pyridine series
  • Pyridines
  • NITRO