ChemicalBook > CAS DataBase List > 3-bromo-5-methylbenzoic acid

3-bromo-5-methylbenzoic acid

Product Name
3-bromo-5-methylbenzoic acid
CAS No.
58530-13-5
Chemical Name
3-bromo-5-methylbenzoic acid
Synonyms
5-broMo-3-Methylbenzoic acid;3-bromo-5-methylbenzoic acid;Benzoic acid, 3-bromo-5-methyl-
CBNumber
CB61558780
Molecular Formula
C8H7BrO2
Formula Weight
215.04
MOL File
58530-13-5.mol
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3-bromo-5-methylbenzoic acid Property

Melting point:
178-179.5℃
Boiling point:
320.3±30.0 °C(Predicted)
Density 
1.599±0.06 g/cm3 (20 ºC 760 Torr)
storage temp. 
Sealed in dry,Room Temperature
form 
solid
pka
3.88±0.10(Predicted)
color 
Pale yellow
InChIKey
NWOMVQDBDBUANF-UHFFFAOYSA-N
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Safety

HS Code 
2916310090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
S17907
Product name
3-BROMO-5-METHYLBENZOIC ACID
Purity
Aldrich
Packaging
100mg
Price
$179
Updated
2024/03/01
TRC
Product number
B687935
Product name
3-BROMO-5-METHYLBENZOIC ACID
Packaging
5g
Price
$415
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB71947
Product name
3-Bromo-5-methylbenzoic acid
Packaging
25g
Price
$550
Updated
2021/12/16
SynQuest Laboratories
Product number
2721-9-18
Product name
3-Bromo-5-methylbenzoic acid
Packaging
25g
Price
$864
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0068600
Product name
3-BROMO-5-METHYL-BENZOIC ACID
Purity
95.00%
Packaging
1G
Price
$958.65
Updated
2021/12/16
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3-bromo-5-methylbenzoic acid Chemical Properties,Usage,Production

Chemical Properties

Off-white powder

Uses

3-Bromo-5-methylbenzoic Acid is an intermediate used to synthesize quinoline amide derivatives as novel VEGFR-2 inhibitors

Synthesis

1-bromo-3,5-dimethylbenzene (15 g, 81 mmol, 1.0 eq) in a mixture of pyridine (133 mL) and H2O (83 mL) was heated to 80°C. KMnO4 (25.6 g, 162 mmol, 2.0 eq) was added in portions over 45 min. After the addition was completed, heating was continued at 80°C for 1.5 h. The hot solution was then filtered, and the filtrate was acidified by addition of concentrated hydrochloric acid. The aqueous solution was extracted with EtOAc and the combined organic extracts washed with water and brine, dried (Na2SO4), filtered and evaporated in vacuo. The residue was purified by column chromatography (CH2Cl2 : MeOH, 80:1 to 40:1) to give 3-bromo-5-methylbenzoic acid. White solid, yield (5.2 g, 29 %). LC-MS: m/z 212.9, 215 [M+H]+. 1H NMR (400 MHz, MeOD) δ 7.91 (s, 1H), 7.79 (s, 1H), 7.57 (s, 1H), 2.38 (s, 3H).

3-bromo-5-methylbenzoic acid Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-bromo-5-methylbenzoic acid manufacturers

Hebei Weibang Biotechnology Co., Ltd
Product
3-bromo-5-methylbenzoic acid 58530-13-5
Price
US $10.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
10 mt
Release date
2024-11-05
Changzhou Anxuan Chemical Co., Ltd
Product
3-bromo-5-methylbenzoic acid 58530-13-5
Price
US $0.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
1TON
Release date
2023-02-15
Henan Bao Enluo International TradeCo.，LTD
Product
3-bromo-5-methylbenzoic acid 58530-13-5
Price
US $50.00/kg
Min. Order
1kg
Purity
99.9%
Supply Ability
10000MT
Release date
2023-08-02

58530-13-5, 3-bromo-5-methylbenzoic acidRelated Search:

Benzoic acid, 3-amino-5-methyl- (9CI) 4-CHLORO-2-METHYLBENZOIC ACID TERT-BUTYL 4-BROMO-3-METHYLBENZOATE 4-HYDROXY-3-METHYLBENZOIC ACID 3-Hydroxy-4-methylbenzoic acid 3-CHLORO-5-METHYL-BENZOIC ACID 4-Amino-2-methylbenzoic acid 3-CHLORO-4-HYDROXYBENZOIC ACID 5-Amino-2-methylbenzoic acid 4-Methyl-3-nitrobenzoic acid 5-HYDROXY-2-METHYL-BENZOIC ACID 3-Hydroxy-2-methylbenzoic acid 2-Methyl-3-nitrobenzoic acid 5-BROMO-2,3-DIHYDROBENZOFURAN-7-CARBOXYLIC ACID 1-Piperidinecarbothioamide, N-[3-(2,4,6-trichlorophenoxy)-1-propyn-1-yl]- 3-Bromo-5-(trifluoromethyl)benzoic acid DIMETHYL 5-BROMOISOPHTHALATE 2-AMINO-3-BROMO-5-METHYLBENZOIC ACID

  • 3-bromo-5-methylbenzoic acid
  • 5-broMo-3-Methylbenzoic acid
  • Benzoic acid, 3-bromo-5-methyl-
  • 58530-13-5