4-Amino-2-methylbenzoic acid
- Product Name
- 4-Amino-2-methylbenzoic acid
- CAS No.
- 2486-75-1
- Chemical Name
- 4-Amino-2-methylbenzoic acid
- Synonyms
- 4-Amino-o-toluic;Tolvaptan Impurity 33;4-Amino-2-methylbenzoicaci;4-Amino-2-methybenzoic acid;4-AMINO-2-METHYLBENZOIC ACID;2-METHYL-4-AMINO-BENZOIC ACID;4-amino-2-methylbenozoic acid;4-azanyl-2-methyl-benzoic acid;Benzoic acid, 4-amino-2-methyl-;4-Amino-2-methylbenzoic Acid >
- CBNumber
- CB4321053
- Molecular Formula
- C8H9NO2
- Formula Weight
- 151.16
- MOL File
- 2486-75-1.mol
4-Amino-2-methylbenzoic acid Property
- Melting point:
- 160-165 °C
- Boiling point:
- 339.5±30.0 °C(Predicted)
- Density
- 1.254±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- solubility
- soluble in Methanol
- form
- Solid
- pka
- 4.86±0.25(Predicted)
- color
- Light orange to Yellow to Green
- InChI
- InChI=1S/C8H9NO2/c1-5-4-6(9)2-3-7(5)8(10)11/h2-4H,9H2,1H3,(H,10,11)
- InChIKey
- XRSQZFJLEPBPOZ-UHFFFAOYSA-N
- SMILES
- C(O)(=O)C1=CC=C(N)C=C1C
- CAS DataBase Reference
- 2486-75-1(CAS DataBase Reference)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- 691437
- Product name
- 4-Amino-2-methylbenzoic acid
- Purity
- 95%
- Packaging
- 5g
- Price
- $85.5
- Updated
- 2025/07/31
- Product number
- A2349
- Product name
- 4-Amino-2-methylbenzoic Acid
- Purity
- >98.0%(HPLC)(T)
- Packaging
- 5g
- Price
- $30
- Updated
- 2025/07/31
- Product number
- A2349
- Product name
- 4-Amino-2-methylbenzoic Acid
- Purity
- >98.0%(HPLC)(T)
- Packaging
- 25g
- Price
- $120
- Updated
- 2025/07/31
- Product number
- A637858
- Product name
- 4-Amino-2-methylbenzoic Acid
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- A637858
- Product name
- 4-Amino-2-methylbenzoic Acid
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
4-Amino-2-methylbenzoic acid Chemical Properties,Usage,Production
Chemical Properties
White powder
Uses
peptide synthesis
reaction suitability
reaction type: solution phase peptide synthesis
Synthesis
1975-51-5
2486-75-1
GENERAL STEPS: Prior to each experiment, the tubular reaction apparatus was equilibrated by pumping solvent for 30 min at 16 bar hydrogen pressure (see Fig. 4). An Omnifit reaction cartridge (20.0 mm outer diameter, 15.0 mm inner diameter) containing 1 g Pd/C catalyst was used. To prevent overpressurization of the system in case of blockage, the upper pressure of the Knauer pump was set to 25 bar. with the injection ring disconnected from the flow line, the injection ring was opened and manually injected with 3.6 mL of a 0.076 M ethanol solution of 2-methyl-4-nitrobenzoic acid (excess feedstock solution in the ring was recovered for reuse). The injection ring was then closed and plugged into the flow stream. Collect the product at the outlet of the system downstream of the backpressure regulator for 120 min. The solvent is removed by reduced pressure distillation (first using a rotary evaporator and then a secondary rotary vane pump) to give 4-amino-2-methylbenzoic acid.
References
[1] Tetrahedron, 2018, vol. 74, # 47, p. 6795 - 6803
[2] Chemische Berichte, 1884, vol. 17, p. 161
[3] Patent: US2012/46467, 2012, A1. Location in patent: Page/Page column 26
4-Amino-2-methylbenzoic acid Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4-Amino-2-methylbenzoic acid manufacturers
- Product
- 4-Amino-2-methylbenzoic acid 2486-75-1
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 500000kg
- Release date
- 2024-10-28
- Product
- 4-Amino-2-methylbenzoic acid 2486-75-1
- Price
- US $70.00-13.00/kg
- Min. Order
- 1kg
- Purity
- 0.99
- Supply Ability
- 20 tons
- Release date
- 2023-09-14
- Product
- Tolvaptan Impurity 33
- Price
- US $0.00-0.00/mg
- Min. Order
- 10mg
- Purity
- 98%
- Supply Ability
- 500mg
- Release date
- 2024-08-12