Ethyl 2,2-dimethylphenylacetate

Product Name: Ethyl 2,2-dimethylphenylacetate
CAS No.: 2901-13-5
Chemical Name: Ethyl 2,2-dimethylphenylacetate
Synonyms: NSC 29060;2-dimethylphenylacetate;Ethyl 2-phenylisobutyrate;Ethyl Dimethylphenylacetate;ETHYL DIMETHYLBENZENEACETATE;Ethyl Dimethylbenzeneacetatee;ETHYL 2,2-DIMETHYLPHENYLACETATE;Ethyl a,a-Dimethylphenylacetate;Ethyl a,a-Dimethylbenzeneacetate;Ethyl 2,2-diMethylbenzeneacetate
CBNumber: CB6156301
Molecular Formula: C12H16O2
Formula Weight: 192.25
MOL File: 2901-13-5.mol

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Ethyl 2,2-dimethylphenylacetate Property

Boiling point:: 68-71 °C(Press: 0.5-0.6 Torr)
Density: 1.0039 g/cm3
vapor pressure: 10-1013.3hPa at 96.5-234.3℃
storage temp.: Sealed in dry,Room Temperature
solubility: Chloroform (Slightly), Methanol (Slightly)
form: Oil
color: Clear Colourless to Pale Yellow
LogP: 3.5
Surface tension: 5.92mN/m at 159.4mg/L and 20℃
CAS DataBase Reference: 2901-13-5(CAS DataBase Reference)

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Safety

HS Code: 2916399090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H412Harmful to aquatic life with long lasting effects

Precautionary statements

P273Avoid release to the environment.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: E916810
Product name: EthylDimethylphenylacetate
Packaging: 10g
Price: $875
Updated: 2021/12/16

AK Scientific

Product number: 2918AB
Product name: Ethyl2-methyl-2-phenylpropanoate
Packaging: 1g
Price: $10
Updated: 2021/12/16

Apolloscientific

Product number: OR963290
Product name: Ethyldimethylbenzeneacetate
Purity: 95%
Packaging: 1g
Price: $182
Updated: 2021/12/16

Matrix Scientific

Product number: 083368
Product name: Ethyl 2-methyl-2-phenylpropanoate
Purity: 97%
Packaging: 1g
Price: $194
Updated: 2021/12/16

Apolloscientific

Product number: OR963290
Product name: Ethyldimethylbenzeneacetate
Purity: 95%
Packaging: 5g
Price: $573
Updated: 2021/12/16

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Ethyl 2,2-dimethylphenylacetate Chemical Properties,Usage,Production

Chemical Properties

Pale Yellow Liquid

Uses

Ethyl Dimethylphenylacetate (cas# 2901-13-5) is a compound useful in organic synthesis.

Synthesis

64-17-5

826-55-1

2901-13-5

Example 1: Synthesis of ethyl 2,2-dimethylphenylacetate In a 10L three-necked flask, 2-methyl-2-phenylpropanecarboxylic acid (500g, 3.1 mol) and 2.5L of dichloromethane were added and dissolved with stirring at room temperature. Subsequently, thionyl chloride (750 g, 6.3 mol) was added slowly, and after addition, the reaction system was heated to reflux and maintained for 15 hours. After the reaction was completed, cooled to room temperature, 400mL of anhydrous ethanol was added slowly dropwise, and stirring was continued for 2 hours after the dropwise addition. The reaction solution was adjusted to pH 9-10 with 10% NaOH solution and the completion of the reaction was monitored by thin layer chromatography (TLC). The organic layer was separated, washed twice each with saturated sodium bicarbonate solution and saturated sodium chloride solution in turn, and dried over anhydrous sodium sulfate. The solvent was removed by concentration under reduced pressure to give a colorless oily product, ethyl 2,2-dimethylbenzeneacetate 560 g, 96% yield.

References

[1] Patent: CN104276952, 2016, B. Location in patent: Paragraph 0027; 0028
[2] MedChemComm, 2013, vol. 4, # 2, p. 367 - 370
[3] Tetrahedron, 2009, vol. 65, # 2, p. 456 - 460
[4] Journal of the American Chemical Society, 1968, vol. 90, p. 2082 - 2096
[5] Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2001, vol. 40, # 8, p. 717 - 718

Ethyl 2,2-dimethylphenylacetate Preparation Products And Raw materials

Raw materials

Preparation Products

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Ethyl 2,2-dimethylphenylacetate Suppliers

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View Lastest Price from Ethyl 2,2-dimethylphenylacetate manufacturers

Career Henan Chemical Co

Product: Ethyl 2,2-dimethylphenylacetate 2901-13-5
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100KG
Release date: 2019-12-25

2901-13-5, Ethyl 2,2-dimethylphenylacetateRelated Search:

Ethyl phenylacetate Ethanol Ethyl acetate Ethyl formate Ethyl 4-hydroxyphenylacetate Ethyl cellulose CHLOROETHANE Ethylparaben Ethyl 4-bromophenylacetate Ethyl chloroacetate Ethyl 4-nitrophenylacetate Ethylbenzene Ethyl acrylate Ethyl bromoacetate CARBETAPENTANE CITRATE MEPERIDINE HYDROCHLORIDE PROADIFEN HYDROCHLORIDE Diethyl ether

ETHYL DIMETHYLBENZENEACETATE

ETHYL 2,2-DIMETHYLPHENYLACETATE

a,a-Dimethyl-benzeneacetic Acid Ethyl Ester

a-methyl-hydratropic Acid Ethyl Ester

Ethyl 2-phenylisobutyrate

Ethyl a,a-Dimethylbenzeneacetate

Ethyl a,a-Dimethylphenylacetate

Ethyl Dimethylphenylacetate

NSC 29060

Ethyl Dimethylbenzeneacetatee

α-methyl-hydratropic Acid Ethyl Ester

Benzeneacetic acid, a,a-diMethyl-, ethyl ester

α,α-DiMethyl-benzeneacetic Acid Ethyl Ester

Benzeneacetic acid, alpha,alpha-diMethyl-, ethyl ester

ethyl 2-methyl-2-phenylpropanoate

ethyl 2-methyl-2-phenyl-propanoate

Ethyl 2,2-diMethylbenzeneacetate

2-(6,6-dimethyl-1-cyclohexa-2,4-dienyl)acetic acid ethyl ester

Benzeneacetic acid, α,α-dimethyl-, ethyl ester

2-dimethylphenylacetate

Benzeneacetic acid, α,α-dimethyl-, ethyl ester (9CI, ACI)

alpha,alpha-Dimethylbenzeneacetic acid ethyl ester

α,α-Dimethyl-ethyl ester benzeneacetic acid

2901-13-5

Aromatics Compounds

Aromatics