ChemicalBook > CAS DataBase List > Ethyl 4-fluoro-3-nitrobenzoate

Ethyl 4-fluoro-3-nitrobenzoate

Product Name
Ethyl 4-fluoro-3-nitrobenzoate
CAS No.
367-80-6
Chemical Name
Ethyl 4-fluoro-3-nitrobenzoate
Synonyms
RARECHEM AL BI 0858;4-fluoro-3-nitro-benzoate;Ethyl 3-Nitro-4-Fluorobenzoate;ETHYL 4-FLUORO-3-NITROBENZOATE;Ethyl 4-fluoro-3-nitrobenzoate-2;5-(Ethoxycarbonyl)-2-fluoronitrobenzene;4-FLUORO-3-NITROBENZOIC ACID ETHYL ESTER;Benzoic acid, 4-fluoro-3-nitro-, ethyl ester
CBNumber
CB6229357
Molecular Formula
C9H8FNO4
Formula Weight
213.16
MOL File
367-80-6.mol
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Ethyl 4-fluoro-3-nitrobenzoate Property

Melting point:
45.3 °C
Boiling point:
312.3±22.0 °C(Predicted)
Density 
1.333±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
form 
crystalline powder
color 
Pale creamy lemon
CAS DataBase Reference
367-80-6(CAS DataBase Reference)
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Safety

HS Code 
2918300090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
E918238
Product name
Ethyl4-fluoro-3-nitrobenzoate
Packaging
250mg
Price
$55
Updated
2021/12/16
TRC
Product number
E918238
Product name
Ethyl4-fluoro-3-nitrobenzoate
Packaging
1g
Price
$75
Updated
2021/12/16
Apolloscientific
Product number
PC1485
Product name
Ethyl4-fluoro-3-nitrobenzoate
Packaging
5g
Price
$22
Updated
2021/12/16
SynQuest Laboratories
Product number
4654-3-X4
Product name
Ethyl 4-fluoro-3-nitrobenzoate
Packaging
5G
Price
$24
Updated
2021/12/16
AK Scientific
Product number
M402
Product name
Ethyl4-fluoro-3-nitrobenzoate
Packaging
5g
Price
$27
Updated
2021/12/16
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Ethyl 4-fluoro-3-nitrobenzoate Chemical Properties,Usage,Production

Synthesis

64-17-5

453-71-4

367-80-6

Step 1: 5.00 g (27.0 mmol) of 4-fluoro-3-nitrobenzoic acid was dissolved in 50 mL of saturated ethanolic hydrochloric acid solution (1.25 M) and the reaction was refluxed for 15 hours. After completion of the reaction, the reaction mixture was evaporated using a rotary evaporator. Purification by fast column chromatography [silica gel, eluent petroleum ether/ethyl acetate (4:1)] afforded 5.48 g (25.7 mmol, 95%) of ethyl 4-fluoro-3-nitrobenzoate as a colorless solid. Thin layer chromatography (TLC) Rf = 0.48 [silica gel, petroleum ether/ethyl acetate (4:1)]. Mass Spectrometry (ESI) m/z: [M + H]+ calculated value of 214.

References

[1] Bioorganic and Medicinal Chemistry Letters, 2006, vol. 16, # 7, p. 1859 - 1863
[2] Patent: US2007/112033, 2007, A1. Location in patent: Page/Page column 17-18
[3] Patent: US2013/79306, 2013, A1. Location in patent: Paragraph 0226; 0227; 0228; 0229
[4] Journal of Medicinal Chemistry, 2012, vol. 55, # 16, p. 7262 - 7272
[5] Journal of Medicinal Chemistry, 2018, vol. 61, # 4, p. 1646 - 1663

Ethyl 4-fluoro-3-nitrobenzoate Preparation Products And Raw materials

Raw materials

Preparation Products

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Ethyl 4-fluoro-3-nitrobenzoate Suppliers

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View Lastest Price from Ethyl 4-fluoro-3-nitrobenzoate manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD
Product
Ethyl 4-fluoro-3-nitrobenzoate 367-80-6
Price
US $3.00-9.00/KG
Min. Order
0.1KG
Purity
99%
Supply Ability
g-kg-tons, free sample is available
Release date
2025-06-25
Career Henan Chemical Co
Product
Ethyl 4-fluoro-3-nitrobenzoate 367-80-6
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
10000KGS
Release date
2020-01-02

367-80-6, Ethyl 4-fluoro-3-nitrobenzoateRelated Search:

Ethanol Ethyl acrylate Ethyl 2-chloromethylbenzoate Ethylbenzene Ethylparaben CHLOROETHANE 4-Fluoronitrobenzene Urethane Ethyl cellulose Ethyl benzoate 1-Fluoro-2-nitrobenzene Ethyl formate Ethyl acetate Fluorine 2-AMINO-6-FLUORO-3-NITROBENZOIC ACID ETHYL ESTER 4-Fluoro-3-nitrobenzoic acid Diethyl ether Ethyl chloroformate

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