ChemicalBook > CAS DataBase List > TERT-BUTYL-(2-IODO-ETHOXY)-DIMETHYL-SILANE

TERT-BUTYL-(2-IODO-ETHOXY)-DIMETHYL-SILANE

Product Name: TERT-BUTYL-(2-IODO-ETHOXY)-DIMETHYL-SILANE
CAS No.: 101166-65-8
Chemical Name: TERT-BUTYL-(2-IODO-ETHOXY)-DIMETHYL-SILANE
Synonyms: DK442;DKSI024;DKFELEX0093;tert-Butyl(2-iodoethoxy);Short-butyl-(2-iodoethoxy)dimethylsilane;TERT-BUTYL-(2-IODO-ETHOXY)-DIMETHYL-SILANE;1-Iodo-2-(tert-butyldimethylsilyloxy)ethane;1-(tert-Butyldimethylsilyloxy)-2-iodoethane;(1,1-DIMETHYLETHYL)(2-IODOETHOXY)DIMETHYL-SILANE;Silane,(1,1-dimethylethyl)(2-iodoethoxy)dimethyl-
CBNumber: CB62452890
Molecular Formula: C8H19IOSi
Formula Weight: 286.23
MOL File: 101166-65-8.mol

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TERT-BUTYL-(2-IODO-ETHOXY)-DIMETHYL-SILANE Property

Boiling point:: 210℃
Density: 1.291
refractive index: 1.48
Flash point:: 81℃
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
form: clear liquid
color: Colorless to Yellow to Orange
InChI: InChI=1S/C8H19IOSi/c1-8(2,3)11(4,5)10-7-6-9/h6-7H2,1-5H3
InChIKey: CAAUZMMMFDVBFD-UHFFFAOYSA-N
SMILES: [Si](C(C)(C)C)(OCCI)(C)C

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Safety

HS Code: 2931.90.9010

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H227Combustible liquid

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

P370+P378In case of fire: Use … for extinction.

P403+P235Store in a well-ventilated place. Keep cool.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TCI Chemical

Product number: B5885
Product name: tert-Butyl(2-iodoethoxy)dimethylsilane
Packaging: 1G
Price: $41
Updated: 2025/07/31

TRC

Product number: B810955
Product name: tert-Butyl(2-iodoethoxy)dimethylsilane
Packaging: 50mg
Price: $65
Updated: 2021/12/16

Oakwood

Product number: 214589
Product name: tert-Butyl(2-iodoethoxy)dimethylsilane
Purity: 95+%
Packaging: 250mg
Price: $20
Updated: 2021/12/16

Matrix Scientific

Product number: 089725
Product name: tert-Butyl(2-iodoethoxy)dimethylsilane
Purity: 95+%
Packaging: 1g
Price: $52
Updated: 2021/12/16

AK Scientific

Product number: J94805
Product name: tert-Butyl(2-iodoethoxy)dimethylsilane
Packaging: 5g
Price: $160
Updated: 2021/12/16

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TERT-BUTYL-(2-IODO-ETHOXY)-DIMETHYL-SILANE Chemical Properties,Usage,Production

Synthesis

624-76-0

18162-48-6

101166-65-8

(i) Preparation of tert-butyl-(2-iodoethoxy)dimethylsilane To a stirred solution of 2-iodoethanol (17.2 g, 100 mmol) and imidazole (8.17 g, 120 mmol) in dichloromethane (100 mL) was slowly added tert-butyldimethylmethylsilyl chloride (15.83 g, 105 mmol) at a controlled rate of addition to maintain the reaction temperature at no more than 30 °C. The reaction was carried out by stirring the mixture for 17 hours. After addition, the reaction mixture was continued to be stirred for 17 hours. Upon completion of the reaction, the organic phase was washed sequentially with water (2 x 50 mL) and brine (50 mL), followed by drying with anhydrous magnesium sulfate. The solvent was evaporated under reduced pressure to afford the colorless liquid-like product tert-butyl-(2-iodoethoxy)dimethylsilane (28.0 g, 97.8 mmol, 98% yield). 1H-NMR (400 MHz, CDCl3): δ = 3.83 (t, 2H, J = 7.0 Hz), 3.20 (t, 2H, J = 7.0 Hz), 0.90 (s, 9H), 0.08 (s, 6H) ppm.

References

[1] Chemistry - A European Journal, 2017, vol. 23, # 5, p. 1157 - 1165
[2] Analytical Chemistry, 2003, vol. 75, # 21, p. 6002 - 6010
[3] Patent: US2013/59970, 2013, A1. Location in patent: Paragraph 0311; 0312; 0313
[4] Patent: US2014/249162, 2014, A1. Location in patent: Paragraph 0234
[5] Patent: EP2781519, 2014, A1. Location in patent: Paragraph 0232

TERT-BUTYL-(2-IODO-ETHOXY)-DIMETHYL-SILANE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from TERT-BUTYL-(2-IODO-ETHOXY)-DIMETHYL-SILANE manufacturers

Shanghai Daken Advanced Materials Co.,Ltd

Product: TERT-BUTYL-(2-IODO-ETHOXY)-DIMETHYL-SILANE 101166-65-8
Price: US $0.00/KG
Min. Order: 1KG
Purity: 98.00%
Supply Ability: 1000KG /month
Release date: 2021-11-26

Career Henan Chemical Co

Product: TERT-BUTYL-(2-IODO-ETHOXY)-DIMETHYL-SILANE 101166-65-8
Price: US $1.00/KG
Min. Order: 1KG
Purity: 97%
Supply Ability: 200kg
Release date: 2020-02-01

101166-65-8, TERT-BUTYL-(2-IODO-ETHOXY)-DIMETHYL-SILANERelated Search:

(TERT.-BUTYLDIMETHYLSILYLOXY)ETHANOL 2-(N-Boc-aMinoMethyl)-5-chloropyridine tert-Butyldiphenylsilane TERT-BUTYL PROPIOLATE TERT-BUTYL 3-(4-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-1H-PYRAZOL-1-YL)AZETIDINE-1-CARBOXYLATE tert-Butyl N-(3-aminopropyl)-N-methylcarbamate TERT-BUTYLDIMETHYL(2-PROPYNYLOXY)SILANE TERT-BUTYL(4-IODOBUTOXY)DIMETHYLSILANE tert-butyl(4S)-4-(3-bromopropyl)-2,2-dimethyl-1,3-oxazolidine-3-carboxylate tert-butyl 7-(aminomethyl)-6,9-dioxa-2-azaspiro[4.5]decane- 2-carboxylate hydrochloride Tert-butyl3-acetylpyrrolidine-1-carboxylate TERT-BUTYL-(2-IODO-ETHOXY)-DIMETHYL-SILANE

TERT-BUTYL-(2-IODO-ETHOXY)-DIMETHYL-SILANE

(1,1-DIMETHYLETHYL)(2-IODOETHOXY)DIMETHYL-SILANE

1-(tert-Butyldimethylsilyloxy)-2-iodoethane

1-Iodo-2-(tert-butyldimethylsilyloxy)ethane

2-Iodo-1-(1,1,2,2-tetramethyl-1-silapropoxy)ethane

Silane,(1,1-dimethylethyl)(2-iodoethoxy)dimethyl-

tert-Butyl(2-iodoethoxy)

DK442

DKFELEX0093

DKSI024

Short-butyl-(2-iodoethoxy)dimethylsilane

101166-65-8

C8H19IOSi