ChemicalBook > CAS DataBase List > 2-(4-Cyclohexylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

2-(4-Cyclohexylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Product Name
2-(4-Cyclohexylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.
820223-94-7
Chemical Name
2-(4-Cyclohexylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
Synonyms
4-Cyclohexylphenylboronic acid, pinacol ester;2-(4-Cyclohexylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane;1,3,2-Dioxaborolane, 2-(4-cyclohexylphenyl)-4,4,5,5-tetramet...;1,3,2-Dioxaborolane, 2-(4-cyclohexylphenyl)-4,4,5,5-tetramethyl-
CBNumber
CB62513425
Molecular Formula
C18H27BO2
Formula Weight
286.22
MOL File
820223-94-7.mol
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2-(4-Cyclohexylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane Property

Boiling point:
387.1±21.0 °C(Predicted)
Density 
1.00±0.1 g/cm3(Predicted)
storage temp. 
Inert atmosphere,2-8°C
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Safety

HS Code 
2931900090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H317May cause an allergic skin reaction

H319Causes serious eye irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
C991785
Product name
4-Cyclohexylphenylboronicacid,pinacolester
Packaging
500mg
Price
$70
Updated
2021/12/16
AK Scientific
Product number
X2274
Product name
4-Cyclohexylphenylboronicacidpinacolester
Packaging
1g
Price
$81
Updated
2021/12/16
SynQuest Laboratories
Product number
6760-1-56
Product name
2-(4-Cyclohexylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
Packaging
1g
Price
$157
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
BOR0006227
Product name
2-(4-CYCLOHEXYLPHENYL)-4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLANE
Purity
95.00%
Packaging
1G
Price
$179.55
Updated
2021/12/16
Matrix Scientific
Product number
093237
Product name
2-(4-Cyclohexylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
Purity
95+%
Packaging
1g
Price
$189
Updated
2021/12/16
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2-(4-Cyclohexylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane Chemical Properties,Usage,Production

Synthesis

25109-28-8

73183-34-3

820223-94-7

Under nitrogen protection, 0.382 g of bis(pinacolato)diboron (1.2 eq.), 27.5 mg of dichloro[[1,1 '-bis(diphenylphosphino)ferrocene]palladium(II) (0.03 eq.), 41.7 mg of [1,1 '-bis(diphenylphosphino)ferrocene] (0.06 eq.), and 0.369 g of potassium acetate (3 eq.) were sequentially added to a solution containing 0.3 g of 1-bromo-4-cyclohexylbenzene to a 5 mL solution of degassed 1,4-dioxane. The reaction mixture was stirred at 80 °C for 17 hours. After completion of the reaction, the reaction solution was diluted with 100 mL of ethyl acetate, washed three times sequentially with 60 mL of water, the organic phase was dried with anhydrous sodium sulfate, and the solvent was removed by concentration under reduced pressure. The crude product was purified by silica gel column chromatography (eluent: 95/5 heptane/ethyl acetate) to give 0.2 g 4-cyclohexylphenylboronic acid pinacol ester in 56% yield.1H NMR (DMSO) δ (ppm): 7.60 (d, 2H), 7.20 (d, 2H), 1.70 (m, 5H), 1.40 (m, 4H), 1.30 (m, 12H) .

References

[1] Patent: WO2005/3115, 2005, A1. Location in patent: Page/Page column 28

2-(4-Cyclohexylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane Preparation Products And Raw materials

Raw materials

Preparation Products

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2-(4-Cyclohexylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane Suppliers

China 34 India 3 United Kingdom 1 United States 5 Global 43
Shanghai Hanhong Scientific Co.,Ltd.
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021-54306202 13764082696
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info@hanhongsci.com
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China
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9ding chemical ( Shanghai) Limited
Tel
4009209199
Fax
86-021-52271987
Email
sales@9dingchem.com
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China
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18209
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AllyChem Co., Ltd.
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0411-62313318 13942603642
Fax
0411-87549748
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China
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ShangHai AmK Pharmaceutical Technology Co., Ltd.
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微信 17321281695 18019252918
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17321281695
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China
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Shijiazhuang Sdyano Fine Chemical Co., Ltd.
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0311-89250318 031166536426
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master@sjzsdyn.com
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China
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Amadis Chemical Company Limited
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0086-571-89925065
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AAB-PHARMA LIMITED
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025-66800956 18800000000
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qq3325708371
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Zhengzhou Huiju Chemical Co., Ltd.
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0371-55900031 18137872243
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QQ：2853979815
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2853979815@qq.com
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China
ProdList
9975
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Sichuan BaiPeng Biotechnology Co., Ltd.
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028-65791793 18140026355
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QQ568470422
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568470422@qq.com
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China
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Aikon International Limited
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025-58859352 18068836627
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02557626880
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View Lastest Price from 2-(4-Cyclohexylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD
Product
2-(4-Cyclohexylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane 820223-94-7
Price
US $3.00-9.00/KG
Min. Order
0.1KG
Purity
99%
Supply Ability
g-kg-tons, free sample is available
Release date
2025-07-03
Career Henan Chemical Co
Product
2-(4-Cyclohexylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane 820223-94-7
Price
US $9.80/KG
Min. Order
1KG
Purity
≥98%
Supply Ability
20 tons
Release date
2020-01-02

820223-94-7, 2-(4-Cyclohexylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolaneRelated Search:

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