Ethyl 5-broMo-2-furoate, 97+%
- Product Name
- Ethyl 5-broMo-2-furoate, 97+%
- CAS No.
- 6132-37-2
- Chemical Name
- Ethyl 5-broMo-2-furoate, 97+%
- Synonyms
- Ethyl 5-bromofuran-2-carboxylate;Ethyl 5-broMo-2-furoate;Ethyl 5-broMo-2-furoate, 97+%;ethyl 5-broMo-2-furancarboxylate;5-Bromo-2-furancarboxylic Acid Ethyl Ester;2-Furancarboxylic acid, 5-broMo-, ethyl ester
- CBNumber
- CB62549097
- Molecular Formula
- C7H7BrO3
- Formula Weight
- 219.03
- MOL File
- 6132-37-2.mol
Ethyl 5-broMo-2-furoate, 97+% Property
- Melting point:
- 17 °C
- Boiling point:
- 234 °C
- Density
- 1.533±0.06 g/cm3(Predicted)
- refractive index
- 1.52
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- form
- clear liquid
- color
- Colorless to Light orange to Yellow
- InChI
- InChI=1S/C7H7BrO3/c1-2-10-7(9)5-3-4-6(8)11-5/h3-4H,2H2,1H3
- InChIKey
- GVAPLPBPJARJEY-UHFFFAOYSA-N
- SMILES
- O1C(Br)=CC=C1C(OCC)=O
Safety
- HS Code
- 2932.19.5100
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- E1285
- Product name
- Ethyl 5-Bromo-2-furancarboxylate
- Purity
- >97.0%(GC)
- Packaging
- 1g
- Price
- $93
- Updated
- 2025/07/31
- Product number
- E1285
- Product name
- Ethyl 5-Bromo-2-furancarboxylate
- Purity
- >97.0%(GC)
- Packaging
- 5g
- Price
- $372
- Updated
- 2025/07/31
- Product number
- E900808
- Product name
- Ethyl5-bromofuran-2-carboxylate
- Packaging
- 250mg
- Price
- $55
- Updated
- 2021/12/16
- Product number
- 44457
- Product name
- Ethyl5-Bromo-2-furancarboxylate,≥97%(GC)
- Purity
- ≥97%(GC)
- Packaging
- 1G
- Price
- $57.5
- Updated
- 2021/12/16
- Product number
- X5330
- Product name
- Ethyl5-bromo-2-furoate
- Packaging
- 5g
- Price
- $231
- Updated
- 2021/12/16
Ethyl 5-broMo-2-furoate, 97+% Chemical Properties,Usage,Production
Synthesis
585-70-6
64-17-5
6132-37-2
To a stirred suspension of 5-bromo-2-furoic acid (15.0 g, 78.54 mmol) in 225 mL of dichloromethane was slowly added oxalyl chloride followed by a catalytic amount of N,N'-dimethylformamide at room temperature. After 1 hour of reaction, ethanol (20 mL) was added followed by triethylamine (22 mL). The reaction was continued with stirring for 15 hours. Upon completion of the reaction, the mixture was concentrated to dryness under reduced pressure to give a residue. Extraction was carried out with excess hexane and hexane-dichloromethane (3:1, v/v) solvent mixture. The organic phases were combined, filtered and the filtrate was concentrated to give a yellow oil. Finally, the product was dried under high vacuum to give ethyl 5-bromofuran-2-carboxylate 17.2 g in 93% yield.
References
[1] Patent: WO2004/11418, 2004, A1. Location in patent: Page 133
[2] Patent: WO2005/68460, 2005, A1. Location in patent: Page/Page column 314-315
[3] Journal of Materials Chemistry A, 2014, vol. 2, # 18, p. 6589 - 6597
[4] Chemical Communications, 2015, vol. 51, # 15, p. 3166 - 3168
[5] Patent: CN106977476, 2017, A. Location in patent: Paragraph 0106-0108
Ethyl 5-broMo-2-furoate, 97+% Preparation Products And Raw materials
Raw materials
Preparation Products
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