9H-Carbazole, 3,6-diiodo-

Product Name: 9H-Carbazole, 3,6-diiodo-
CAS No.: 57103-02-3
Chemical Name: 9H-Carbazole, 3,6-diiodo-
Synonyms: 3,6-Diiodocarbazole;6-diiodo-9H-carbazole;3,6-Diiodocarbazole>3,6-Diiodo-9H-carbazole;9H-Carbazole, 3,6-diiodo-;9H-Carbazole, 3,6-diiodo-, 10 mM in DMSO;Pentamethylcyclopentadienylbis(triphenylphosphine)
CBNumber: CB62605900
Molecular Formula: C12H7I2N
Formula Weight: 419
MOL File: 57103-02-3.mol

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9H-Carbazole, 3,6-diiodo- Property

Melting point:: 205.0 to 209.0 °C
Boiling point:: 498.3±25.0 °C(Predicted)
Density: 2.326±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
form: powder to crystal
pka: 15.68±0.30(Predicted)
color: White to Light yellow to Light orange
InChI: InChI=1S/C12H7I2N/c13-7-1-3-11-9(5-7)10-6-8(14)2-4-12(10)15-11/h1-6,15H
InChIKey: PECAOKZHORDWAI-UHFFFAOYSA-N
SMILES: N1C2=C(C=C(I)C=C2)C2=C1C=CC(I)=C2

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Safety

HS Code: 29339900

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TCI Chemical

Product number: D4548
Product name: 3,6-Diiodocarbazole
Purity: >98.0%(GC)
Packaging: 5g
Price: $111
Updated: 2025/07/31

TCI Chemical

Product number: D4548
Product name: 3,6-Diiodocarbazole
Purity: >98.0%(GC)
Packaging: 25g
Price: $360
Updated: 2025/07/31

TRC

Product number: D493085
Product name: 3,6-Diiodo-9H-carbazole
Packaging: 100mg
Price: $75
Updated: 2021/12/16

Apolloscientific

Product number: OR54455
Product name: 3,6-Diiodo-carbazole
Packaging: 5g
Price: $37
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H31-H-16
Product name: 3,6-Diiodocarbazole
Packaging: 5G
Price: $40
Updated: 2021/12/16

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9H-Carbazole, 3,6-diiodo- Chemical Properties,Usage,Production

Synthesis

86-74-8

57103-02-3

General procedure for the synthesis of 3,6-diiodo-9H-carbazole from carbazole: Carbazole (24 g, 144 mmol) was dissolved in acetic acid (360 mL) and heated to 80 °C. Subsequently, finely ground potassium iodide (31.5 g, 189 mmol) was added to the reaction system and stirred for several minutes. Next, potassium iodate (24 g, 100 mmol) was carefully added in portions and the reaction temperature was maintained at 80 °C until the iodine was completely consumed. After completion of the reaction, the mixture was cooled to 40 °C and the solid product was collected by filtration. It was washed sequentially with acetic acid (30 mL), methanol (100 mL) and water to afford 3,6-diiodo-9H-carbazole (51 g, 90% yield) as a yellow solid. NMR hydrogen spectrum (300MHz, CDCl3, δ): 8.33 (multiple peaks, 2H), 8.15 (multiple peaks, 1H), 7.70-7.60 (multiple peaks, 2H), 7.23-7.20 (multiple peaks, 2H).

References

[1] Chemistry - An Asian Journal, 2010, vol. 5, # 10, p. 2162 - 2167
[2] Patent: US2009/54649, 2009, A1. Location in patent: Page/Page column 34-35
[3] Chemistry - A European Journal, 2015, vol. 21, # 48, p. 17379 - 17390
[4] Journal of Organic Chemistry, 2015, vol. 80, # 4, p. 2392 - 2396
[5] European Journal of Organic Chemistry, 2013, # 29, p. 6619 - 6628

9H-Carbazole, 3,6-diiodo- Preparation Products And Raw materials

Raw materials

Preparation Products

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9H-Carbazole, 3,6-diiodo- Suppliers

Americas 1 CHINA 146 Europe 1 India 2 Japan 1 United Kingdom 1 United States 6 Global 158

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View Lastest Price from 9H-Carbazole, 3,6-diiodo- manufacturers

Shanghai UCHEM Inc.

Product: 3,6-Diiodo-9H-carbazole 57103-02-3
Price: US $36.00-358.00/g
Min. Order: 25g
Purity: 0.98
Supply Ability: 10kg
Release date: 2023-12-07

Henan Fengda Chemical Co., Ltd

Product: 3,6-Diiodo-9H-carbazole 57103-02-3
Price: US $200.00-1.00/KG
Min. Order: 1KG
Purity: 99%, 99.5% Sublimated
Supply Ability: g-kg-tons, free sample is available
Release date: 2023-12-30

LY Global chemicals co.,ltd .

Product: 9H-Carbazole, 3,6-diiodo- 57103-02-3
Price: US $0.00/kg
Min. Order: 1kg
Purity: 95.0%min
Supply Ability: 1000kg
Release date: 2023-03-10

57103-02-3, 9H-Carbazole, 3,6-diiodo-Related Search:

9-Phenyl-9H,9'H-[3,3']bicarbazolyl 3,6-BIS(TERT-BUTYL)CARBAZOLE 3-Bromo-9H-carbazole 3,6-DIPHENYL-9H-CARBAZOLE

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Pentamethylcyclopentadienylbis(triphenylphosphine)

9H-Carbazole, 3,6-diiodo-, 10 mM in DMSO

57103-02-3

C12H7I2N