ChemicalBook > CAS DataBase List > 5-Fluoro-2-nitrobenzadehyde

5-Fluoro-2-nitrobenzadehyde

Product Name
5-Fluoro-2-nitrobenzadehyde
CAS No.
395-81-3
Chemical Name
5-Fluoro-2-nitrobenzadehyde
Synonyms
5-FLUORO-2-NITROBENZALDEHYDE;KML-73;KML-105;uoro-2-nitrobenzaL;5-Fluoro-2-nitrobenzadehyde;2-NITRO-5-FLUOROBENZALDEHYDE;5-Fluoro-2-nitrobenzladehyde;4-Fluoro-2-formylnitrobenzene;4-Chloro-5'-fluorobenzophenone;5-Fluoro-2-nitrobenzaldehyde>
CBNumber
CB6317142
Molecular Formula
C7H4FNO3
Formula Weight
169.11
MOL File
395-81-3.mol
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5-Fluoro-2-nitrobenzadehyde Property

Melting point:
92-94°C
Boiling point:
153°C 23mm
Density 
1.443±0.06 g/cm3(Predicted)
Flash point:
>110°C
storage temp. 
Keep in dark place,Sealed in dry,Room Temperature
Water Solubility 
Insoluble in water
form 
powder to crystal
color 
White to Light red to Green
Sensitive 
Air Sensitive
BRN 
1869010
InChI
InChI=1S/C7H4FNO3/c8-6-1-2-7(9(11)12)5(3-6)4-10/h1-4H
InChIKey
KKAFVHUJZPVWND-UHFFFAOYSA-N
SMILES
C(=O)C1=CC(F)=CC=C1[N+]([O-])=O
CAS DataBase Reference
395-81-3(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi,Xn
Risk Statements 
36/37/38
Safety Statements 
26-36-37
HazardClass 
IRRITANT
HS Code 
29124990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TCI Chemical
Product number
F0645
Product name
5-Fluoro-2-nitrobenzaldehyde
Purity
>98.0%(GC)
Packaging
5g
Price
$46
Updated
2025/07/31
TCI Chemical
Product number
F0645
Product name
5-Fluoro-2-nitrobenzaldehyde
Purity
>98.0%(GC)
Packaging
25g
Price
$169
Updated
2025/07/31
Matrix Scientific
Product number
002191
Product name
5-Fluoro-2-nitrobenzaldehyde
Purity
98%
Packaging
5g
Price
$10
Updated
2021/12/16
AK Scientific
Product number
X3079
Product name
5-Fluoro-2-nitrobenzaldehyde
Packaging
5g
Price
$14
Updated
2021/12/16
Matrix Scientific
Product number
002191
Product name
5-Fluoro-2-nitrobenzaldehyde
Purity
98%
Packaging
25g
Price
$39
Updated
2021/12/16
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5-Fluoro-2-nitrobenzadehyde Chemical Properties,Usage,Production

Chemical Properties

5-Fluoro-2-nitrobenzaldehyde is a very light yellow-light reddish yellow solid at room temperature and pressure, it is easily oxidized to form white benzoic acid products, and needs to be stored at low temperature.

Uses

5-Fluoro-2-nitrobenzaldehyde can be used as an intermediate in pharmaceutical chemistry and organic synthesis, and is used to prepare herbicides, plant growth regulators, etc.

Synthesis

287121-32-8

395-81-3

General procedure for the synthesis of 5-fluoro-2-nitrobenzaldehyde from 5-fluoro-2-nitrobenzyl alcohol: 5-fluoro-2-nitrobenzyl alcohol (13.92 g, 81.08 mmol) was dissolved in dichloromethane (284 mL). To the solution was added 4?molecular sieves (73 g) and pyridinium dichromate (36.58 g, 97.3 mmol). The reaction mixture was stirred at 20 °C for 6 hours. After completion of the reaction, the crude reaction mixture was filtered through a short silica gel column. The filtrate was concentrated under reduced pressure to remove the solvent and the residue was purified by fast column chromatography (silica gel, 10-20% ethyl acetate/hexane as eluent) to afford 9.43 g (69% yield) of the target compound 5-fluoro-2-nitrobenzaldehyde as a colorless oil.1H-NMR (CDCl3) data: δ 10.44 (d, 1H), 8.22 (dd, 1H) , 7.62 (dd, 1H), 7.41 (ddd, 1H).

References

[1] Journal of Medicinal Chemistry, 2004, vol. 47, # 16, p. 3934 - 3937
[2] Patent: WO2003/76442, 2003, A1. Location in patent: Page/Page column 65

5-Fluoro-2-nitrobenzadehyde Preparation Products And Raw materials

Raw materials

Preparation Products

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5-Fluoro-2-nitrobenzadehyde Suppliers

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View Lastest Price from 5-Fluoro-2-nitrobenzadehyde manufacturers

Honest Joy Holdings Limited
Product
5-Fluoro-2-nitrobenzaldehyde 395-81-3
Price
US $0.00/KG
Min. Order
1KG
Purity
99.3%
Supply Ability
100 tons
Release date
2022-02-21
Zhuozhou Wenxi import and Export Co., Ltd
Product
5-Fluoro-2-nitrobenzadehyde 395-81-3
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-07-10
Zhuozhou Wenxi import and Export Co., Ltd
Product
5-Fluoro-2-nitrobenzadehyde 395-81-3
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-07-09

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