2-METHOXY-3,5-DIBROMO-PYRIDINE

Product Name: 2-METHOXY-3,5-DIBROMO-PYRIDINE
CAS No.: 13472-60-1
Chemical Name: 2-METHOXY-3,5-DIBROMO-PYRIDINE
Synonyms: Dopaquinone Monomer;3,5-DIBROMO-2-METHOXYPYRIDINE;2-METHOXY-3,5-DIBROMO-PYRIDINE;3-methyl-5-nitropyridin-3-amine;Pyridine, 3,5-dibroMo-2-Methoxy-;3,5-DibroMo-2-Methoxypyridine;2-METHOXY-5-PICOLINE (2-METHOXY-5-METHYLPYRIDINE);2-METHOXY-3,5-DIBROMO-PYRIDINE ISO 9001：2015 REACH
CBNumber: CB6325909
Molecular Formula: C6H5Br2NO
Formula Weight: 266.92
MOL File: 13472-60-1.mol

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2-METHOXY-3,5-DIBROMO-PYRIDINE Property

Melting point:: 46-51℃
Boiling point:: 235.7±35.0 °C(Predicted)
Density: 1.919±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
solubility: soluble in Methanol
form: powder to crystal
pka: -1.31±0.20(Predicted)
color: White to Orange to Green

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Safety

Hazard Codes: Xi,Xn
Risk Statements: 36/37/38-41-22
Safety Statements: 26-36-45
RIDADR: UN 2811
WGK Germany: 1
Hazard Note: Harmful
HazardClass: IRRITANT
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H302Harmful if swallowed

H318Causes serious eye damage

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 722731
Product name: 3,5-Dibromo-2-methoxypyridine
Purity: 97%
Packaging: 1g
Price: $44
Updated: 2023/06/20

Sigma-Aldrich

Product number: 722731
Product name: 3,5-Dibromo-2-methoxypyridine
Purity: 97%
Packaging: 5g
Price: $116
Updated: 2022/05/15

TCI Chemical

Product number: D5099
Product name: 3,5-Dibromo-2-methoxypyridine
Purity: >98.0%(GC)
Packaging: 1g
Price: $27
Updated: 2025/07/31

TCI Chemical

Product number: D5099
Product name: 3,5-Dibromo-2-methoxypyridine
Purity: >98.0%(GC)
Packaging: 5g
Price: $89
Updated: 2025/07/31

TRC

Product number: D425863
Product name: 3,5-Dibromo-2-methoxypyridine
Packaging: 100mg
Price: $45
Updated: 2021/12/16

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2-METHOXY-3,5-DIBROMO-PYRIDINE Chemical Properties,Usage,Production

Synthesis

13472-85-0

13472-60-1

The general procedure for the synthesis of 2-methoxy-3,5-dibromopyridine from 5-bromo-2-methoxypyridine was as follows: bromine (17.8 g, 111 mmol) was slowly added to a mixed solution containing 5-bromo-2-methoxypyridine (12.0 g, 63.8 mmol), sodium acetate (5.23 g, 63.8 mmol) and acetic acid (65 mL). The reaction mixture was stirred at 80 °C for 4 hours, followed by continued stirring at room temperature for 12 hours. After completion of the reaction, the mixture was diluted with ether and washed sequentially with water, saturated sodium bicarbonate solution and brine. The organic layer was separated, dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure. The crude product was purified by column chromatography with the eluent being a petroleum ether solution of 1-5% ethyl acetate to give 10.6 g of the target product 2-methoxy-3,5-dibromopyridine. The product was characterized by 1H NMR (300 MHz, DMSO-d6) with chemical shifts of 8.20-8.40 (m, 2H) and 3.92 (s, 3H).

References

[1] Patent: US2010/81673, 2010, A1. Location in patent: Page/Page column 14
[2] Patent: US2015/210671, 2015, A1. Location in patent: Paragraph 0173; 0181; 0182
[3] Patent: US9145393, 2015, B2. Location in patent: Page/Page column 37; 38

2-METHOXY-3,5-DIBROMO-PYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-METHOXY-3,5-DIBROMO-PYRIDINE Suppliers

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View Lastest Price from 2-METHOXY-3,5-DIBROMO-PYRIDINE manufacturers

Shaanxi Dideu New Materials Co. Ltd

Product: 2-METHOXY-3,5-DIBROMO-PYRIDINE 13472-60-1
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 98.0%
Supply Ability: 10000KGS
Release date: 2025-05-30

Henan Fengda Chemical Co., Ltd

Product: 2-METHOXY-3,5-DIBROMO-PYRIDINE 13472-60-1
Price: US $5.00-0.10/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: g-kg-tons, free sample is available
Release date: 2024-04-09

Shaanxi Dideu Medichem Co. Ltd

Product: 3,5-Dibromo-2-methoxypyridine 13472-60-1
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 20T
Release date: 2019-12-25

13472-60-1, 2-METHOXY-3,5-DIBROMO-PYRIDINERelated Search:

3-Iodo-2-methoxypyridine 5-BROMO-2-METHOXY-3-CYANOPYRIDINE 2-Methoxy-3-(trifluoromethyl)pyridine 2-Methoxy-5-nitro-3-picoline 6-Chloro-2-methoxy-3-nitropyridine 2-Methoxy-3-fluoro-5-bromopyridine 5-AMINO-2-METHOXY-3-METHYLPYRIDINE HCL 5-BROMO-2-METHOXY-3-NITRO-PYRIDINE 2-Methoxy-3-nitropyridine 5-AMINO-3-BROMO-2-METHOXYPYRIDINE 3-BROMO-5-FLUORO-2-METHOXYPYRIDINE 3-BROMO-2-METHOXY-6-PICOLINE 3-BROMO-5-CHLORO-2-METHOXY-PYRIDINE 3,5-Dibromopyridine 2-METHOXY-5-PICOLINE

3,5-DIBROMO-2-METHOXYPYRIDINE

2-METHOXY-3,5-DIBROMO-PYRIDINE

2-METHOXY-5-PICOLINE (2-METHOXY-5-METHYLPYRIDINE)

Pyridine, 3,5-dibroMo-2-Methoxy-

3,5-<WBR>DibroMo-<WBR>2-<WBR>Methoxypyridine

3-methyl-5-nitropyridin-3-amine

2-METHOXY-3,5-DIBROMO-PYRIDINE ISO 9001：2015 REACH

Dopaquinone Monomer

13472-60-1

Heterocycle-Pyridine series

Pyridine