1-Methylpiperidine-4-carboxylic acid hydrochloride

Product Name: 1-Methylpiperidine-4-carboxylic acid hydrochloride
CAS No.: 71985-80-3
Chemical Name: 1-Methylpiperidine-4-carboxylic acid hydrochloride
Synonyms: BIO-FARMA BF002150;RARECHEM AH CK 0139;TIMTEC-BB SBB003751;Lasmiditan Impurity 45;N-MethylisonipecoticacidHCl;4-CARBOXY-1-METHYL-PIPERIDINE HCL;1-Methyl-piperidine-4-carboxylic a;Methylpiperidincarbonsurehydrochlorid;1-Methyl-4-piperidinecarboxylic acid HCl;1-METHYL-PIPERIDINE-4-CARBOXYLIC ACID HCL
CBNumber: CB6341912
Molecular Formula: C7H14ClNO2
Formula Weight: 179.64
MOL File: 71985-80-3.mol

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1-Methylpiperidine-4-carboxylic acid hydrochloride Property

Melting point:: 226-228°C (dec.)
storage temp.: Inert atmosphere,Room Temperature
form: solid
color: Off-white
InChI: InChI=1S/C7H13NO2.ClH/c1-8-4-2-6(3-5-8)7(9)10;/h6H,2-5H2,1H3,(H,9,10);1H
InChIKey: NLUDEWJJEMHIIL-UHFFFAOYSA-N
SMILES: N1(C)CCC(C(O)=O)CC1.[H]Cl
CAS DataBase Reference: 71985-80-3(CAS DataBase Reference)

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38-20/21/22
Safety Statements: 26-36-24/25-36/37
HazardClass: IRRITANT
HS Code: 29339900

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M320978
Product name: 1-Methylpiperidine-4-carboxylic acid hydrochloride
Packaging: 500mg
Price: $75
Updated: 2021/12/16

Matrix Scientific

Product number: 016314
Product name: 1-Methylpiperidine-4-carboxylic acidhydrochloride
Packaging: 1g
Price: $10
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H21-5-Z0
Product name: 1-Methylpiperidine-4-carboxylic acid hydrochloride
Purity: 98%
Packaging: 1g
Price: $21
Updated: 2021/12/16

ChemScene

Product number: CS-W004085
Product name: 1-Methylpiperidine-4-carboxylic acid hydrochloride
Purity: ≥97.0%
Packaging: 25g
Price: $30
Updated: 2021/12/16

Frontier Specialty Chemicals

Product number: JK118455
Product name: 1-Methylpiperidine-4-carboxylic acid hydrochloride
Purity: 98%
Packaging: 1g
Price: $33
Updated: 2021/12/16

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1-Methylpiperidine-4-carboxylic acid hydrochloride Chemical Properties,Usage,Production

Chemical Properties

Off-white solid

Synthesis

The synthesis method of 1-Methylpiperidine-4-carboxylic acid Hydrochloride is shown below: Charge isonipecotic acid, palladium, and purified water into a reaction vessel. Heat the resulting mixture to 90 to 95° C. Charge formic acid and formaldehyde to the vessel. Cool the resulting mixture to 20 to 30° C. Filter the reaction mixture through GF/F. Wash the filter cake with purified water. Concentrate the combined filtrates to ca 2 vol at atmospheric pressure. Adjust the temperature 65 to 75° C. Charge conc—hydrochloric acid to the vessel. Charge acetonitrile to the vessel at ≧70° C. and concentrate the solution to ca 2 vol at atmospheric pressure. Charge acetonitrile to the vessel. Moreover, concentrate the solution at atmospheric pressure to ca 2 vol. Charge acetonitrile to the vessel. Moreover, concentrate the solution at atmospheric pressure to ca 3 vol. Check the water content by KF analysis of the supernatant liquors using AX reagent. Cool the reaction mixture to 20 to 25° C. Stir the reaction mixture for 1 to 2 hours. Filter the reaction mixture. Wash the filter cake with acetonitrile. Dry the product up to 50° C. until ≦0.5% w/w by LOD and ≦0.2% w/w water.

1-Methylpiperidine-4-carboxylic acid hydrochloride Preparation Products And Raw materials

Raw materials

Formaldehyde Formic acid Chloroform Diethyl ether Hydrochloric acid Isonipecotic acid

Preparation Products

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1-Methylpiperidine-4-carboxylic acid hydrochloride Suppliers

Canada 1 China 129 France 1 Germany 5 India 5 Russia 1 United Kingdom 6 United States 16 Global 164

Alchem Pharmtech,Inc.

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TimTec Corporation

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View Lastest Price from 1-Methylpiperidine-4-carboxylic acid hydrochloride manufacturers

Hangzhou ICH Biofarm Co., Ltd

Product: 1-METHYLPIPERIDINE-4-CARBOXYLIC ACID HYDROCHLORIDE 71985-80-3
Price: US $0.00/kg
Min. Order: 1kg
Purity: 99.0%min
Supply Ability: 10000kg
Release date: 2023-06-09

Career Henan Chemical Co

Product: 1-METHYLPIPERIDINE-4-CARBOXYLIC ACID HYDROCHLORIDE 71985-80-3
Price: US $1.00/KG
Min. Order: 1KG
Purity: ≥98%
Supply Ability: 20 tons
Release date: 2020-01-09

71985-80-3, 1-Methylpiperidine-4-carboxylic acid hydrochlorideRelated Search:

1-METHYL-PIPERIDINE-4-CARBOXYLIC ACID 1-METHYLPIPERIDINE-4-CARBOXYLIC ACID HYDROCHLORIDE 1-METHYLPIPERIDINE-2-CARBOXYLIC ACID HYDROCHLORIDE (S)-1-Methylpiperidine-2-carboxylic acid hydrochloride 1-METHYLPIPERIDINE-2-CARBOXYLIC ACID HYDROCHLORIDE 1-METHYLPIPERIDINE-3-CARBOXYLIC ACID HYDROCHLORIDE (R)-1-Methylpiperidine-2-carboxylic acid hydrochloride

4-CARBOXY-1-METHYL-PIPERIDINE HCL

BIO-FARMA BF002150

1-METHYL-PIPERIDINE-4-CARBOXYLIC ACID HCL

1-METHYLPIPERIDINE-4-CARBOXYLIC ACID HYDROCHLORIDE

1-METHYLPIPERIDINO-4-CARBOXYLIC ACID HYDROCHLORIDE

1-METHYL-4-PIPERIDINECARBOXYLIC ACID HYDROCHLORIDE

TIMTEC-BB SBB003751

RARECHEM AH CK 0139

4-Carboxy-1-methylpiperidine hydrochloride, 1-Methylisonipecotic acid hydrochloride

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4-Piperidinecarboxylic acid, 1-methyl-, hydrochloride (1:1)

Methylpiperidincarbonsurehydrochlorid

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N-MethylisonipecoticacidHCl

1-Methylpiperidine-4-carboxylic acid hydrochloride 98%

1-METHYL-PIPERIDINE-4-CARBOXYLIC ACID X HCL

1-Methylpiperidine-4-carboxylic acid hydrochloride ,98%

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1-Methyl-4-piperidinecarboxylic acid，hydrochloride (1:1)(For export only)

1-Methyl-piperidine-4-carboxylic a

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1-METHYLPIPERIDINE-4-CARBOXYLIC ACID HYDROCHLORIDE

Lasmiditan Impurity 45

71985-80-3

Piperidine