ChemicalBook > CAS DataBase List > Methyl 6-(1H-pyrazol-1-yl)pyridine-3-carboxylate

Methyl 6-(1H-pyrazol-1-yl)pyridine-3-carboxylate

Product Name: Methyl 6-(1H-pyrazol-1-yl)pyridine-3-carboxylate
CAS No.: 321533-62-4
Chemical Name: Methyl 6-(1H-pyrazol-1-yl)pyridine-3-carboxylate
Synonyms: METHYL 6-(1H-PYRAZOL-1-YL)NICOTINATE;6-PYRAZOL-1-YL-NICOTINIC ACID METHYL ESTER;methyl 6-pyrazol-1-ylpyridine-3-carboxylate;6-Pyrazol-1-yl-nicotinic acid methyl ester ,97%;METHYL 6-(1H-PYRAZOL-1-YL)PYRIDINE-3-CARBOXYLATE;Methyl 6-(1H-pyrazol-1-yl)-3-pyridinecarboxylate;6-(1-pyrazolyl)-3-pyridinecarboxylic acid methyl ester;3-Pyridinecarboxylic acid, 6-(1H-pyrazol-1-yl)-, methyl ester
CBNumber: CB6349185
Molecular Formula: C10H9N3O2
Formula Weight: 203.2
MOL File: 321533-62-4.mol

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Methyl 6-(1H-pyrazol-1-yl)pyridine-3-carboxylate Property

Boiling point:: 330.8±27.0 °C(Predicted)
Density: 1.27±0.1 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
pka: -0.42±0.19(Predicted)
Appearance: White to off-white Solid

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Safety

Risk Statements: 20/21/22
Safety Statements: 3/9-36/37
HS Code: 29331990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M593163
Product name: Methyl6-(1H-pyrazol-1-yl)nicotinate
Packaging: 50mg
Price: $60
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0126779
Product name: METHYL 6-(1H-PYRAZOL-1-YL)NICOTINATE
Purity: 95.00%
Packaging: 1MG
Price: $586.97
Updated: 2021/12/16

Matrix Scientific

Product number: 138460
Product name: Methyl 6-(1H-pyrazol-1-yl)nicotinate
Purity: 95%+
Packaging: 5g
Price: $594
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0126779
Product name: METHYL 6-(1H-PYRAZOL-1-YL)NICOTINATE
Purity: 95.00%
Packaging: 10MG
Price: $618.5
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0126779
Product name: METHYL 6-(1H-PYRAZOL-1-YL)NICOTINATE
Purity: 95.00%
Packaging: 5MG
Price: $623.82
Updated: 2021/12/16

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Methyl 6-(1H-pyrazol-1-yl)pyridine-3-carboxylate Chemical Properties,Usage,Production

Chemical Properties

Off-white solid

Synthesis

288-13-1

73781-91-6

321533-62-4

Example 7. Preparation of 0-(6-pyrazol-1-yl-pyridin-3-ylmethyl)-hydroxylamine (compound of Formula (XI)); Step 7a. Preparation of methyl 6-pyrazol-1-yl-nicotinate (compound of Formula (XI-a)); To a solution of pyrazole (19.4 g, 0.28 mol) dissolved in 100 mL of anhydrous DMSO (at temperature 0°C) was added, in one portion, over 30 minutes, a solution of pyrazole (19.4 g, 0.28 mol) dissolved in NaH (7.5 g, 0.3 mol). The reaction mixture was slowly warmed up to room temperature and stirred continuously at that temperature for 30 min. Subsequently, methyl 6-chloronicotinate (35 g, 0.2 mol) was added to the stirring reaction mixture and stirred vigorously for 6 hours. Upon completion of the reaction, the mixture was cooled to about 0 °C and slowly poured into pre-cooled saturated aqueous NH4Cl solution. The precipitate formed was collected by filtration, washed with water and dried to give the compound of formula (XI-a) (38.3 g, 93% yield) as an off-white solid.

References

[1] Patent: WO2005/70918, 2005, A1. Location in patent: Page/Page column 40
[2] Patent: US2008/153812, 2008, A1. Location in patent: Page/Page column 102

Methyl 6-(1H-pyrazol-1-yl)pyridine-3-carboxylate Preparation Products And Raw materials

Raw materials

Sodium hydride Methyl 6-chloronicotinate Pyrazole Dimethyl sulfoxide

Preparation Products

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View Lastest Price from Methyl 6-(1H-pyrazol-1-yl)pyridine-3-carboxylate manufacturers

Career Henan Chemical Co

Product: Methyl 6-(1H-pyrazol-1-yl)pyridine-3-carboxylate 321533-62-4
Price: US $2.00/KG
Min. Order: 1g
Purity: 98%min
Supply Ability: ask
Release date: 2020-01-08

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321533-62-4