3-(BENZYLOXY)-5-BROMOPYRIDINE

Product Name: 3-(BENZYLOXY)-5-BROMOPYRIDINE
CAS No.: 130722-95-1
Chemical Name: 3-(BENZYLOXY)-5-BROMOPYRIDINE
Synonyms: B67304;3-Bromo-5-bezyloxypyridine;5-Benzyloxy-3-broMopyridine;3-(BENZYLOXY)-5-BROMOPYRIDINE;3-Benzyloxy-5-bromopyridine >3-bromo-5-phenylmethoxypyridine;3-(Benzyloxy)-5-bromopyridine ,97%;Pyridine, 3-bromo-5-(phenylmethoxy)-;C12H10BrNO 3-(BENZYLOXY)-5-BROMOPYRIDINE;3-(BENZYLOXY)-5-BROMOPYRIDINE ISO 9001：2015 REACH
CBNumber: CB6406909
Molecular Formula: C12H10BrNO
Formula Weight: 264.12
MOL File: 130722-95-1.mol

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3-(BENZYLOXY)-5-BROMOPYRIDINE Property

Melting point:: 69.0 to 73.0 °C
Boiling point:: 343.7±27.0 °C(Predicted)
Density: 1.438±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
form: powder to crystal
pka: 2.23±0.10(Predicted)
color: White to Light yellow
λmax: 290nm(MeOH)(lit.)
InChI: InChI=1S/C12H10BrNO/c13-11-6-12(8-14-7-11)15-9-10-4-2-1-3-5-10/h1-8H,9H2
InChIKey: YSHKYZAWTWKQKK-UHFFFAOYSA-N
SMILES: C1=NC=C(OCC2=CC=CC=C2)C=C1Br

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Safety

Risk Statements: 36/37/38
Safety Statements: 26-36/37/39
HS Code: 29333990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TCI Chemical

Product number: B4775
Product name: 3-Benzyloxy-5-bromopyridine
Purity: >98.0%(GC)(T)
Packaging: 1g
Price: $71
Updated: 2025/07/31

TCI Chemical

Product number: B4775
Product name: 3-Benzyloxy-5-bromopyridine
Purity: >98.0%(GC)(T)
Packaging: 5g
Price: $243
Updated: 2025/07/31

TRC

Product number: B291590
Product name: 3-(Benzyloxy)-5-bromopyridine
Packaging: 100mg
Price: $75
Updated: 2021/12/16

ChemScene

Product number: CS-W003401
Product name: 3-(Benzyloxy)-5-bromopyridine
Purity: 98.38%
Packaging: 10g
Price: $78
Updated: 2021/12/16

ChemScene

Product number: CS-W003401
Product name: 3-(Benzyloxy)-5-bromopyridine
Purity: 98.38%
Packaging: 5g
Price: $44
Updated: 2021/12/16

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3-(BENZYLOXY)-5-BROMOPYRIDINE Chemical Properties,Usage,Production

Chemical Properties

White solid

Synthesis

625-92-3

100-51-6

130722-95-1

1. benzyl alcohol (4.60 g, 42.6 mmol) was slowly added dropwise to a stirred suspension of sodium hydride (60% mineral oil dispersion, 1.70 g, 42.5 mmol) in dimethylformamide (DMF, 50 mL) under dry conditions. 2. the reaction mixture was heated to 60 °C and stirred at this temperature for 1 h to ensure complete deprotonation. 3. 3,5-dibromopyridine (10.0 g, 42.2 mmol) was dissolved in dimethylformamide (DMF, 20 mL) and this solution was subsequently added to the above reaction mixture. 4. The reaction system was warmed to 80 °C and the reaction was continued with stirring for 2 hours to complete the nucleophilic substitution reaction. 5. Upon completion of the reaction, the reaction mixture was cooled to room temperature and subsequently separated by extraction with ethyl acetate and water. 6. The organic layer was separated and dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give the crude product. 7. The crude product was purified by fast column chromatography to afford the target compound 3-benzyloxy-5-bromopyridine (4.75 g, 43% yield). 8. Mass spectrometry (MS) analysis showed the following: m/z calculated value (M + H) + 265, measured value 265, as expected.

References

[1] Bioorganic and Medicinal Chemistry Letters, 2006, vol. 16, # 12, p. 3150 - 3155
[2] Journal of Medicinal Chemistry, 2012, vol. 55, # 2, p. 717 - 724
[3] Patent: US2013/184313, 2013, A1. Location in patent: Paragraph 1099; 1100
[4] Tetrahedron, 2011, vol. 67, # 26, p. 4767 - 4773
[5] Tetrahedron, 2001, vol. 57, # 20, p. 4447 - 4454

3-(BENZYLOXY)-5-BROMOPYRIDINE Preparation Products And Raw materials

Raw materials

3,5-Dibromopyridine N,N-Dimethylformamide Benzyl alcohol Sodium Dichloromethane

Preparation Products

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3-(BENZYLOXY)-5-BROMOPYRIDINE Suppliers

Americas 1 China 85 Europe 1 France 1 Germany 1 India 4 Japan 1 United Kingdom 1 United States 17 Global 112

Beijing HengPuGao Pharmaceutical Chemistry Technology Co., Ltd.

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J & K SCIENTIFIC LTD.

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View Lastest Price from 3-(BENZYLOXY)-5-BROMOPYRIDINE manufacturers

Shanghai Rlavie Technology Co ltd

Product: 3-Benzyloxy-5-bromopyridine 130722-95-1
Price: US $0.00-0.00/kg
Min. Order: 0.0001kg
Purity: 98%min
Supply Ability: 100kgs/month
Release date: 2022-05-10

Dideu Industries Group Limited

Product: 3-(BENZYLOXY)-5-BROMOPYRIDINE 130722-95-1
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons min
Release date: 2021-08-23

Shaanxi Dideu Medichem Co. Ltd

Product: 3-Benzyloxy-5-Bromo-Pyridine 130722-95-1
Price: US $0.00-0.00/Kg
Min. Order: 1KG
Purity: 99.0%
Supply Ability: 500 MT
Release date: 2020-05-12

130722-95-1, 3-(BENZYLOXY)-5-BROMOPYRIDINERelated Search:

4-(BENZYLOXY)-3-BROMOPYRIDINE 3-(benzyloxy)-2-bromopyridine 2-(BENZYLOXY)-3-BROMOPYRIDINE 2-BENZYLOXY-5-BROMOPYRIDINE 3-Bromo-5-ethoxypyridine 2-Amino-5-bromo-3-benzloxypyridine 3-(BENZYLOXY)-5-BROMOPYRIDINE 3-Bromo-5-methylpyridine 3-Bromo-5-hydroxypyridine 3-Bromo-5-(4-methoxybenzyloxy)pyridine

3-(BENZYLOXY)-5-BROMOPYRIDINE

3-(Benzyloxy)-5-bromopyridine ,97%

B67304

5-Benzyloxy-3-broMopyridine

3-Bromo-5-bezyloxypyridine

C12H10BrNO 3-(BENZYLOXY)-5-BROMOPYRIDINE

3-bromo-5-phenylmethoxypyridine

3-Benzyloxy-5-bromopyridine &gt

Pyridine, 3-bromo-5-(phenylmethoxy)-

3-(BENZYLOXY)-5-BROMOPYRIDINE ISO 9001：2015 REACH

130722-95-1

pharmacetical