2-PHENYLPYRIMIDINE

Product Name: 2-PHENYLPYRIMIDINE
CAS No.: 7431-45-0
Chemical Name: 2-PHENYLPYRIMIDINE
Synonyms: 2-PHENYLPYRIMIDINE;2-Phenylpyrimidine> Pyrimidine, 2-phenyl-
CBNumber: CB6455907
Molecular Formula: C10H8N2
Formula Weight: 156.18
MOL File: 7431-45-0.mol

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2-PHENYLPYRIMIDINE Property

Melting point:: 37.0 to 41.0 °C
Boiling point:: 100°C/5mmHg(lit.)
Density: 1.106±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
form: powder to lump
pka: 1.00±0.13(Predicted)
color: White to Almost white

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Safety

Hazard Codes: Xi
Risk Statements: 41
Safety Statements: 26-39
HazardClass: IRRITANT
HS Code: 2933599590

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TCI Chemical

Product number: P1945
Product name: 2-Phenylpyrimidine
Purity: >98.0%(GC)
Packaging: 1g
Price: $702
Updated: 2023/06/20

TCI Chemical

Product number: P1945
Product name: 2-Phenylpyrimidine
Purity: >98.0%(GC)
Packaging: 200mg
Price: $183
Updated: 2024/03/01

TRC

Product number: B522673
Product name: 2-phenylpyrimidine
Packaging: 100mg
Price: $65
Updated: 2021/12/16

Matrix Scientific

Product number: 009803
Product name: 2-Phenylpyrimidine
Purity: 99%
Packaging: 250mg
Price: $150
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H32-1-H4
Product name: 2-Phenylpyrimidine
Packaging: 250mg
Price: $151
Updated: 2021/12/16

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2-PHENYLPYRIMIDINE Chemical Properties,Usage,Production

Synthesis Reference(s)

Tetrahedron, 48, p. 8117, 1992 DOI: 10.1016/S0040-4020(01)80481-6

Synthesis

1722-12-9

98-80-6

7431-45-0

General procedure for the synthesis of 2-phenylpyrimidine from 2-chloropyrimidine and phenylboronic acid: 2-chloropyrimidine (0.50 g, 4.37 mmol), phenylboronic acid (0.69 g, 5.68 mmol), sodium carbonate (Na2CO3, 0.92 g, 8.70 mmol), palladium dichloride (PdCl2, 38.7 mg, 0.22 mmol) and 1,4-bis(diphenylphosphino)butane (dppb, 92.9 mg, 0.22 mmol). The air in the reaction system was displaced with nitrogen for 10 min, followed by the addition of a predegassed solvent mixture of toluene (12 mL), water (6 mL) and ethanol (2 mL). The reaction mixture was stirred at 100 °C for 20 hours. Upon completion of the reaction, the mixture was filtered through a pad of diatomaceous earth and the filtrate was concentrated under reduced pressure to remove the volatile solvent. The crude product was purified by silica gel column chromatography with the eluent being a solvent mixture of 10% ether/dichloromethane, resulting in a white solid product in 65% yield. The spectral data of the product were in agreement with those reported in the literature.

References

[1] European Journal of Organic Chemistry, 2010, # 23, p. 4376 - 4380
[2] Chemical Communications, 2014, vol. 50, # 91, p. 14129 - 14132
[3] Organic and Biomolecular Chemistry, 2013, vol. 11, # 17, p. 2756 - 2760
[4] European Journal of Organic Chemistry, 2012, # 31, p. 6248 - 6259,12
[5] European Journal of Organic Chemistry, 2012, # 31, p. 6248 - 6259

2-PHENYLPYRIMIDINE Preparation Products And Raw materials

Raw materials

Benzamidine hydrochloride 1,1,3,3-Tetramethoxypropane

Preparation Products

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2-PHENYLPYRIMIDINE Suppliers

China 49 Germany 1 India 3 Japan 1 United Kingdom 2 United States 11 Global 67

J & K SCIENTIFIC LTD.

Tel: 18210857532; 18210857532
Fax: 86-10-82849933
Email: jkinfo@jkchemical.com
Country: China
ProdList: 96815
Advantage: 76

TCI (Shanghai) Development Co., Ltd.

Tel: 021-67121386
Fax: 021-67121385
Email: Sales-CN@TCIchemicals.com
Country: China
ProdList: 24529
Advantage: 81

Tetranov Biopharm

Tel: 13526569071
Email: sales@leadmedpharm.com
Country: China
ProdList: 7892
Advantage: 64

Shanghai Hanhong Scientific Co.,Ltd.

Tel: 021-54306202 13764082696
Email: info@hanhongsci.com
Country: China
ProdList: 42934
Advantage: 64

TOKYO CHEMICAL INDUSTRY CO., LTD.

Tel: 03-36680489
Fax: 03-3668-0520
Email: Sales-JP@TCIchemicals.com
Country: Japan
ProdList: 28387
Advantage: 80

9ding chemical ( Shanghai) Limited

Tel: 4009209199
Fax: 86-021-52271987
Email: sales@9dingchem.com
Country: China
ProdList: 22514
Advantage: 55

Clearsynth Labs Limited

Tel: +91-22-26355700
Fax: +91-22-26355701
Email: info@clearsynth.com
Country: India
ProdList: 9679
Advantage: 58

Bide Pharmatech Ltd.

Tel: 400-164-7117 13681763483
Fax: +86-21-61629029
Email: product02@bidepharm.com
Country: China
ProdList: 42446
Advantage: 60

Shanghai KaiYuLin pharmaceutical technology co., LTD

Tel: 021-18721936-595 18721936595
Fax: -
Email: shkylpharma@126.com
Country: China
ProdList: 734
Advantage: 55

Chengdu Research Accelerators Technology Co., Ltd.

Tel: 028-64353063
Fax: 028-64353063 QQ:784253935
Email: reacchemical@163.com
Country: China
ProdList: 5253
Advantage: 58

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View Lastest Price from 2-PHENYLPYRIMIDINE manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 2-Phenyl-pyrimidine 7431-45-0
Price: US $3652.00/KG
Min. Order: 1KG
Purity: 98.0%
Supply Ability: 1T
Release date: 2020-06-19

Henan Fengda Chemical Co., Ltd

Product: 2-Phenylpyrimidine 7431-45-0
Price: US $188.00-1.00/KG
Min. Order: 1KG
Purity: 99%, 99.5% Sublimated
Supply Ability: g-kg-tons, free sample is available
Release date: 2024-01-05

Career Henan Chemical Co

Product: Pyrimidine, 2-phenyl- 7431-45-0
Price: US $1.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 200kgs
Release date: 2020-01-09

7431-45-0, 2-PHENYLPYRIMIDINERelated Search:

4-CHLORO-2-PHENYLQUINAZOLINE 2-PHENYL-4-[3H]QUINAZOLINONE 6-(Chloromethyl)-2-phenylpyrimidin-4-ol 6-HYDROXY-2-MERCAPTO-4-PHENYLPYRIMIDINE 2-CHLORO-4-PHENYLPYRIMIDINE-5-CARBONYL CHLORIDE 2-mercapto-4-phenylpyrimidin 5-ETHYL-5-PHENYLPYRIMIDINE-2,4,6-TRIONE 2-HYDROXY-4-PHENYLPYRIMIDINE-5-CARBOXYLIC ACID ETHYL 2-CHLORO-4-PHENYLPYRIMIDINE-5-CARBOXYLATE ETHYL 2-HYDROXY-4-PHENYLPYRIMIDINE-5-CARBOXYLATE 6-phenylpyrimidin 5-Ethylhexahydro-4,6-dioxo-5-phenylpyrimidine,5-Ethylhexahydro-5-phenylpyrimidine-4,6-dione 4-CHLORO-6-(METHYLSULFANYL)-2-PHENYL-5-PYRIMIDINECARBONITRILE 2-(4-CYANOPHENYL)-5-N-PENTYLPYRIMIDINE 4-HYDROXY-2-(2-HYDROXYPHENYL)-QUINAZOLINE 4-AMINO-2-(4-METHYLPHENYL)-6-(METHYLTHIO)PYRIMIDINE-5-CARBONITRILE 4-CHLORO-2,6-DIPHENYL-5-PYRIMIDINECARBONITRILE 4,6-dimethoxy-5-nitro-2-phenylpyrimidine

Pyrimidine, 2-phenyl-

2-PHENYLPYRIMIDINE

2-Phenylpyrimidine&gt

7431-45-0

Building Blocks

Pyrimidine