ChemicalBook > CAS DataBase List > 4-PYRIDIN-3-YL-BENZOIC ACID

4-PYRIDIN-3-YL-BENZOIC ACID

Product Name
4-PYRIDIN-3-YL-BENZOIC ACID
CAS No.
4385-75-5
Chemical Name
4-PYRIDIN-3-YL-BENZOIC ACID
Synonyms
AKOS BAR-0406;4-PYRID-3-YLBENZOIC ACID;4-pyridin-3-ylbenzoicaci;4-(3-PYRIDYL)BENZOIC ACID;4-(3'-Pyridyl)benzoic Acid;4-PYRIDIN-3-YL-BENZOIC ACID;4-(3-PYRIDINYL)BENZOIC ACID;4-pyridine-3-yl-benzoic acid;4-Pyridin-3-ylbenzoicacid97%;4-Pyridin-3-yl-benzoicacid95%
CBNumber
CB6496269
Molecular Formula
C12H9NO2
Formula Weight
199.21
MOL File
4385-75-5.mol
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4-PYRIDIN-3-YL-BENZOIC ACID Property

Melting point:
271-274
Boiling point:
398.8±25.0 °C(Predicted)
Density 
1.241±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
form 
solid
pka
3.65±0.10(Predicted)
color 
White
InChI
InChI=1S/C12H9NO2/c14-12(15)10-5-3-9(4-6-10)11-2-1-7-13-8-11/h1-8H,(H,14,15)
InChIKey
GYUKEVKPDRXPAB-UHFFFAOYSA-N
SMILES
C(O)(=O)C1=CC=C(C2=CC=CN=C2)C=C1
CAS DataBase Reference
4385-75-5(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi
Hazard Note 
Harmful
HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
P992578
Product name
4-(3''-Pyridyl)benzoicAcid
Packaging
100mg
Price
$75
Updated
2021/12/16
Matrix Scientific
Product number
007710
Product name
4-(3-Pyridinyl)benzoic acid
Purity
97%
Packaging
500mg
Price
$30
Updated
2021/12/16
ChemScene
Product number
CS-0036181
Product name
4-Pyridin-3-ylbenzoicacid
Packaging
1g
Price
$70
Updated
2021/12/16
AK Scientific
Product number
W6300
Product name
4-Pyridin-3-yl-benzoicacid
Packaging
5g
Price
$111
Updated
2021/12/16
ChemScene
Product number
CS-0036181
Product name
4-Pyridin-3-ylbenzoicacid
Packaging
5g
Price
$122
Updated
2021/12/16
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4-PYRIDIN-3-YL-BENZOIC ACID Chemical Properties,Usage,Production

Definition

ChEBI: 4-Pyrid-3-ylbenzoic acid is a phenylpyridine.

Synthesis

626-55-1

14047-29-1

4385-75-5

Example 157 Synthesis of 4-(pyridin-3-yl)benzoic acid: in a mixed solvent of acetonitrile (40 mL) and water (40 mL), 4-carboxyphenylboronic acid (1.66 g, 10 mmol), 3-bromopyridine (1.72 g, 11 mmol), potassium carbonate (5.5 g, 40 mmol), and bis(triphenylphosphine)palladium(II) chloride (400 mg. 0.37 mmol). The reaction mixture was degassed and displaced three times with nitrogen. Subsequently, the mixture was stirred under reflux conditions for 24 hours. Upon completion of the reaction, the reaction suspension was filtered while hot and the filtrate was concentrated to half of the original volume. The concentrated aqueous phase was washed with dichloromethane. The aqueous phase was adjusted to pH=3 with 1 M hydrochloric acid, the solid was precipitated, filtered and the solid was washed with water. Finally, the resulting solid was dried under vacuum to give 1.7 g of white solid 4-(pyridin-3-yl)benzoic acid in 85% yield.LC-MS (ESI) m/z: 200 (M+1)+.

References

[1] Patent: US2009/197863, 2009, A1. Location in patent: Page/Page column 73-74
[2] Archiv der Pharmazie, 2008, vol. 341, # 8, p. 478 - 484
[3] Synlett, 2000, # 6, p. 829 - 831
[4] Patent: US6399656, 2002, B1
[5] European Journal of Medicinal Chemistry, 2015, vol. 101, p. 780 - 789

4-PYRIDIN-3-YL-BENZOIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 4-PYRIDIN-3-YL-BENZOIC ACID manufacturers

Career Henan Chemical Co
Product
4-PYRIDIN-3-YL-BENZOIC ACID 4385-75-5
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
1ton
Release date
2019-07-11

4385-75-5, 4-PYRIDIN-3-YL-BENZOIC ACIDRelated Search:

4-(5-Methyl-2-pyridinyl)benzoic acid 4-PYRIDIN-3-YL-BENZOIC ACID 4-(6-(Trifluoromethyl)pyridin-2-yl)benzoic acid 4-Pyrid-4-ylbenzoic acid 1-(4-Trifluoromethylphenyl)piperidin-4-ol 3-(6-Bromopyridin-2-yl)benzoic acid 4-(4,4-DIMETHYL-PIPERIDIN-1-YL)-BENZOIC ACID 3-(5-NITROPYRIDIN-2-YL)BENZOIC ACID 3-PYRIDIN-2-YL-BENZOIC ACID, 95+% 4-(2-Pyridyl)benzoic acid 3-Pyridin-3-yl-benzoic acid ,97% 4-(3-QUINOLINYL)BENZOIC ACID METHYL 4-(3-PYRIDINYL)BENZOATE METHYL 4-(6-METHOXY-3-PYRIDINYL)BENZOATE 4-(6-AMINO-PYRIDIN-3-YL)-BENZOIC ACID 4-(4-(Methoxycarbonyl)pyridin-3-yl)benzoic acid,4-(6-(Methoxycarbonyl)pyridin-3-yl)benzoic acid,4-(5-(Methoxycarbonyl)pyridin-3-yl)benzoic acid 3-(6-(Methoxycarbonyl)pyridin-3-yl)benzoic acid,3-(5-(Methoxycarbonyl)pyridin-3-yl)benzoic acid 4-[3-[2-(Dimethylamino-d6)-2-oxoethyl]-6-methylimidazo[1,2-a]pyridin-2-yl]benzoic Acid

  • AKOS BAR-0406
  • 4-(3-PYRIDINYL)BENZOIC ACID
  • 4-(3-PYRIDYL)BENZOIC ACID
  • 4-PYRIDIN-3-YL-BENZOIC ACID
  • 4-PYRID-3-YLBENZOIC ACID
  • 4-Pyridin-3-yl-benzoicacid95%
  • 4-Pyridin-3-ylbenzoic acid 97%
  • 4-(2-Chloropyridin-3-yl)benzoic acid
  • 4-(2-Fluoropyridin-3-yl)benzoic acid
  • 4-(5-Fluoropyridin-3-yl)benzoic acid
  • 4-(6-Fluoropyridin-3-yl)benzoic acid
  • 4-pyridine-3-yl-benzoic acid
  • Benzoic acid, 4-(3-pyridinyl)-
  • 4-Pyridin-3-ylbenzoicacid97%
  • 4-(pyridin-3-yl)benzoic acid hydrochloride
  • 4-(3'-Pyridyl)benzoic Acid
  • 4-pyridin-3-ylbenzoicaci
  • 4385-75-5
  • Building Blocks
  • Carboxy
  • Pyridine
  • pharmacetical
  • API intermediates