2-BROMO-4-METHOXYPHENOL

Product Name: 2-BROMO-4-METHOXYPHENOL
CAS No.: 17332-12-6
Chemical Name: 2-BROMO-4-METHOXYPHENOL
Synonyms: 2-BROMO-4-METHOXYPHENOL;Phenol, 3-bromo-4-methoxy-;3-Bromo-4-methoxyphenol 98%
CBNumber: CB6717618
Molecular Formula: C7H7BrO2
Formula Weight: 203.03
MOL File: 17332-12-6.mol

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2-BROMO-4-METHOXYPHENOL Property

Melting point:: 47°
Boiling point:: 281.1±20.0 °C(Predicted)
Density: 1.585±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
pka: 9.49±0.18(Predicted)
Appearance: Light brown to black Solid
InChI: InChI=1S/C7H7BrO2/c1-10-7-3-2-5(9)4-6(7)8/h2-4,9H,1H3
InChIKey: NOJOUQQJSGRBMN-UHFFFAOYSA-N
SMILES: C1(O)=CC=C(OC)C(Br)=C1
CAS DataBase Reference: 17332-12-6(CAS DataBase Reference)

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Safety

HazardClass: IRRITANT
HS Code: 2909500090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B683810
Product name: 3-Bromo-4-Methoxyphenol
Packaging: 1g
Price: $60
Updated: 2021/12/16

TRC

Product number: B683810
Product name: 3-Bromo-4-Methoxyphenol
Packaging: 2.5g
Price: $85
Updated: 2021/12/16

TRC

Product number: B683810
Product name: 3-Bromo-4-Methoxyphenol
Packaging: 5g
Price: $140
Updated: 2021/12/16

Matrix Scientific

Product number: 072744
Product name: 3-Bromo-4-methoxyphenol
Purity: 95+%
Packaging: 1g
Price: $51
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB139866
Product name: 3-Bromo-4-methoxyphenol
Packaging: 1g
Price: $100
Updated: 2021/12/16

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2-BROMO-4-METHOXYPHENOL Chemical Properties,Usage,Production

Uses

3-Bromo-4-methoxyphenol is a malate dehyrogenase inhibitor.

Synthesis

124764-37-0

17332-12-6

General procedure for the synthesis of 3-bromo-4-methoxyphenol from 3-bromo-4-methoxyphenyl acetate: a solution of potassium hydroxide (290 mg, 5.19 mmol) in water (2.5 mL) was added to a solution of 3-bromo-4-methoxyphenyl acetate (1.2 g, 4.9 mmol) in methanol (18.5 mL). The reaction mixture was stirred at room temperature for 30 min, followed by removal of the solvent under reduced pressure. Water (40 mL) was added to the residue and 1.2 M aqueous hydrochloric acid (4.3 mL) was added dropwise until the mixture was acidic. The mixture was extracted with dichloromethane (2 x 40 mL), the organic phases were combined and dried over anhydrous sodium sulfate. After filtration, the filtrate was evaporated under reduced pressure to give 3-bromo-4-methoxyphenol (976 mg, 98% yield) as a light yellow solid.LCMS analysis (Method A): retention time (RT) = 2.11 min; no ionization was observed.TLC analysis: Rf = 0.28 (unfolding reagent ratio 1:4 ethyl acetate:hexane).

References

[1] Patent: WO2009/109743, 2009, A1. Location in patent: Page/Page column 37; 38
[2] Patent: CN105001107, 2016, B. Location in patent: Paragraph 0045; 0047
[3] Patent: WO2004/16621, 2004, A1. Location in patent: Page 31

2-BROMO-4-METHOXYPHENOL Preparation Products And Raw materials

Raw materials

Preparation Products

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2-BROMO-4-METHOXYPHENOL Suppliers

China 105 France 1 Germany 2 India 1 United Kingdom 4 United States 26 Global 139

Sichuan Lancent Medical Devices Co., Ltd.

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View Lastest Price from 2-BROMO-4-METHOXYPHENOL manufacturers

Hebei Chuanghai Biotechnology Co., Ltd

Product: 2-BROMO-4-METHOXYPHENOL 17332-12-6
Price: US $10.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 10 mt
Release date: 2024-11-05

Henan Bao Enluo International TradeCo.，LTD

Product: 2-BROMO-4-METHOXYPHENOL 17332-12-6
Price: US $50.00/kg
Min. Order: 1kg
Purity: 99.9%
Supply Ability: 10000MT
Release date: 2023-08-02

Honest Joy Holdings Limited

Product: 3-Bromo-4-methoxyphenol 17332-12-6
Price: US $0.00/KG
Min. Order: 1KG
Purity: 98.5%
Supply Ability: 100 tons
Release date: 2022-01-17

17332-12-6, 2-BROMO-4-METHOXYPHENOLRelated Search:

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2-BROMO-4-METHOXYPHENOL

3-Bromo-4-methoxyphenol 98%

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