Methyl 2-acetylamino-3-chloropropionate
- Product Name
- Methyl 2-acetylamino-3-chloropropionate
- CAS No.
- 18635-38-6
- Chemical Name
- Methyl 2-acetylamino-3-chloropropionate
- Synonyms
- Nsc146379;Ac-L-Ala(Cl)-OMe;Ac-DL-Ala(Cl)-Ome;Ac-β-chloro-Ala-OMe;Methyl 2-acetylamino;Ac-beta-chloro-Ala-OMe;2-acetylamino-3-chloropropionate;MethylN-acetyl-3-chloropropionate;Methyl2-acetylamino-3-chloropropanoate;METHYL 2-ACETYLAMINO-3-CHLOROPROPIONATE
- CBNumber
- CB6736495
- Molecular Formula
- C6H10ClNO3
- Formula Weight
- 179.6
- MOL File
- 18635-38-6.mol
Methyl 2-acetylamino-3-chloropropionate Property
- Melting point:
- 74-76°C
- Boiling point:
- 303.6±27.0 °C(Predicted)
- Density
- 1?+-.0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C
- solubility
- Dichloromethane, Ethyl Acetate, Methanol
- pka
- 14.01±0.46(Predicted)
- form
- Solid
- color
- White
- InChI
- InChI=1S/C6H10ClNO3/c1-4(9)8-5(3-7)6(10)11-2/h5H,3H2,1-2H3,(H,8,9)/t5-/m0/s1
- InChIKey
- IGKDMFMKAAPDDN-YFKPBYRVSA-N
- SMILES
- C(OC)(=O)[C@H](CCl)NC(C)=O
- CAS DataBase Reference
- 18635-38-6(CAS DataBase Reference)
N-Bromosuccinimide Price
- Product number
- A172038
- Product name
- L-N-Acetyl-β-chloroalanineMethylEster
- Packaging
- 50mg
- Price
- $155
- Updated
- 2021/12/16
- Product number
- R760
- Product name
- Methyl2-acetylamino-3-chloropropionate
- Packaging
- 5g
- Price
- $198.5
- Updated
- 2021/12/16
- Product number
- AS44061
- Product name
- N-Acetyl-3-chloro-DL-alanine methyl ester
- Purity
- 95%
- Packaging
- 1g
- Price
- $34
- Updated
- 2021/12/16
- Product number
- AS44061
- Product name
- N-Acetyl-3-chloro-DL-alanine methyl ester
- Purity
- 95%
- Packaging
- 5G
- Price
- $90
- Updated
- 2021/12/16
- Product number
- HCH0036716
- Product name
- METHYL 2-ACETYLAMINO-3-CHLOROPROPIONATE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $619.7
- Updated
- 2021/12/16
Methyl 2-acetylamino-3-chloropropionate Chemical Properties,Usage,Production
Chemical Properties
White Solid
Synthesis
32345-44-1
108-24-7
18635-38-6
30 g of (R)-methyl 2-amino-3-chloropropionate was suspended in 400 mL of diethyl ether and cooled to 0-5°C. 20 mL of ethanoic anhydride was slowly added dropwise with stirring, maintaining the reaction temperature at 0-5°C, and stirring was continued for 40 minutes after completion of the dropwise addition. Subsequently, the reaction mixture was slowly warmed to 15-25°C and stirring was continued for 1-2 hours. Upon completion of the reaction, the precipitated solid product was collected by filtration and washed with cold diethyl ether. The resulting solid was dried under vacuum to afford 33.3 g of methyl (R)-2-acetamido-3-chloropropionate in 85% yield.
References
[1] Patent: CN104710324, 2016, B. Location in patent: Paragraph 0075; 0076
Methyl 2-acetylamino-3-chloropropionate Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from Methyl 2-acetylamino-3-chloropropionate manufacturers
- Product
- Methyl 2-acetylamino-3-chloropropionate 18635-38-6
- Price
- US $0.00/G/KG
- Min. Order
- 1G/KG
- Purity
- 99%
- Supply Ability
- 100MT
- Release date
- 2025-04-23
- Product
- Methyl 2-acetylamino-3-chloropropionate 18635-38-6
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1ton
- Release date
- 2022-10-12
- Product
- Methyl 2-acetylamino-3-chloropropionate 18635-38-6
- Price
- US $5.00-0.10/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2024-04-16