(1-METHYL-1H-IMIDAZOL-5-YL)METHANOL

Product Name: (1-METHYL-1H-IMIDAZOL-5-YL)METHANOL
CAS No.: 38993-84-9
Chemical Name: (1-METHYL-1H-IMIDAZOL-5-YL)METHANOL
Synonyms: RARECHEM AL BD 0940;1-Methyl-5-imidazolemethanol;1-Methyl-1H-imidazol-5-methanol;(3-methylimidazol-4-yl)methanol;1-Methyl-1H-imidazole-5-methanol;1H-Imidazole-5-methanol,1-methyl-;1-METHYL-5-(HYDROXYMETHYL)IMIDAZOLE;(1-METHYL-1H-IMIDAZOL-5-YL)METHANOL;5-(HydroxyMethyl)-1-MethyliMidazole;(3-METHYL-3H-IMIDAZOL-4-YL)-METHANOL
CBNumber: CB6775364
Molecular Formula: C5H8N2O
Formula Weight: 112.13
MOL File: 38993-84-9.mol

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(1-METHYL-1H-IMIDAZOL-5-YL)METHANOL Property

Melting point:: 113 °C
Boiling point:: 324.9±17.0 °C(Predicted)
Density: 1.16±0.1 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
solubility: DMSO (Sparingly), Methanol (Slightly)
form: Solid
pka: 14.35±0.10(Predicted)
color: Pale Yellow

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Safety

Hazard Codes: Xi,Xn
Risk Statements: 36/37/38-22
Safety Statements: 26-36/37/39-37/39-36
HazardClass: IRRITANT
HS Code: 2933299090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M321303
Product name: (1-Methyl-1H-imidazol-5-yl)methanol
Packaging: 50mg
Price: $45
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H01-1-M8
Product name: 5-(Hydroxymethyl)-1-methyl-1H-imidazole
Packaging: 250mg
Price: $35
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H01-1-M8
Product name: 5-(Hydroxymethyl)-1-methyl-1H-imidazole
Packaging: 1g
Price: $105
Updated: 2021/12/16

Matrix Scientific

Product number: 057545
Product name: (1-Methyl-1H-imidazol-5-yl)methanol
Purity: 95%
Packaging: 1g
Price: $132
Updated: 2021/12/16

Apolloscientific

Product number: OR10499
Product name: 5-(Hydroxymethyl)-1-methyl-1H-imidazole
Packaging: 1g
Price: $143
Updated: 2021/12/16

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(1-METHYL-1H-IMIDAZOL-5-YL)METHANOL Chemical Properties,Usage,Production

Synthesis

39021-62-0

38993-84-9

General procedure for the synthesis of 1-methyl-1H-imidazol-5-yl)methanol from 1-methyl-1H-5-formyl-imidazole: 1-methyl-1H-5-formyl-imidazole (4.0 g, 15 mmol) was suspended in tetrahydrofuran (THF) (10 mL) and the resulting solution was cooled to 0 °C. Lithium aluminum hydride (300 mg, 32.0 mmol) was added in batches over 10 min and the resulting suspension was continued to be stirred for 10 min. Under vigorous stirring, the excess hydride was quenched by bulk addition of solid Na2SO4-10H2O (~1 g). Additional THF was added as needed to prevent the slurry from solidifying. The resulting suspension was continued to be stirred for 1 h. Subsequent filtration to remove the sulfate and solvent removal under reduced pressure afforded the target alcohol (1.3 g, 80% yield).1H NMR (400 MHz, CD3OD): δ 7.57 (s, 1H), 6.89 (s, 1H), 4.58 (s, 2H), 3.72 (s, 3H).13C NMR (100 MHz. CD3OD): δ140.1,132.7,128.1,31.9,31.0.

References

[1] Journal of Medicinal Chemistry, 2006, vol. 49, # 19, p. 5710 - 5727
[2] Patent: WO2006/102159, 2006, A2. Location in patent: Page/Page column 22
[3] Journal of the American Chemical Society, 1949, vol. 71, p. 2444,2447

(1-METHYL-1H-IMIDAZOL-5-YL)METHANOL Preparation Products And Raw materials

Raw materials

Preparation Products

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(1-METHYL-1H-IMIDAZOL-5-YL)METHANOL Suppliers

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View Lastest Price from (1-METHYL-1H-IMIDAZOL-5-YL)METHANOL manufacturers

Career Henan Chemical Co

Product: (1-METHYL-1H-IMIDAZOL-5-YL)METHANOL 38993-84-9
Price: US $9.80/KG
Min. Order: 1g
Purity: ≥99.0%
Supply Ability: 100kg
Release date: 2020-01-02

38993-84-9, (1-METHYL-1H-IMIDAZOL-5-YL)METHANOLRelated Search:

METHYL 1-METHYL-2-SULFANYL-1H-IMIDAZOLE-5-CARBOXYLATE ETHYL 2,7-DIMETHYLIMIDAZO[1,2-A]PYRIDINE-3-CARBOXYLATE 2-METHYL-IMIDAZO[1,2-A]PYRIDINE-3-CARBOXYLIC ACID ETHYL ESTER 1-(2-CYANOETHYL)-2-PHENYL-4,5-DI-CYANOETHOXYMETHYL IMIDAZOLE (2-Butyl-4-Chloro-1-((2'-(1-Trityl-1h-Tetrazole-5-Yl)Biphenyl-4-Yl)Methyl)-1h-Imidazol-5-Yl)Methanol (1-METHYL-1H-IMIDAZOL-2-YL)METHANOL (2-Butyl-4-chloro-1-((2'-(1-trityl-1H-tetrazol-5-yl)biphenyl-4-yl)methyl)-1H-imidazol-5-yl)methanol (5-METHYL-1H-IMIDAZOL-4-YL)METHANOL HYDROCHLORIDE,(4-METHYL-1H-IMIDAZOL-5-YL)METHANOL HYDROCHLORIDE (1-METHYL-1H-IMIDAZOL-4-YL)METHANOL (2-[(4-FLUOROBENZYL)SULFANYL]-1-METHYL-1H-IMIDAZOL-5-YL)METHANOL (2-([3-CHLORO-5-(TRIFLUOROMETHYL)-2-PYRIDINYL]SULFANYL)-1-METHYL-1H-IMIDAZOL-5-YL)METHANOL ETHYL 6-METHYL-2-PHENYLIMIDAZO[1,2-A]PYRIDINE-3-CARBOXYLATE (2-MERCAPTO-1-METHYL-1H-IMIDAZOL-5-YL)METHANOL ETHYL 7-METHYL-2-PHENYLIMIDAZO[1,2-A]PYRIDINE-3-CARBOXYLATE ETHYL 6-CHLORO-2-PHENYLIMIDAZO[1,2-A]PYRIDINE-3-CARBOXYLATE 2,7-DIMETHYLPYRIDO[1,6-A]-1H-IMIDAZOLE-3-CARBOXYLIC ACID, ETHYL ESTER (2-[(2,6-DICHLOROBENZYL)SULFANYL]-1-METHYL-1H-IMIDAZOL-5-YL)METHANOL ETHYL 8-METHYL-2-PHENYLIMIDAZO[1,2-A]PYRIDINE-3-CARBOXYLATE

RARECHEM AL BD 0940

(3-METHYL-3H-IMIDAZOL-4-YL)-METHANOL

5-HYDROXYMETHYL-1-METHYL-1H-IMIDAZOLE

(1-METHYL-1H-IMIDAZOL-5-YL)METHANOL

1-METHYL-5-(HYDROXYMETHYL)IMIDAZOLE

(3-methylimidazol-4-yl)methanol

1H-Imidazole-5-methanol,1-methyl-

5-(HydroxyMethyl)-1-MethyliMidazole

1-Methyl-1H-imidazole-5-methanol

1-Methyl-5-imidazolemethanol

1-Methyl-1H-imidazol-5-methanol

38993-84-9

blocks

Imidazoles

Imidazol&Benzimidazole