ChemicalBook > CAS DataBase List > 2-Amino-3-methoxypyridine

2-Amino-3-methoxypyridine

Product Name: 2-Amino-3-methoxypyridine
CAS No.: 10201-71-5
Chemical Name: 2-Amino-3-methoxypyridine
Synonyms: 3-Methoxy-2-PyridinaMine;3-Methoxypyridin-2-amine;2-Amino-3-methoxypyridine;3-Methoxy-2-aMinopyridine;2-PyridinaMine, 3-Methoxy-;2-Amino-3-methoxypyridine, >=98%;2-Amino-3-methoxypyridine ISO 9001：2015 REACH
CBNumber: CB6967323
Molecular Formula: C6H8N2O
Formula Weight: 124.14
MOL File: 10201-71-5.mol

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2-Amino-3-methoxypyridine Property

Boiling point:: 235.0±20.0 °C(Predicted)
Density: 1.139±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 8.43±0.10(Predicted)
form: solid
color: Dark brown

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Safety

Hazard Codes: Xn
Risk Statements: 22
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: A634710
Product name: 2-Amino-3-methoxypyridine
Packaging: 500mg
Price: $60
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H30-1-01
Product name: 2-Amino-3-methoxypyridine
Purity: 97%
Packaging: 250mg
Price: $30
Updated: 2021/12/16

AK Scientific

Product number: X8586
Product name: 2-Amino-3-methoxypyridine
Packaging: 1g
Price: $39
Updated: 2021/12/16

Matrix Scientific

Product number: 072687
Product name: 2-Amino-3-methoxypyridine
Purity: 95+%
Packaging: 1g
Price: $51
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H30-1-01
Product name: 2-Amino-3-methoxypyridine
Purity: 97%
Packaging: 1g
Price: $55
Updated: 2021/12/16

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2-Amino-3-methoxypyridine Chemical Properties,Usage,Production

Chemical Properties

solid

Synthesis

20265-37-6

10201-71-5

Under nitrogen protection, 2-nitro-3-methoxypyridine (32 g, 208 mmol) was dissolved in a solvent mixture of ethyl acetate (150 mL) and methanol (35 mL) and 10% palladium-carbon catalyst (1.5 g, 1.4 mmol) was added. After displacing the reaction system with hydrogen three times, the reaction mixture was stirred under hydrogen atmosphere for 3 hours. Upon completion of the reaction, the system was again displaced three times with nitrogen, the reaction mixture was filtered through a diatomaceous earth pad, and the filter cake was washed with ethyl acetate (2 x 35 mL). The filtrates were combined, concentrated under reduced pressure and dried under high vacuum to give 25.8 g of 2-amino-3-methoxypyridine (100% yield). The product was analyzed by LC-MS showing m/z: 125.0 (MH+); 1H NMR (300 MHz, CDCl3) δ: 7.66 (m, 1H), 6.90 (m, 1H), 6.61 (m, 2H), 4.64 (s, br, 2H), 3.83 (s, 3H).

References

[1] Patent: US2013/210818, 2013, A1. Location in patent: Paragraph 0380
[2] Patent: WO2009/115572, 2009, A2. Location in patent: Page/Page column 114-115
[3] Patent: WO2014/206903, 2014, A1. Location in patent: Page/Page column 15; 16
[4] Green Chemistry, 2017, vol. 19, # 3, p. 809 - 815
[5] Patent: WO2013/92739, 2013, A1. Location in patent: Page/Page column 16

2-Amino-3-methoxypyridine Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-Amino-3-methoxypyridine manufacturers

Dideu Industries Group Limited

Product: 2-Amino-3-methoxypyridine 10201-71-5
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons Min
Release date: 2021-10-26

Career Henan Chemical Co

Product: 2-Amino-3-methoxypyridine 10201-71-5
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 200kg
Release date: 2019-12-26

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10201-71-5

Heterocycle-Pyridine series

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Pyridine