ChemicalBook > CAS DataBase List > tert-Butyl 3-aminobenzylcarbamate

tert-Butyl 3-aminobenzylcarbamate

Product Name: tert-Butyl 3-aminobenzylcarbamate
CAS No.: 147291-66-5
Chemical Name: tert-Butyl 3-aminobenzylcarbamate
Synonyms: 178769;3-Amino-N-Boc-benzylamine;α-(Boc-amino)-m-toluidine;alpha-(Boc-amino)-m-toluidine;tert-Butyl 3-aminobenzylcarbamate;3-(Aminomethyl)aniline, 3-BOC protected;3-Amino-N-(tert-butoxycarbonyl)benzylamine;3-[(tert-Butoxycarbonylamino)methyl]aniline;tert-Butyl 3-aminobenzylcarbamate AldrichCPR;alpha-(tert-Butoxycarbonyl)amino-m-toluidine
CBNumber: CB71117454
Molecular Formula: C12H18N2O2
Formula Weight: 222.28
MOL File: 147291-66-5.mol

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tert-Butyl 3-aminobenzylcarbamate Property

Melting point:: 48.0 to 56.0 °C
Boiling point:: 386.0±25.0 °C(Predicted)
Density: 1.095±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
solubility: soluble in Methanol
form: powder to crystal
pka: 12.31±0.46(Predicted)
color: White to Light yellow

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Safety

Hazard Codes: Xn
Risk Statements: 22
WGK Germany: 3
HS Code: 2924297099

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TCI Chemical

Product number: A2718
Product name: 3-Amino-N-(tert-butoxycarbonyl)benzylamine
Purity: >98.0%(GC)(T)
Packaging: 1g
Price: $302
Updated: 2025/07/31

TCI Chemical

Product number: A2718
Product name: 3-Amino-N-(tert-butoxycarbonyl)benzylamine
Purity: >98.0%(GC)(T)
Packaging: 5g
Price: $905
Updated: 2024/03/01

TRC

Product number: T135660
Product name: tert-Butyl 3-aminobenzylcarbamate
Packaging: 250mg
Price: $90
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4756-1-07
Product name: tert-Butyl 3-aminobenzylcarbamate
Purity: 97%
Packaging: 1g
Price: $108
Updated: 2021/12/16

Activate Scientific

Product number: AS85893
Product name: 3-(Boc-aminomethyl)aniline
Purity: 95+%
Packaging: 1g
Price: $139
Updated: 2021/12/16

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tert-Butyl 3-aminobenzylcarbamate Chemical Properties,Usage,Production

Synthesis

147291-65-4

147291-66-5

Step 2: Synthesis of tert-butyl 3-aminobenzylcarbamate (3); To a solution of tert-butyl 3-nitrobenzylcarbamate (2, 0.69 g, 2.73 mmol) in ethanol (20 mL) was added 10% Pd-C (50 mg), and the resulting mixture was stirred for 30 min at room temperature under hydrogen atmosphere. The reaction progress was monitored by thin layer chromatography (TLC). After completion of the reaction, the reaction mixture was filtered through diatomaceous earth and washed with ethanol. Ethanol was evaporated from the filtrate under reduced pressure to give tert-butyl 3-aminobenzylcarbamate (3, 0.6 g, 98%). NMR hydrogen spectrum (400 MHz, CDCl3): δ 7.22 (s, 1H), 7.10-7.00 (t, 1H), 6.70-6.60 (d, 1H), 6.60-6.50 (m, 1H), 4.20 (bs, 2H), 1.40 (s, 9H).

References

[1] Patent: WO2011/140338, 2011, A1. Location in patent: Page/Page column 60-61
[2] Chemical Communications, 2014, vol. 50, # 97, p. 15305 - 15308
[3] Bioorganic and Medicinal Chemistry, 2003, vol. 11, # 19, p. 4189 - 4206
[4] Journal of Medicinal Chemistry, 1998, vol. 41, # 15, p. 2858 - 2871
[5] Bioorganic and Medicinal Chemistry Letters, 2002, vol. 12, # 6, p. 883 - 886

tert-Butyl 3-aminobenzylcarbamate Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from tert-Butyl 3-aminobenzylcarbamate manufacturers

Honest Joy Holdings Limited

Product: tert-Butyl 3-aminobenzylcarbamate 147291-66-5
Price: US $0.00/KG
Min. Order: 1KG
Purity: 98.7%
Supply Ability: 100 tons
Release date: 2022-02-08

Career Henan Chemical Co

Product: tert-Butyl 3-aminobenzylcarbamate 147291-66-5
Price: US $1.00/KG
Min. Order: 1KG
Purity: 95%~99%
Supply Ability: 1ton
Release date: 2019-12-18

147291-66-5, tert-Butyl 3-aminobenzylcarbamateRelated Search:

tert-Butyl 3-bromo-2-fluorobenzoate 2-Pyridinecarboxylic acid, 3-broMo-6-fluoro-, 1,1-diMethylethyl ester N-(3-BOC-AMINOMETHYLPHENYL)-N-(4-METHOXYPHENYL)AMINE TERT-BUTYL 5-AMINOISOINDOLINE-2-CARBOXYLATE 7-AMINO-3,4-DIHYDRO-1H-ISOQUINOLINE-2-CARBOXYLIC ACID TERT-BUTYL ESTER tert-Butyl 3-aminobenzylcarbamate 7-AMINO-2-(TERT-BUTOXYCARBONYL)-1,2,3,4-TETRAHYDROISOQUINOLINE-3-CARBOXYLIC ACID 5-AMINO-2-BOC-1,2,3,4-TETRAHYDROISOQUINOLINE 7-AMINO-4-BOC-2,3,4,5-TETRAHYDRO-1H-BENZO[E][1,4]DIAZEPINE Boc-(S)-3-amino-3-(3-nitro-phenyl)-propanoic acid N-(4-BROMOPHENYL-N-(3-BOC-AMINOMETHYLPHENYL)AMINE [1-(3-AMINO-PHENYL)-ETHYL]-CARBAMIC ACID TERT-BUTYL ESTER (4-FLUORO-3-NITRO-BENZYL)-CARBAMIC ACID TERT-BUTYL ESTER 3-N-BOC-3-(3-NITROPHENYL)PROPIONIC ACID {3-[2-(4-HYDROXY-PHENYL)-ACETYLAMINO]-BENZYL}-CARBAMIC ACID TERT-BUTYL ESTER 5-NITRO-3,4-DIHYDRO-1H-ISOQUINOLINE-2-CARBOXYLIC ACID TERT-BUTYL ESTER Boc-(R)-3-amino-3-(3-nitro-phenyl)-propanoic acid TERT-BUTYL 5-AMINO-1H-BENZO[DE]ISOQUINOLINE-2(3H)-CARBOXYLATE

(3-Aminobenzyl)carbamic acid tert-butyl ester

tert-butyl N-[(3-aMinophenyl)Methyl]carbaMate

N-(3-aMinophenylMethyl)carbaMic acid t-butyl ester

3-(Aminomethyl)aniline, 3-BOC protected

tert-Butyl (3-aminobenzyl)carbamate, 3-{[(tert-Butoxycarbonyl)amino]methyl}aniline

3-Amino-N-(tert-butoxycarbonyl)benzylamine

tert-Butyl 3-aminobenzylcarbamate AldrichCPR

tert-Butyl 3-aminobenzylcarbamate

3-Amino-<i>N</i>-(<i>tert</i>-butoxycarbonyl)benzylamine

178769

Carbamic acid,N-[(3-aminophenyl)methyl]-, 1,1-dimethylethyl ester

3-Amino-N-(tert-butoxycarbonyl)benzylamine &gt

3-[(tert-Butoxycarbonylamino)methyl]aniline

3-Amino-N-Boc-benzylamine

alpha-(Boc-amino)-m-toluidine

alpha-(tert-Butoxycarbonyl)amino-m-toluidine

α-(Boc-amino)-m-toluidine

2-methylpropan-2-yl {[(3-aminophenyl)methyl]amino}methanoate

147291-66-5