2-Pyridinecarboxylicacid,5-amino-,ethylester(9CI)
- Product Name
- 2-Pyridinecarboxylicacid,5-amino-,ethylester(9CI)
- CAS No.
- 119830-47-6
- Chemical Name
- 2-Pyridinecarboxylicacid,5-amino-,ethylester(9CI)
- Synonyms
- Ethyl 5-aminopicolinate;ethyl 3-amino-pyridine-6-carboxylate;5-Aminopyridine-2-carboxylic acid ethyl ester;5-amino-2-pyridinecarboxylic acid ethyl ester;2-Pyridinecarboxylic acid, 5-aMino-, ethyl ester;2-Pyridinecarboxylicacid,5-amino-,ethylester(9CI)
- CBNumber
- CB71296793
- Molecular Formula
- C8H10N2O2
- Formula Weight
- 166.18
- MOL File
- 119830-47-6.mol
2-Pyridinecarboxylicacid,5-amino-,ethylester(9CI) Property
- storage temp.
- 2-8°C(protect from light)
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B434550
- Product name
- Ethyl5-Aminopicolinate
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- CHM0118595
- Product name
- ETHYL 5-AMINOPYRIDINE-2-CARBOXYLATE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $497.93
- Updated
- 2021/12/16
- Product number
- 161228
- Product name
- 5-Aminopyridine-2-carboxylic acid ethyl ester
- Purity
- 95%+
- Packaging
- 500mg
- Price
- $580
- Updated
- 2021/12/16
- Product number
- 3426AA
- Product name
- Ethyl5-aminopicolinate
- Packaging
- 250mg
- Price
- $719
- Updated
- 2021/12/16
- Product number
- 3426AA
- Product name
- Ethyl5-aminopicolinate
- Packaging
- 500mg
- Price
- $793
- Updated
- 2021/12/16
2-Pyridinecarboxylicacid,5-amino-,ethylester(9CI) Chemical Properties,Usage,Production
Synthesis
30563-98-5
119830-47-6
The general procedure for the synthesis of ethyl 5-amino-2-pyridinecarboxylate from ethyl 5-nitropyridinecarboxylate was as follows: a suspension of ethyl 5-nitropyridine-2-carboxylate (2.00 g, 10.2 mmol) and 10% Pd/C (200 mg) in ethanol (30 mL) was subjected to a hydrogen atmosphere, and the reaction was oscillated for 4 hr at a pressure of 40 psi. Upon completion of the reaction, the catalyst was removed by diatomaceous earth filtration and rinsed with ethanol. The filtrate was concentrated under reduced pressure to give 1.47 g (87% yield) of yellow solid product. The 1H NMR spectrum of this product was in agreement with literature reports (Min, RS; Aksenov, VS Chem. Heterocycl. Compd. (Engl. Transl.) 1988, 24, 885-886), and it could be used in subsequent reactions without further purification.
References
[1] Patent: US2005/38078, 2005, A1. Location in patent: Page/Page column 30
[2] Patent: WO2004/14904, 2004, A1. Location in patent: Page 54
[3] Journal of Organic Chemistry, 1984, vol. 49, # 20, p. 3681 - 3684
2-Pyridinecarboxylicacid,5-amino-,ethylester(9CI) Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-Pyridinecarboxylicacid,5-amino-,ethylester(9CI) manufacturers
- Product
- 2-Pyridinecarboxylicacid,5-amino-,ethylester(9CI) 119830-47-6
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-11
- Product
- 2-Pyridinecarboxylicacid,5-amino-,ethylester(9CI) 119830-47-6
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-09