5-BROMO-2-HYDROXY-3-PICOLINE
- Product Name
- 5-BROMO-2-HYDROXY-3-PICOLINE
- CAS No.
- 89488-30-2
- Chemical Name
- 5-BROMO-2-HYDROXY-3-PICOLINE
- Synonyms
- 5-Bromo-2-hydroxy-3-methyL;5-BROMO-3-METHYL-2-PYRIDONE;2-Hydorxy-5-Bromo-3-Picoline;2-HYDROXY-5-BROMO-3-PICOLINE;5-BROMO-2-HYDROXY-3-PICOLINE;5-BROMO-3-METHYL-2-PYRIDINOL;5-BROMO-3-METHYL-PYRIDIN-2-OL;5-Bromo-2-hydroxy-3-picoline,98%;5-bromo-3-methyl-1H-pyridin-2-one;5-Bromo-3-methyl-2(1H)-pyridinone
- CBNumber
- CB7163320
- Molecular Formula
- C6H6BrNO
- Formula Weight
- 188.02
- MOL File
- 89488-30-2.mol
5-BROMO-2-HYDROXY-3-PICOLINE Property
- Melting point:
- 170-174 °C(lit.)
- Boiling point:
- 295.1±40.0 °C(Predicted)
- Density
- 1.5296 (rough estimate)
- refractive index
- 1.5500 (estimate)
- storage temp.
- Inert atmosphere,Room Temperature
- solubility
- soluble in Methanol
- pka
- 10.55±0.10(Predicted)
- form
- Solid
- color
- Off-white
- CAS DataBase Reference
- 89488-30-2(CAS DataBase Reference)
Safety
- Hazard Codes
- Xn,Xi
- Risk Statements
- 22-38-41-36/37/38
- Safety Statements
- 36/37/39-36-26
- WGK Germany
- 3
- Hazard Note
- Harmful
- HazardClass
- IRRITANT
- HS Code
- 29337900
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H318Causes serious eye damage
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
N-Bromosuccinimide Price
- Product number
- 636355
- Product name
- 5-Bromo-2-hydroxy-3-methylpyridine
- Purity
- 97%
- Packaging
- 1g
- Price
- $81.2
- Updated
- 2023/01/07
- Product number
- B2797
- Product name
- 5-Bromo-2-hydroxy-3-methylpyridine
- Purity
- >98.0%(GC)
- Packaging
- 1g
- Price
- $16
- Updated
- 2025/07/31
- Product number
- B2797
- Product name
- 5-Bromo-2-hydroxy-3-methylpyridine
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $57
- Updated
- 2025/07/31
- Product number
- B696253
- Product name
- 5-Bromo-2-hydroxy-3-picoline
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- B696253
- Product name
- 5-Bromo-2-hydroxy-3-picoline
- Packaging
- 250mg
- Price
- $55
- Updated
- 2021/12/16
5-BROMO-2-HYDROXY-3-PICOLINE Chemical Properties,Usage,Production
Chemical Properties
creamish to light brown crystalline powder
Uses
5-Bromo-3-methylpyridin-2(1H)-one is a biochemical reagent that can be used as a biological material or organic compound for life science related research.
Synthesis
3430-21-5
89488-30-2
The general procedure for the synthesis of 5-bromo-3-methylpyridin-2-one from 2-amino-3-methyl-5-bromopyridine is as follows: Example 1. 1A. To a solution of 2.6 M H2SO4 (70 mL) of 2-amino-5-bromo-3-methylpyridine (5.0 g, 26.7 mmol) was added dropwise an aqueous solution (10 mL) of sodium 2-nitrite (5.0 g, 72.5 mmol) at 0 °C. 1B. The reaction mixture was slowly warmed to room temperature and stirring was continued for 1.5 hours. 1C. Upon completion of the reaction, the mixture was filtered and the resulting solid was washed with cold water. 1D. The washed solid was dissolved in dichloromethane (100 mL), dried by adding anhydrous magnesium sulfate, and the solvent was subsequently concentrated to give 5-bromo-3-methylpyridin-2-one (4.2 g, 84% yield). MS (DCI/NH3) m/z: 188/190 (M+H)+.
References
[1] Patent: US2002/19388, 2002, A1
[2] Patent: EP1428824, 2004, A1. Location in patent: Page 49
[3] Patent: WO2008/67644, 2008, A1. Location in patent: Page/Page column 39
5-BROMO-2-HYDROXY-3-PICOLINE Preparation Products And Raw materials
Raw materials
Preparation Products
5-BROMO-2-HYDROXY-3-PICOLINE Suppliers
- Tel
- 18210857532; 18210857532
- Fax
- 86-10-82849933
- jkinfo@jkchemical.com
- Country
- China
- ProdList
- 96815
- Advantage
- 76
- Tel
- 4006356688 18621169109
- Fax
- 86-21-61259102
- market03@meryer.com
- Country
- China
- ProdList
- 40228
- Advantage
- 62
- Tel
- 021-67121386
- Fax
- 021-67121385
- Sales-CN@TCIchemicals.com
- Country
- China
- ProdList
- 24529
- Advantage
- 81
- Tel
- 400-021-7337 2355568890
- Fax
- 0086-21-50182339
- sales@demochem.com
- Country
- China
- ProdList
- 2572
- Advantage
- 57
- Tel
- 021-021-58432009 400-005-6266
- Fax
- 021-58436166
- sales8178@energy-chemical.com
- Country
- China
- ProdList
- 44801
- Advantage
- 61
- Tel
- 0311-89250318 031166536426
- Fax
- 4000311741
- master@sjzsdyn.com
- Country
- China
- ProdList
- 2809
- Advantage
- 65
- Tel
- 86-027-67849912
- Fax
- 86-027-87531808
- sales@chemwish.com
- Country
- China
- ProdList
- 35896
- Advantage
- 56
- Tel
- +86 (0) 571 85 58 67 18
- Fax
- 0086-571-85864795
- Country
- China
- ProdList
- 18207
- Advantage
- 66
- Tel
- 010-010-82967028 13522913783
- Fax
- +86-10-82967029
- 2355560935@qq.com
- Country
- China
- ProdList
- 12000
- Advantage
- 60
- Tel
- 13817811078
- Fax
- 86-021-50426522,50426273
- sales@jingyan-chemical.com
- Country
- China
- ProdList
- 9976
- Advantage
- 60
View Lastest Price from 5-BROMO-2-HYDROXY-3-PICOLINE manufacturers
- Product
- 5-BROMO-2-HYDROXY-3-PICOLINE 89488-30-2
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 98.0%
- Supply Ability
- 10000KGS
- Release date
- 2025-05-30
- Product
- 5-BROMO-2-HYDROXY-3-PICOLINE 89488-30-2
- Price
- US $5.00-0.10/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2024-04-09
- Product
- 5-BROMO-2-HYDROXY-3-PICOLINE 89488-30-2
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons Min
- Release date
- 2021-09-24