9,10-Bis(chloromethyl)anthracene
- Product Name
- 9,10-Bis(chloromethyl)anthracene
- CAS No.
- 10387-13-0
- Chemical Name
- 9,10-Bis(chloromethyl)anthracene
- Synonyms
- icr-450;9,10-Bis-(chlorometh;Bischloromethylanthracene;9, 10-DI(CHLOROMETHYL)ANTHRA;9,10-bis(chlormethyl)anthracene;9,1-bis(chloromethyl)anthracene;9, 10-DI(CHLOROMETHYL)ANTHRACENE;9,10-BIS(CHLOROMETHYL)ANTHRACENE;9,10-bis(chloromethyl)-anthracen;9,10-Dis-(chloromethyl)anthracene
- CBNumber
- CB7197554
- Molecular Formula
- C16H12Cl2
- Formula Weight
- 275.17
- MOL File
- 10387-13-0.mol
9,10-Bis(chloromethyl)anthracene Property
- Melting point:
- 258-260°C
- Boiling point:
- 355.58°C (rough estimate)
- Density
- 1.1151 (rough estimate)
- refractive index
- 1.5610 (estimate)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- solubility
- very faint turbidity in hot Toluene
- form
- powder to crystal
- color
- Crystals from xylene; yellow blades from toluene
- CAS DataBase Reference
- 10387-13-0(CAS DataBase Reference)
- EPA Substance Registry System
- Anthracene, 9,10-bis(chloromethyl)- (10387-13-0)
Safety
- Risk Statements
- 36/37/38
- Safety Statements
- 26-36/37/39
- RIDADR
- 3261
- RTECS
- CA9365000
- HS Code
- 2903.99.8001
- HazardClass
- 8
- PackingGroup
- II
- Toxicity
- mma-sat 100 ng/plate PNASA6 72,5135,75
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H290May be corrosive to metals
H314Causes severe skin burns and eye damage
- Precautionary statements
-
P234Keep only in original container.
P260Do not breathe dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P390Absorb spillage to prevent material damage.
P405Store locked up.
P406Store in corrosive resistant/… container with a resistant inner liner.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- S278343
- Product name
- 9,10-BIS-CHLOROMETHYL-ANTHRACENE
- Purity
- Aldrich<sup>CPR</sup>
- Packaging
- 1 unit
- Price
- $30.7
- Updated
- 2025/07/31
- Product number
- S17435
- Product name
- 9,10-BIS(CHLOROMETHYL)ANTHRACENE
- Purity
- Aldrich<sup>CPR</sup>
- Packaging
- 1 unit
- Price
- $185
- Updated
- 2025/07/31
- Product number
- S278343
- Product name
- 9,10-BIS-CHLOROMETHYL-ANTHRACENE
- Purity
- Aldrich
- Packaging
- 10mg
- Price
- $29.8
- Updated
- 2024/03/01
- Product number
- S17435
- Product name
- 9,10-BIS(CHLOROMETHYL)ANTHRACENE
- Purity
- Aldrich
- Packaging
- 250mg
- Price
- $179
- Updated
- 2024/03/01
- Product number
- S330345
- Product name
- 9,10-BIS-CHLOROMETHYL-ANTHRACENE
- Purity
- AldrichCPR
- Packaging
- 25MG
- Price
- $28.6
- Updated
- 2023/06/20
9,10-Bis(chloromethyl)anthracene Chemical Properties,Usage,Production
Safety Profile
Poison by intravenous route.Questionable carcinogen with experimental neoplastigenicdata. Mutation data reported. When heated todecomposition it emits toxic fumes of Cl-.
Synthesis
50-00-0
120-12-7
10387-13-0
A dioxane (20 mL) solution of anthracene (1.78 g, 10 mmol), anhydrous ZnCl2 (1.64 g, 12 mmol), and paraformaldehyde (1.50 g, 50 mmol) was added sequentially to a reactor vessel equipped with a stirrer. A concentrated aqueous hydrochloric acid solution (40 mL) was added slowly and dropwise with stirring, and the reaction temperature was controlled to be below 50 °C. The reaction mixture was stirred at room temperature until homogeneous and then heated to a mild reflux condition and kept for 3 hours. After completion of the reaction, the mixture was allowed to stand at room temperature for 16 hours to complete crystallization. The resulting fine grained solid was separated by diafiltration and washed sequentially with deionized water and dioxane. The crude product was purified by recrystallization with toluene to give 1.8 g of light yellow solid product in 64.1% yield. The structure of the product was confirmed by 1H NMR (500 MHz, CDCl3): δ 8.40 (m, 4H), 7.62 (m, 4H), 5.61 ppm (s, 4H).
References
[1] Journal of Organic Chemistry, 1998, vol. 63, # 18, p. 6153 - 6159
[2] Journal of Physical Chemistry B, 2005, vol. 109, # 10, p. 4377 - 4390
[3] Angewandte Chemie - International Edition, 2013, vol. 52, # 46, p. 12086 - 12090
[4] Angew. Chem., 2013, vol. 125, # 46, p. 12308 - 12312,5
[5] RSC Advances, 2015, vol. 5, # 90, p. 73951 - 73957
9,10-Bis(chloromethyl)anthracene Preparation Products And Raw materials
Raw materials
Preparation Products
9,10-Bis(chloromethyl)anthracene Suppliers
- Tel
- 800-4238616
- Fax
- +1-888-520-1075 / +1-503-283-1987
- sales@tciamerica.com
- Country
- Americas
- ProdList
- 23653
- Advantage
- 75
View Lastest Price from 9,10-Bis(chloromethyl)anthracene manufacturers
- Product
- 9,10-Bis(chloromethyl)anthracene 10387-13-0
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 98%min
- Supply Ability
- 30tons/month
- Release date
- 2023-04-07
- Product
- 9,10-Bis(chloromethyl)anthracene 10387-13-0
- Price
- US $100.00-1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2023-12-26
- Product
- 9,10-Bis(chloromethyl)anthracene 10387-13-0
- Price
- US $2.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1 ton
- Release date
- 2018-08-20