ChemicalBook > CAS DataBase List > 9,10-Bis(chloromethyl)anthracene

9,10-Bis(chloromethyl)anthracene

Product Name
9,10-Bis(chloromethyl)anthracene
CAS No.
10387-13-0
Chemical Name
9,10-Bis(chloromethyl)anthracene
Synonyms
icr-450;9,10-Bis-(chlorometh;Bischloromethylanthracene;9, 10-DI(CHLOROMETHYL)ANTHRA;9,10-bis(chlormethyl)anthracene;9,1-bis(chloromethyl)anthracene;9, 10-DI(CHLOROMETHYL)ANTHRACENE;9,10-BIS(CHLOROMETHYL)ANTHRACENE;9,10-bis(chloromethyl)-anthracen;9,10-Dis-(chloromethyl)anthracene
CBNumber
CB7197554
Molecular Formula
C16H12Cl2
Formula Weight
275.17
MOL File
10387-13-0.mol
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9,10-Bis(chloromethyl)anthracene Property

Melting point:
258-260°C
Boiling point:
355.58°C (rough estimate)
Density 
1.1151 (rough estimate)
refractive index 
1.5610 (estimate)
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
solubility 
very faint turbidity in hot Toluene
form 
powder to crystal
color 
Crystals from xylene; yellow blades from toluene
CAS DataBase Reference
10387-13-0(CAS DataBase Reference)
EPA Substance Registry System
Anthracene, 9,10-bis(chloromethyl)- (10387-13-0)
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Safety

Risk Statements 
36/37/38
Safety Statements 
26-36/37/39
RIDADR 
3261
RTECS 
CA9365000
HS Code 
2903.99.8001
HazardClass 
8
PackingGroup 
II
Toxicity
mma-sat 100 ng/plate PNASA6 72,5135,75
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H290May be corrosive to metals

H314Causes severe skin burns and eye damage

Precautionary statements

P234Keep only in original container.

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P390Absorb spillage to prevent material damage.

P405Store locked up.

P406Store in corrosive resistant/… container with a resistant inner liner.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
S278343
Product name
9,10-BIS-CHLOROMETHYL-ANTHRACENE
Purity
Aldrich<sup>CPR</sup>
Packaging
1 unit
Price
$30.7
Updated
2025/07/31
Sigma-Aldrich
Product number
S17435
Product name
9,10-BIS(CHLOROMETHYL)ANTHRACENE
Purity
Aldrich<sup>CPR</sup>
Packaging
1 unit
Price
$185
Updated
2025/07/31
Sigma-Aldrich
Product number
S278343
Product name
9,10-BIS-CHLOROMETHYL-ANTHRACENE
Purity
Aldrich
Packaging
10mg
Price
$29.8
Updated
2024/03/01
Sigma-Aldrich
Product number
S17435
Product name
9,10-BIS(CHLOROMETHYL)ANTHRACENE
Purity
Aldrich
Packaging
250mg
Price
$179
Updated
2024/03/01
Sigma-Aldrich
Product number
S330345
Product name
9,10-BIS-CHLOROMETHYL-ANTHRACENE
Purity
AldrichCPR
Packaging
25MG
Price
$28.6
Updated
2023/06/20
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9,10-Bis(chloromethyl)anthracene Chemical Properties,Usage,Production

Safety Profile

Poison by intravenous route.Questionable carcinogen with experimental neoplastigenicdata. Mutation data reported. When heated todecomposition it emits toxic fumes of Cl-.

Synthesis

50-00-0

120-12-7

10387-13-0

A dioxane (20 mL) solution of anthracene (1.78 g, 10 mmol), anhydrous ZnCl2 (1.64 g, 12 mmol), and paraformaldehyde (1.50 g, 50 mmol) was added sequentially to a reactor vessel equipped with a stirrer. A concentrated aqueous hydrochloric acid solution (40 mL) was added slowly and dropwise with stirring, and the reaction temperature was controlled to be below 50 °C. The reaction mixture was stirred at room temperature until homogeneous and then heated to a mild reflux condition and kept for 3 hours. After completion of the reaction, the mixture was allowed to stand at room temperature for 16 hours to complete crystallization. The resulting fine grained solid was separated by diafiltration and washed sequentially with deionized water and dioxane. The crude product was purified by recrystallization with toluene to give 1.8 g of light yellow solid product in 64.1% yield. The structure of the product was confirmed by 1H NMR (500 MHz, CDCl3): δ 8.40 (m, 4H), 7.62 (m, 4H), 5.61 ppm (s, 4H).

References

[1] Journal of Organic Chemistry, 1998, vol. 63, # 18, p. 6153 - 6159
[2] Journal of Physical Chemistry B, 2005, vol. 109, # 10, p. 4377 - 4390
[3] Angewandte Chemie - International Edition, 2013, vol. 52, # 46, p. 12086 - 12090
[4] Angew. Chem., 2013, vol. 125, # 46, p. 12308 - 12312,5
[5] RSC Advances, 2015, vol. 5, # 90, p. 73951 - 73957

9,10-Bis(chloromethyl)anthracene Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 9,10-Bis(chloromethyl)anthracene manufacturers

WUHAN FORTUNA CHEMICAL CO., LTD
Product
9,10-Bis(chloromethyl)anthracene 10387-13-0
Price
US $0.00/KG
Min. Order
1KG
Purity
98%min
Supply Ability
30tons/month
Release date
2023-04-07
Henan Fengda Chemical Co., Ltd
Product
9,10-Bis(chloromethyl)anthracene 10387-13-0
Price
US $100.00-1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
g-kg-tons, free sample is available
Release date
2023-12-26
Career Henan Chemical Co
Product
9,10-Bis(chloromethyl)anthracene 10387-13-0
Price
US $2.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
1 ton
Release date
2018-08-20

10387-13-0, 9,10-Bis(chloromethyl)anthraceneRelated Search:


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  • 9, 10-DI(CHLOROMETHYL)ANTHRACENE 98%
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  • 9,10-Bis-(chlorometh
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  • 9,10-Bis(chloromethyl)anthracene &gt
  • Anthracene, 9,10-bis(chloromethyl)-
  • 9,10-Bis(chloromethyl)anthracene ISO 9001:2015 REACH
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  • 10387-13-0
  • C16H12C12
  • C16H12Cl2
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