ChemicalBook > CAS DataBase List > (4-OXO-4-PHENYL-BUTYL)-CARBAMIC ACID TERT-BUTYL ESTER

(4-OXO-4-PHENYL-BUTYL)-CARBAMIC ACID TERT-BUTYL ESTER

Product Name
(4-OXO-4-PHENYL-BUTYL)-CARBAMIC ACID TERT-BUTYL ESTER
CAS No.
116437-41-3
Chemical Name
(4-OXO-4-PHENYL-BUTYL)-CARBAMIC ACID TERT-BUTYL ESTER
Synonyms
4-(Boc-amino)-1-phenyl-butan-1-o;4-(Boc-amino)-1-phenyl-1-butanone;4-(BOC-AMINO)-1-PHENYL-BUTAN-1-ONE;4-(N-BOC-Amino)-1-phenylbutan-1-one;tert-butyl 4-oxo-4-phenylbutylcarbaMate;tert-Butyl N-(4-oxo-4-phenylbutyl)carbamate;(4-Oxo-4-phenyl-butyl)-carbamic acid tert-butyl;1,1-Dimethylethyl N-(4-oxo-4-phenylbutyl)carbamate;(4-OXO-4-PHENYL-BUTYL)-CARBAMIC ACID TERT-BUTYL ESTER;N-(4-oxo-4-phenylbutyl)carbaMic acid tert-butyl ester
CBNumber
CB7198829
Molecular Formula
C15H21NO3
Formula Weight
263.33
MOL File
116437-41-3.mol
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(4-OXO-4-PHENYL-BUTYL)-CARBAMIC ACID TERT-BUTYL ESTER Property

Melting point:
90-91°C
Boiling point:
406.8±28.0 °C(Predicted)
Density 
1.058±0.06 g/cm3(Predicted)
storage temp. 
2-8°C
pka
12.66±0.46(Predicted)
Appearance
White to pink Solid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H410Very toxic to aquatic life with long lasting effects

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P273Avoid release to the environment.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

P391Collect spillage. Hazardous to the aquatic environment

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC
Product number
B810083
Product name
tert-Butyl(4-Oxo-4-phenylbutyl)carbamate
Packaging
250mg
Price
$90
Updated
2021/12/16
SynQuest Laboratories
Product number
4656-1-72
Product name
tert-Butyl N-(4-oxo-4-phenylbutyl)carbamate
Purity
98.0%
Packaging
1g
Price
$100
Updated
2021/12/16
ChemScene
Product number
CS-M1642
Product name
Carbamicacid,N-(4-oxo-4-phenylbutyl)-,1,1-dimethylethylester
Packaging
5g
Price
$167
Updated
2021/12/16
ChemScene
Product number
CS-M1642
Product name
Carbamicacid,N-(4-oxo-4-phenylbutyl)-,1,1-dimethylethylester
Packaging
10g
Price
$306
Updated
2021/12/16
AK Scientific
Product number
2693AA
Product name
tert-Butyl(4-oxo-4-phenylbutyl)carbamate
Packaging
5g
Price
$327
Updated
2021/12/16
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(4-OXO-4-PHENYL-BUTYL)-CARBAMIC ACID TERT-BUTYL ESTER Chemical Properties,Usage,Production

Synthesis

85909-08-6

100-58-3

116437-41-3

Step A: Preparation of tert-butyl N-(4-oxo-4-phenylbutyl)carbamate: tert-butyl 2-oxo-pyrrolidine-1-carboxylate (7.03 g, 38 mmol) was dissolved in tetrahydrofuran (130 mL) and cooled to -78°C. Phenylmagnesium bromide (1.0 M solution, 50 mL) was slowly added at -78 °C. The reaction mixture was stirred at -78 °C for 2 h before the reaction was quenched with 2 M hydrochloric acid solution (35 mL). Subsequently, the reaction mixture was slowly warmed to room temperature and the aqueous layer was extracted with ethyl acetate (2 x 100 mL). The organic phases were combined, washed with saturated brine (50 mL), dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give 9.56 g of the title compound in 96% yield.

References

[1] Patent: WO2006/44825, 2006, A2. Location in patent: Page/Page column 55
[2] Patent: US2012/184542, 2012, A1. Location in patent: Page/Page column 109
[3] Organic Letters, 2011, vol. 13, # 16, p. 4348 - 4351

(4-OXO-4-PHENYL-BUTYL)-CARBAMIC ACID TERT-BUTYL ESTER Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from (4-OXO-4-PHENYL-BUTYL)-CARBAMIC ACID TERT-BUTYL ESTER manufacturers

Career Henan Chemical Co
Product
(4-OXO-4-PHENYL-BUTYL)-CARBAMIC ACID TERT-BUTYL ESTER 116437-41-3
Price
US $3.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
200KG
Release date
2020-02-20

116437-41-3, (4-OXO-4-PHENYL-BUTYL)-CARBAMIC ACID TERT-BUTYL ESTERRelated Search:

tert-butyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2-(trifluoromethyl)benzylcarbamate (4-Amino-phenyl)-methyl-carbamic acid tert-butyl ester Carbamic acid, N-(4-formyl-3-hydroxyphenyl)-, 1,1-dimethylethyl ester tert-butyl (4-(ethoxycarbonyl)thiazol-2-yl)methylcarbamate tert-Butyl (4-bromo-7-fluorobenzo[d]thiazol-2-yl)carbamate [4-(6-FORMYLPYRIDIN-2-YL)PHENYL]CARBAMIC ACID TERT-BUTYL ESTER Carbamic acid, N-[4-(difluoromethyl)-2-thiazolyl]-, 1,1-dimethylethyl ester (5-AMINO-2-METHYL-PHENYL)-CARBAMIC ACID TERT-BUTYL ESTER 4-(2-CHLORO-3-ETHYL-QUINOLINE-6-CARBONYL)-PIPERIDINE-1-CARBOXYLIC ACIDTERT-BUTYL ESTER BIO-FARMA BF002997 BENZYL (2S)-2-[(TERT-BUTOXYCARBONYL)AMINO]-5-OXO-5-PHENYLPENTANOATE TERT-BUTYL 4-(4-FLUOROBENZOYL)PIPERIDINE-1-CARBOXYLATE BIO-FARMA BF003000 1-BOC-4-(4-CHLORO-BENZOYL)-PIPERIDINE 1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE (4-OXO-4-PHENYL-BUTYL)-CARBAMIC ACID TERT-BUTYL ESTER

  • CarbaMic acid, N-(4-oxo-4-phenylbutyl)-, 1,1-diMethylethyl ester
  • tert-butyl 4-oxo-4-phenylbutylcarbaMate
  • N-(4-oxo-4-phenylbutyl)carbaMic acid tert-butyl ester
  • tert-Butyl N-(4-oxo-4-phenylbutyl)carbamate
  • 4-(BOC-AMINO)-1-PHENYL-BUTAN-1-ONE
  • (4-OXO-4-PHENYL-BUTYL)-CARBAMIC ACID TERT-BUTYL ESTER
  • (4-Oxo-4-phenyl-butyl)-carbamic acid tert-butyl
  • 4-(BOC-AMINO)-1-PHENYL-BUTAN-1-ONE, (4-OXO-4-PHENYL-BUTYL)-CARBAMIC ACID TERT-BUTYL ESTER >98%
  • 4-(Boc-amino)-1-phenyl-butan-1-o
  • 1,1-Dimethylethyl N-(4-oxo-4-phenylbutyl)carbamate
  • 4-(Boc-amino)-1-phenyl-1-butanone
  • 4-(N-BOC-Amino)-1-phenylbutan-1-one
  • 116437-41-3