ChemicalBook > CAS DataBase List > 1-(5-Bromo-2-nitro-phenyl)-ethanone
1-(5-Bromo-2-nitro-phenyl)-ethanone
- Product Name
- 1-(5-Bromo-2-nitro-phenyl)-ethanone
- CAS No.
- 41877-24-1
- Chemical Name
- 1-(5-Bromo-2-nitro-phenyl)-ethanone
- Synonyms
- 1-(5-Bromo-2-nitrophenyl)ethan-1-one;1-(5-Bromo-2-nitrophenyl);5'-Bromo-2'-nitroacetophenone;1-(5-Bromo-2-nitro-phenyl)-ethano;1-(5-Bromo-2-nitro-phenyl)-ethanone;Ethanone, 1-(5-bromo-2-nitrophenyl)-;5-BroMo-2-nitroacetophenone (1-(5-broMo-2-nitrophenyl)-ethanone)
- CBNumber
- CB72103913
- Molecular Formula
- C8H6BrNO3
- Formula Weight
- 244.04
- MOL File
- 41877-24-1.mol
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1-(5-Bromo-2-nitro-phenyl)-ethanone Property
- Melting point:
- 92-94 °C
- Boiling point:
- 345.6±27.0 °C(Predicted)
- Density
- 1.637±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- Off-white to yellow Solid
- InChI
- InChI=1S/C8H6BrNO3/c1-5(11)7-4-6(9)2-3-8(7)10(12)13/h2-4H,1H3
- InChIKey
- AFDAUYYWZNNSFV-UHFFFAOYSA-N
- SMILES
- C(=O)(C1=CC(Br)=CC=C1[N+]([O-])=O)C
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Safety
- HS Code
- 2914790090
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N-Bromosuccinimide Price
TRC
- Product number
- B686603
- Product name
- 1-(5-Bromo-2-nitrophenyl)ethanone
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
ChemScene
- Product number
- CS-0040255
- Product name
- 1-(5-Bromo-2-nitrophenyl)ethanone
- Purity
- 99.96%
- Packaging
- 1g
- Price
- $37
- Updated
- 2021/12/16
AK Scientific
- Product number
- J50896
- Product name
- 1-(5-Bromo-2-nitrophenyl)ethanone
- Packaging
- 1g
- Price
- $49
- Updated
- 2021/12/16
SynQuest Laboratories
- Product number
- 4654-9-08
- Product name
- 1-(5-Bromo-2-nitrophenyl)ethan-1-one
- Purity
- 98.0%
- Packaging
- 250mg
- Price
- $50
- Updated
- 2021/12/16
Biosynth Carbosynth
- Product number
- FB32876
- Product name
- 1-(5-Bromo-2-nitrophenyl)ethanone
- Packaging
- 250mg
- Price
- $60
- Updated
- 2021/12/16
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1-(5-Bromo-2-nitro-phenyl)-ethanone Chemical Properties,Usage,Production
Synthesis
2142-63-4
41877-24-1
General procedure for the synthesis of 1-(5-bromo-2-nitrophenyl)ethanone from 3'-bromoacetophenone: 100 g of 3'-bromoacetophenone was slowly added dropwise to 500 ml of a mixture of sulfuric acid and nitric acid (1:7, v/v), pre-cooled to -20°C, kept the reaction temperature at -20°C and stirred overnight. Upon completion of the reaction, the reaction mixture was quenched by pouring it into ice water, and the precipitate was collected by filtration to give 107 g of 2-nitro-5-bromoacetophenone, the product was a yellow solid in 87% yield.
References
[1] Patent: CN102898374, 2016, B. Location in patent: Paragraph 0027-0029
[2] Chemical Communications, 2015, vol. 52, # 2, p. 331 - 334
[3] Bioorganic and Medicinal Chemistry, 2016, vol. 24, # 11, p. 2504 - 2518
[4] Journal of the American Chemical Society, 1996, vol. 118, # 34, p. 8127 - 8135
1-(5-Bromo-2-nitro-phenyl)-ethanone Preparation Products And Raw materials
Raw materials
Preparation Products
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