2-Aminobenzo[b]thiophene

Product Name: 2-Aminobenzo[b]thiophene
CAS No.: 4521-30-6
Chemical Name: 2-Aminobenzo[b]thiophene
Synonyms: benzothiophen-2-amine;2-Aminobenzo[b]thiophene
CBNumber: CB72140424
Molecular Formula: C8H7NS
Formula Weight: 149.21
MOL File: 4521-30-6.mol

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2-Aminobenzo[b]thiophene Property

Melting point:: 115-117 °C
Boiling point:: 313.1±15.0 °C(Predicted)
Density: 1.294±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
solubility: Chloroform (Sligthly), DMSO (Slightly), Methanol (Slightly)
form: Solid
pka: 3.79±0.10(Predicted)
color: Pale Red to Very Dark Brown

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B206875
Product name: Benzo[b]thiophen-2-amine
Packaging: 250mg
Price: $470
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB140394
Product name: Benzo[b]thiophen-2-amine
Packaging: 100mg
Price: $59
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB140394
Product name: Benzo[b]thiophen-2-amine
Packaging: 250mg
Price: $117.5
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB140394
Product name: Benzo[b]thiophen-2-amine
Packaging: 500mg
Price: $205
Updated: 2021/12/16

AK Scientific

Product number: W6356
Product name: Benzo[b]thiophen-2-amine
Packaging: 250mg
Price: $219
Updated: 2021/12/16

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2-Aminobenzo[b]thiophene Chemical Properties,Usage,Production

Synthesis

89673-36-9

4521-30-6

General procedure for the synthesis of benzo[b]thiophen-2-amine from tert-butyl benzothiophen-2-ylcarbamate: tert-butyl 1-benzothiophen-2-ylcarbamate (1.0 g, 4.01 mmol) was added to a solution of 1-benzothiophen-2-ylcarbamate in dichloromethane (DCM, 10 mL), and the reaction was stirred at room temperature for 12 hours. Upon completion of the reaction, the reaction mixture was concentrated and the resulting residue was redissolved in dichloromethane, washed sequentially with 1N sodium hydroxide solution (2 x 50 mL) and saturated saline, and the organic phase was dried with anhydrous sodium sulfate. The drier was removed by filtration and the filtrate was concentrated to give the pure benzo[b]thiophen-2-amine (0.54 g, 91% yield).LCMS (m/z): 150.0 (M + H).

References

[1] Patent: WO2006/41968, 2006, A1. Location in patent: Page/Page column 38
[2] Patent: US2007/105864, 2007, A1. Location in patent: Page/Page column 193
[3] Patent: US2007/117804, 2007, A1. Location in patent: Page/Page column 125

2-Aminobenzo[b]thiophene Preparation Products And Raw materials

Raw materials

Preparation Products

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2-Aminobenzo[b]thiophene Suppliers

China 47 India 1 United Kingdom 1 United States 5 Global 54

Shandong Xiya Chemical Co., Ltd

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View Lastest Price from 2-Aminobenzo[b]thiophene manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 2-Aminobenzo[b]thiophene 4521-30-6
Price: US $25.00-11.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 200000KG
Release date: 2024-08-12

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2-Aminobenzo[b]thiophene

benzothiophen-2-amine

4521-30-6