2-Aminobenzo[b]thiophene
- Product Name
- 2-Aminobenzo[b]thiophene
- CAS No.
- 4521-30-6
- Chemical Name
- 2-Aminobenzo[b]thiophene
- Synonyms
- benzothiophen-2-amine;2-Aminobenzo[b]thiophene
- CBNumber
- CB72140424
- Molecular Formula
- C8H7NS
- Formula Weight
- 149.21
- MOL File
- 4521-30-6.mol
2-Aminobenzo[b]thiophene Property
- Melting point:
- 115-117 °C
- Boiling point:
- 313.1±15.0 °C(Predicted)
- Density
- 1.294±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
- solubility
- Chloroform (Sligthly), DMSO (Slightly), Methanol (Slightly)
- form
- Solid
- pka
- 3.79±0.10(Predicted)
- color
- Pale Red to Very Dark Brown
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B206875
- Product name
- Benzo[b]thiophen-2-amine
- Packaging
- 250mg
- Price
- $470
- Updated
- 2021/12/16
- Product number
- CHM0391809
- Product name
- BENZO[B]THIOPHEN-2-AMINE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $496.28
- Updated
- 2021/12/16
- Product number
- FB140394
- Product name
- Benzo[b]thiophen-2-amine
- Packaging
- 2g
- Price
- $615
- Updated
- 2021/12/16
- Product number
- 075877
- Product name
- Benzo[b]thiophen-2-amine
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $629
- Updated
- 2021/12/16
- Product number
- 075877
- Product name
- Benzo[b]thiophen-2-amine
- Purity
- 95+%
- Packaging
- 1g
- Price
- $1357
- Updated
- 2021/12/16
2-Aminobenzo[b]thiophene Chemical Properties,Usage,Production
Synthesis
89673-36-9
4521-30-6
General procedure for the synthesis of benzo[b]thiophen-2-amine from tert-butyl benzothiophen-2-ylcarbamate: tert-butyl 1-benzothiophen-2-ylcarbamate (1.0 g, 4.01 mmol) was added to a solution of 1-benzothiophen-2-ylcarbamate in dichloromethane (DCM, 10 mL), and the reaction was stirred at room temperature for 12 hours. Upon completion of the reaction, the reaction mixture was concentrated and the resulting residue was redissolved in dichloromethane, washed sequentially with 1N sodium hydroxide solution (2 x 50 mL) and saturated saline, and the organic phase was dried with anhydrous sodium sulfate. The drier was removed by filtration and the filtrate was concentrated to give the pure benzo[b]thiophen-2-amine (0.54 g, 91% yield).LCMS (m/z): 150.0 (M + H).
References
[1] Patent: WO2006/41968, 2006, A1. Location in patent: Page/Page column 38
[2] Patent: US2007/105864, 2007, A1. Location in patent: Page/Page column 193
[3] Patent: US2007/117804, 2007, A1. Location in patent: Page/Page column 125
2-Aminobenzo[b]thiophene Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-Aminobenzo[b]thiophene manufacturers
- Product
- 2-Aminobenzo[b]thiophene 4521-30-6
- Price
- US $25.00-11.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 200000KG
- Release date
- 2024-08-12