2-METHOXY-6-METHYLBENZALDEHYDE

Product Name: 2-METHOXY-6-METHYLBENZALDEHYDE
CAS No.: 54884-55-8
Chemical Name: 2-METHOXY-6-METHYLBENZALDEHYDE
Synonyms: 6-Methoxy-2-methylbenzaldehyde;2-METHOXY-6-METHYLBENZALDEHYDE;Benzaldehyde, 2-Methoxy-6-Methyl-
CBNumber: CB7225811
Molecular Formula: C9H10O2
Formula Weight: 150.17
MOL File: 54884-55-8.mol

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2-METHOXY-6-METHYLBENZALDEHYDE Property

Melting point:: 40-41℃
Boiling point:: 256℃
Density: 1.062
Flash point:: 113℃
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
Appearance: Off-white to yellow <40°C Solid,>41°C Liquid

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Safety

HS Code: 2912490090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M263450
Product name: 2-Methoxy-6-methylbenzaldehyde
Packaging: 100mg
Price: $45
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2715-1-44
Product name: 2-Methoxy-6-methylbenzaldehyde
Purity: 97%
Packaging: 1g
Price: $108
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0379052
Product name: 2-METHOXY-6-METHYL BENZALDEHYDE
Purity: 95.00%
Packaging: 5MG
Price: $502.14
Updated: 2021/12/16

AK Scientific

Product number: Z4871
Product name: 2-Methoxy-6-methylbenzaldehyde
Packaging: 10g
Price: $702
Updated: 2021/12/16

Chemenu

Product number: CM253595
Product name: 2-Methoxy-6-methylbenzaldehyde
Purity: 95+%
Packaging: 25g
Price: $926
Updated: 2021/12/16

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2-METHOXY-6-METHYLBENZALDEHYDE Chemical Properties,Usage,Production

Synthesis Reference(s)

Synthesis, p. 1000, 1983 DOI: 10.1055/s-1983-30599

Synthesis

2944-49-2

54884-55-8

General procedure for the synthesis of 2-methoxy-6-methylbenzaldehyde from 1-methoxy-2,3-dimethylbenzene: Potassium peroxydisulfate (89.31 g, 0.33 mol) and copper(II) sulfate pentahydrate (27.22 g, 0.11 mol) were added to a mixture of 1-methoxy-2,3-dimethylbenzene (15 g, 0.11 mol) in aqueous acetonitrile ( 750 mL, V/V=1:1). The reaction mixture was stirred under reflux conditions for 15 minutes until complete consumption of the feedstock was confirmed by thin layer chromatography (TLC) detection. Upon completion of the reaction, the mixture was cooled to room temperature and the product was extracted with dichloromethane (2 x 225 mL). The organic layers were combined and washed sequentially with water (2 x 100 mL) and saturated saline (100 mL). The organic layer was dried over anhydrous sodium sulfate and concentrated under reduced pressure to obtain the crude product. The crude product was purified by silica gel column chromatography with the eluent of 4/96 (V/V) ethyl acetate/hexane to afford 2-methoxy-6-methylbenzaldehyde (7.32 g, 44.2% yield). The structure of the product was confirmed by 1H NMR (300 MHz, CDCl3): δ 2.60 (3H, s), 3.90 (3H, s), 6.80 (2H, t), 7.40 (1H, t), 10.65 (1H, s).

References

[1] Tetrahedron, 1996, vol. 52, # 6, p. 2199 - 2216
[2] Chemical Communications, 2013, vol. 49, # 77, p. 8626 - 8628
[3] Angewandte Chemie - International Edition, 2013, vol. 52, # 2, p. 762 - 766
[4] Angew. Chem., 2013, vol. 125, # 2, p. 791 - 796,6
[5] Chemistry - A European Journal, 2015, vol. 21, # 29, p. 10322 - 10325

2-METHOXY-6-METHYLBENZALDEHYDE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-METHOXY-6-METHYLBENZALDEHYDE Suppliers

China 79 India 1 Switzerland 1 United States 6 Global 87

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View Lastest Price from 2-METHOXY-6-METHYLBENZALDEHYDE manufacturers

Career Henan Chemical Co

Product: 2-METHOXY-6-METHYLBENZALDEHYDE 54884-55-8
Price: US $9.80/KG
Min. Order: 1KG
Purity: 97%-99%
Supply Ability: 1kg -1000kg
Release date: 2020-01-03

54884-55-8, 2-METHOXY-6-METHYLBENZALDEHYDERelated Search:

(+)-Bicuculline PSOROMIC ACID 2,4-DIMETHOXY-6-METHYLBENZALDEHYDE 7-HYDROXY-5-METHYLFLAVONE 2,3,4-Trimethoxy-6-methylbenzaldehyde (-)-BICUCULLINE METHOBROMIDE 6-Formyl-2,3-dimethoxybenzoic acid 5,7-DIMETHYLCHROMONE-3-CARBOXALDEHYDE FUMARPROTOCETRARIC ACID 1,5-dimethoxyanthraquinone STICTIC ACID 1,5-DIPHENOXYANTHRAQUINONE 1,8-diphenoxyanthraquinone 1,8-dimethoxyanthraquinone 1-(2-METHOXY-4,6-DIMETHYLPHENYL)ETHANONE 5-(CHLOROMETHYL)MECONIN AKOS 237-82 AKOS 220-64

2-METHOXY-6-METHYLBENZALDEHYDE

6-Methoxy-2-methylbenzaldehyde

Benzaldehyde, 2-Methoxy-6-Methyl-

54884-55-8