ChemicalBook > CAS DataBase List > N4-METHYL-6-CHLORO-5-NITROPYRIMIDIN-4-AMINE

N4-METHYL-6-CHLORO-5-NITROPYRIMIDIN-4-AMINE

Product Name
N4-METHYL-6-CHLORO-5-NITROPYRIMIDIN-4-AMINE
CAS No.
23126-82-1
Chemical Name
N4-METHYL-6-CHLORO-5-NITROPYRIMIDIN-4-AMINE
Synonyms
AKOS BBS-00003135;6-Chloro-N-methyl-5-nitro-4-pyrimidinamine;N4-METHYL-6-CHLORO-5-NITROPYRIMIDIN-4-AMINE;4-Pyrimidinamine, 6-chloro-N-methyl-5-nitro-
CBNumber
CB7260333
Molecular Formula
C5H5ClN4O2
Formula Weight
188.57
MOL File
23126-82-1.mol
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N4-METHYL-6-CHLORO-5-NITROPYRIMIDIN-4-AMINE Property

Melting point:
134 °C
Boiling point:
374.9±42.0 °C(Predicted)
Density 
1.582±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
pka
-0.74±0.10(Predicted)
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
C429353
Product name
6-Chloro-N-methyl-5-nitro-4-pyrimidinamine
Packaging
10mg
Price
$45
Updated
2021/12/16
Biosynth Carbosynth
Product number
FC156281
Product name
6-Chloro-N-methyl-5-nitro-4-pyrimidinamine
Packaging
250mg
Price
$100
Updated
2021/12/16
Biosynth Carbosynth
Product number
FC156281
Product name
6-Chloro-N-methyl-5-nitro-4-pyrimidinamine
Packaging
500mg
Price
$150
Updated
2021/12/16
Matrix Scientific
Product number
072587
Product name
6-Chloro-N-methyl-5-nitro-4-pyrimidinamine
Purity
95+%
Packaging
250mg
Price
$231
Updated
2021/12/16
AK Scientific
Product number
J50356
Product name
6-Chloro-N-methyl-5-nitro-4-pyrimidinamine
Packaging
250mg
Price
$234
Updated
2021/12/16
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N4-METHYL-6-CHLORO-5-NITROPYRIMIDIN-4-AMINE Chemical Properties,Usage,Production

Synthesis

4316-93-2

74-89-5

23126-82-1

To a stirred solution of 4,6-dichloro-5-nitropyrimidine (1.5 mmol), monomethylamine (0.5 mmol), Pd2(dba)3 (0.01 mmol), R-BINAP (0.03 mmol), and potassium carbonate (0.7 mmol) in toluene (5 mL) was reacted under argon protection for 3.5 hours at room temperature. Upon completion of the reaction, the mixture was filtered and concentrated. The residue was purified by silica gel column chromatography to afford the target product 6-chloro-N-methyl-5-nitro-4-pyrimidinamine.

References

[1] Chinese Chemical Letters, 2017, vol. 28, # 3, p. 583 - 587
[2] Patent: EP1598354, 2005, A1. Location in patent: Page/Page column 90
[3] Journal of Applied Chemistry, 1957, vol. 7, p. 109,112
[4] Journal of the American Chemical Society, 1957, vol. 79, p. 490,493
[5] European Journal of Medicinal Chemistry, 2010, vol. 45, # 8, p. 3389 - 3393

N4-METHYL-6-CHLORO-5-NITROPYRIMIDIN-4-AMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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N4-METHYL-6-CHLORO-5-NITROPYRIMIDIN-4-AMINE Suppliers

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23126-82-1, N4-METHYL-6-CHLORO-5-NITROPYRIMIDIN-4-AMINERelated Search:

6-CHLORO-5-NITROPYRIMIDIN-4-AMINE 4-(6-CHLORO-5-NITRO-4-PYRIMIDINYL)-1-PIPERAZINECARBOXYLIC ACID 1,1-DIMETHYLETHYL ESTER 4-CHLORO-6-(4-METHYL-1-PIPERAZINYL)-5-NITROPYRIMIDINE IFLAB-BB F2124-0125 IFLAB-BB F2124-0130 N4-METHYL-6-CHLORO-5-NITROPYRIMIDIN-4-AMINE 1-(6-CHLORO-5-NITRO-4-PYRIMIDINYL)-1,2,3,4-TETRAHYDROQUINOLINE IFLAB-BB F2124-0139 IFLAB-BB F2124-0138 4-CHLORO-5-NITRO-6-(1-PYRROLIDINYL)PYRIMIDINE IFLAB-BB F2124-0140 N-benzyl-6-chloro-5-nitro-4-pyrimidinamine IFLAB-BB F2124-0124 IFLAB-BB F2124-0129 6-CHLORO-N-ETHYL-5-NITRO-2-(TRIFLUOROMETHYL)PYRIMIDIN-4-AMINE AKOS BBS-00003136 IFLAB-BB F2124-0135 6-CHLORO-N-ISOPROPYL-5-NITRO-2-(TRIFLUOROMETHYL)PYRIMIDIN-4-AMINE

  • 6-Chloro-N-methyl-5-nitro-4-pyrimidinamine
  • N4-METHYL-6-CHLORO-5-NITROPYRIMIDIN-4-AMINE
  • AKOS BBS-00003135
  • 4-Pyrimidinamine, 6-chloro-N-methyl-5-nitro-
  • 23126-82-1